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Sensitive polar gas sensor using active surface of piezoelectric crystals and ultra-long propagation of surface acoustic wave

Research Project

Project/Area Number 24686013
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypePartial Multi-year Fund
Research Field Applied physics, general
Research InstitutionTohoku University

Principal Investigator

TSUJI Toshihiro  東北大学, 工学(系)研究科(研究院), 助教 (70374965)

Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥24,960,000 (Direct Cost: ¥19,200,000、Indirect Cost: ¥5,760,000)
Fiscal Year 2014: ¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2013: ¥6,110,000 (Direct Cost: ¥4,700,000、Indirect Cost: ¥1,410,000)
Fiscal Year 2012: ¥13,910,000 (Direct Cost: ¥10,700,000、Indirect Cost: ¥3,210,000)
Keywords圧電結晶 / 弾性表面波 / ボールSAWセンサ / 加工変質層 / 非晶質シリカ / 紫外線照射 / 微量水分 / 温度補償
Outline of Final Research Achievements

Active surface of piezoelectric crystals is useful for the detection of polar gas molecules when it is used as a sensitive film of a surface acoustic wave (SAW) sensor because of its low attenuation nature. In this work, the target polar gas is the trace moisture that is industrially important and the concentration is less than 1 ppm. During investigation, it was found that one of origins of quartz active surface was a damaged layer of amorphous silica and was imitated by the silica film synthesized by sol-gel reaction. In the case of application to the ball SAW sensor where significant long propagation of SAW is available, it was shown that the sensor could be used for the trace moisture sensor with high sensitivity and significant fast response.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (43 results)

All 2015 2014 2013 2012 Other

All Journal Article (12 results) (of which Acknowledgement Compliant: 5 results,  Peer Reviewed: 10 results,  Open Access: 4 results) Presentation (23 results) Book (3 results) Remarks (2 results) Patent(Industrial Property Rights) (3 results)

  • [Journal Article] ボールSAWセンサを用いた小型・高速・高感度な微量水分計の開発2015

    • Author(s)
      辻俊宏、渡邊圭、東出祐介、大泉透、竹田宣生、赤尾慎吾、塚原祐輔、山中一司
    • Journal Title

      圧電材料・デバイスシンポジウム2015講演論文集

      Volume: 2015 Pages: 107-112

    • Related Report
      2014 Annual Research Report
    • Acknowledgement Compliant
  • [Journal Article] Temperature Compensation of Ball SAW Sensor by Two-Frequency Measurement Using Undersampling2014

    • Author(s)
      T. Tsuji, T. Oizumi, N. Takeda, S. Akao, Y. Tsukahara, K. Yamanaka
    • Journal Title

      Proc. Symp. Ultrason. Electron.

      Volume: 35 Pages: 99-100

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Highly Sensitive Trace Moisture Ball Surface Acoustic Wave Sensor Using SiOx Film2014

    • Author(s)
      S. Hagihara, T. Tsuji, T. Oizumi, N. Takeda, S. Akao, T. Ohgi, K. Takayanagi, T. Yanagisawa, N. Nakaso, Y. Tsukahara, K. Yamanaka
    • Journal Title

      Jpn. J. Appl. Phys.

      Volume: 53(7)

    • NAID

      210000144234

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Detection of Trace Water Vapor Using SiO<i><sub>x</sub></i>-Coated Ball SAW Sensor2014

    • Author(s)
      K. Takayanagi, S. Akao, T. Yanagisaewa, N. Nakaso, Y. Tsukahara, S. Hagihara, T. Oizumi, N. Takeda, T. Tsuji, K. Yamanaka
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 55 Issue: 7 Pages: 988-993

    • DOI

      10.2320/matertrans.I-M2014807

    • NAID

      130004455325

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Highly Sensitive Ball Surface Acoustic Wave Hydrogen Sensor with Porous Pd-Alloy Film2014

    • Author(s)
      T. Tsuji, R. Mihara, T. Saito, S. Hagihara, T. Oizumi, N. Takeda, T. Ohgi, T. Yanagisawa, S. Akao, N. Nakaso, K. Yamanaka
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 55 Issue: 7 Pages: 1040-1044

    • DOI

      10.2320/matertrans.I-M2014816

    • NAID

      130004455338

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] SiOx膜を用いたボールSAWセンサによる高感度微量水分測定システムの開発2014

    • Author(s)
      萩原啓、大場俊弘、小清水秀和、辻俊宏、大泉透、竹田宣生、赤尾慎吾、大木恒郎、高柳浩介、柳沢恭行、中曽教尊、塚原祐輔、山中一司
    • Journal Title

      圧電材料・デバイスシンポジウム2014 講演論文集

      Volume: 2014 Pages: 47-52

    • Related Report
      2013 Annual Research Report
  • [Journal Article] Highly Sensitive Trace Moisture Ball SAW Sensor Using SiOx film2013

    • Author(s)
      Satoshi Hagihara, Toshihiro Tsuji, Toru Oizumi, Nobuo Takeda, Shingo Akao, Tsuneo Ohgi, Kosuke Takayanagi, Takayuki Yanagisawa, Noritaka Nakaso, Yusuke Tsukahara, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 34 Pages: 381-382

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fast and Sensitive Ball SAW Hydrogen Sensor with Porous Pd-Pt Alloy film2013

    • Author(s)
      Toshihiro Tsuji, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Tsuneo Ohgi, Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 34 Pages: 155-156

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Measurement of Trace Moisture Using Ball SAW Sensor2012

    • Author(s)
      Satoshi Hagihara, Toshihiro Tsuji, Toru Oizumi, Nobuo Takeda, Shingo Akao, Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 33 Pages: 439-440

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Frequency Dependence Analysis of Ball SAW Sensor's Response2012

    • Author(s)
      Toshihiro Tsuji, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Shingo Akao, Kosuke Takayanagi, Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Journal Title

      Proceedings of Symposium on Ultrasonic Electronics

      Volume: 33 Pages: 49-50

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of High Precision Metal Micro-Electro-Mechanical-Systems Column for Portable Surface Acoustic Wave Gas Chromatograph2012

    • Author(s)
      Iwaya Takamitsu, Akao Shingo, Sakamoto Toshihiro, Tsuji Toshihiro, Nakaso Noritaka, Yamanaka Kazushi
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 51 Issue: 7S Pages: 07GC24-07GC24

    • DOI

      10.1143/jjap.51.07gc24

    • NAID

      210000140947

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Continuous Measurement of Multiple Gases Using Ball Surface Acoustic Wave Gas Chromatograph2012

    • Author(s)
      Takamitsu IWAYA, Shingo AKAO, Toshihiro SAKAMOTO, Toshihiro TSUJI, Noritaka NAKASO, Kazushi YAMANAKA
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 51 Issue: 7S Pages: 07GC22-07GC22

    • DOI

      10.1143/jjap.51.07gc22

    • NAID

      210000140945

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Presentation] ゾルゲルSiOx膜を用いたボールSAW微量水分センサの低ガス流量 における感度2015

    • Author(s)
      辻 俊宏, 渡邊 圭, 東出 祐介, 大泉 透, 竹田 宣生, 赤尾 慎吾, 塚原 祐輔, 山 中 一司
    • Organizer
      応用物理学会春季学術講演会
    • Place of Presentation
      東海大学(神奈川)
    • Year and Date
      2015-03-11 – 2015-03-14
    • Related Report
      2014 Annual Research Report
  • [Presentation] アンダーサンプリングを用いた実用的ボールSAWセンサ2015

    • Author(s)
      辻 俊宏, 大泉 透, 竹田 宣生, 赤尾 慎 吾, 塚原 祐輔, 山中 一司
    • Organizer
      応用物理学会春季学術講演会
    • Place of Presentation
      東海大学(神奈川)
    • Year and Date
      2015-03-11 – 2015-03-14
    • Related Report
      2014 Annual Research Report
  • [Presentation] ボールSAWセンサを用いた小型・高速・高感度な微量水分計の開発2015

    • Author(s)
      辻俊宏、渡邊圭、東出祐介、大泉透、竹田宣生、赤尾慎吾、塚原祐輔、山中一司
    • Organizer
      圧電材料・デバイスシンポジウム
    • Place of Presentation
      東北大学(仙台)
    • Year and Date
      2015-02-18 – 2015-02-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] Temperature compensation of ball SAW sensor by two-frequency measurement using undersampling2014

    • Author(s)
      Toshihiro Tsuji, Toru Oizumi, Nobuo Takeda, Shingo Akao, Yusuke Tsukahara, Kazushi Yamanaka
    • Organizer
      Symposium on Ultrasonic Electronics
    • Place of Presentation
      明治大学(東京)
    • Year and Date
      2014-12-03 – 2014-12-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] Vacuum pressure sensor available beyond atmospheric pressure using leaky attenuation of ball surface acoustic wave sensor2014

    • Author(s)
      T. Tsuji, T. Oizumi, N. Takeda, T. Ohgi, T. Yanagisawa, S. Akao, N. Nakaso, K. Yamanaka
    • Organizer
      IEEE IUS
    • Place of Presentation
      米国シカゴ
    • Year and Date
      2014-09-03 – 2014-09-06
    • Related Report
      2014 Annual Research Report
  • [Presentation] Trace moisture measurement of 10 nmol/mol using a 3mm diameter silica coated ball SAW sensor2014

    • Author(s)
      K. Yamanaka, S. Hagihara, T. Tsuji, T. Oizumi, N. Takeda, S. Akao, T. Ohgi, K. Takayanagi, T. Yanagisawa, N. Nakaso, Y. Tsukahara
    • Organizer
      IEEE IUS
    • Place of Presentation
      米国シカゴ
    • Year and Date
      2014-09-03 – 2014-09-06
    • Related Report
      2014 Annual Research Report
  • [Presentation] 微量水分計測のためのボールSAWセンサシステムの高度化2014

    • Author(s)
      辻俊宏、萩原啓、大場俊弘、小清水秀和、大泉透、竹田宣生、赤尾慎吾、大木恒郎、高柳浩介、柳沢恭行、中曽教尊、塚原祐輔、山中一司
    • Organizer
      第61回応用物理学会春季学術講演会
    • Place of Presentation
      神奈川県
    • Related Report
      2013 Annual Research Report
  • [Presentation] SiOx膜を用いたボールSAWセンサによる高感度微量水分測定システムの開発2014

    • Author(s)
      萩原啓、大場俊弘、小清水秀和、辻俊宏、大泉透、竹田宣生、赤尾慎吾、大木恒郎、高柳浩介、柳沢恭行、中曽教尊、塚原祐輔、山中一司
    • Organizer
      圧電材料・デバイスシンポジウム2014
    • Place of Presentation
      宮城
    • Related Report
      2013 Annual Research Report
  • [Presentation] ボールSAWセンサを用いた微量水分の高感度測定2013

    • Author(s)
      萩原啓、斎藤智弘、三原亮插.大泉透、竹田宣生、赤尾慎吾、大木恒郎、柳沢恭行、高柳浩介、中曽教尊、辻俊宏、塚原祐輔、山中一司
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      神奈川
    • Year and Date
      2013-03-29
    • Related Report
      2012 Annual Research Report
  • [Presentation] Pd-Pt合金膜を用いたボールSAWセンサによる水素の高感度計測2013

    • Author(s)
      辻俊宏、三原亮祐、斎藤智弘、萩原啓、大泉透、竹田宣生、大木恒郎、柳沢恭行、赤尾慎吾、中曽教尊、山中一司
    • Organizer
      第60回応用物理学会春季学術講演会
    • Place of Presentation
      神奈川
    • Year and Date
      2013-03-29
    • Related Report
      2012 Annual Research Report
  • [Presentation] Pd-Pt合金膜を用いたボールSAWセンサによる水素の高感度計測2013

    • Author(s)
      辻俊宏、三原亮祐、斎藤智弘、萩原啓、大泉透、竹田宣生、大木恒郎、柳沢恭行、赤尾慎吾、中曽教尊、山中一司
    • Organizer
      圧電材料.デバイスシンポジウム2013
    • Place of Presentation
      宮城
    • Year and Date
      2013-01-28
    • Related Report
      2012 Annual Research Report
  • [Presentation] Highly Sensitive Trace Moisture Ball SAW Sensor Using SiOx film2013

    • Author(s)
      Satoshi Hagihara, Toshihiro Tsuji, Toru Oizumi, Nobuo Takeda, Shingo Akao, Tsuneo Ohgi, Kosuke Takayanagi, Takayuki Yanagisawa, Noritaka Nakaso, Yusuke Tsukahara, Kazushi Yamanaka
    • Organizer
      The 34th Symposium on Ultrasonic Electronics USE2013
    • Place of Presentation
      京都
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fast and Sensitive Ball SAW Hydrogen Sensor with Porous Pd-Pt Alloy film2013

    • Author(s)
      Toshihiro Tsuji, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Tsuneo Ohgi, Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      The 34th Symposium on Ultrasonic Electronics USE2013
    • Place of Presentation
      京都
    • Related Report
      2013 Annual Research Report
  • [Presentation] Response of quartz ball surface acoustic wave (SAW) sensor2013

    • Author(s)
      Kazushi Yamanaka, Satoshi Hagihara, Tomohiro Saito, Toru Oizumi, Nobuo Takeda, Shingo Akao, Kosuke Takayanagi, Takayuki Yanagisawa, Noritaka Nakaso, Yusuke Tsukahara, Toshihiro Tsuji
    • Organizer
      2013 Joint UFFC, EFTF, and PFM Symposium
    • Place of Presentation
      チェコ共和国, プラハ
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fast and Sensitive H2 detection by ball surface acoustic wave (SAW) sensor with porous Pd-Pt alloy film2013

    • Author(s)
      Toshihiro Tsuji, Ryosuke Mihara, Tomohiro Saito, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Tsuneo Ohgi, Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      2013 Joint UFFC, EFTF, and PFM Symposium
    • Place of Presentation
      チェコ共和国, プラハ
    • Related Report
      2013 Annual Research Report
  • [Presentation] Detection of Trace Water Vapor Using SiOx-Coated Ball SAW Sensor2013

    • Author(s)
      Kosuke Takayanagi, Tsuneo Ohgi, Shingo Akao, Noritaka Nakaso, Yusuke Tsukahara, Yoshikazu Ohara, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      3rd International Symposium on Laser Ultrasonics and Advanced Sensing
    • Place of Presentation
      神奈川県
    • Related Report
      2013 Annual Research Report
  • [Presentation] Meander Propagation Route of Suface Acoustic Wave on a Trigonal Crystal Ball Observed Using Non Contact electrodes2013

    • Author(s)
      Takayuki Yanagisawa, Tsuneo Ohgi, Shingo Akao, Noritaka Nakaso, Yusuke Tsukahara, Yoshikazu Ohara, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      3rd International Symposium on Laser Ultrasonics and Advanced Sensing
    • Place of Presentation
      神奈川県
    • Related Report
      2013 Annual Research Report
  • [Presentation] Measurement of trace water vapor using ball surface acoustic wave (SAW) sensor2013

    • Author(s)
      Satoshi Hagihara, Tomohiro Saito, Rosuke Mihara, Toru Oizumi, Nobuo Takada, Shingo Akao, Tsuneo Ohgi, Kosuke Takayanagi, Takayuki Yanagisawa, Noritaka Nakaso, Toshihiro Tsuji, Kazushi Yamanaka
    • Organizer
      3rd International Symposium on Laser Ultrasonics and Advanced Sensing
    • Place of Presentation
      神奈川県
    • Related Report
      2013 Annual Research Report
  • [Presentation] Highly Sensitive Ball SAW Hydrogen Sensor with Porous Pd Alloy film2013

    • Author(s)
      Toshihiro Tsuji, Rosuke Mihara, Tomohiro Saito, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Tsuneo Ohgi, Takayuki Yanagisawa, Shingo Akao, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      3rd International Symposium on Laser Ultrasonics and Advanced Sensing
    • Place of Presentation
      神奈川県
    • Related Report
      2013 Annual Research Report
  • [Presentation] Measurement of Trace Moisture Using Ball SAW Sensor2012

    • Author(s)
      Satoshi Hagihara, Toshihiro Tsuji, Toru Oizumi, Nobuo Takeda, Shingo Akao, Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      第33回超音波エレクトロニクスの基礎と応用に関するシンポジウム
    • Place of Presentation
      千葉
    • Year and Date
      2012-11-15
    • Related Report
      2012 Annual Research Report
  • [Presentation] Frequency Dependence Analysis of Ball SAW Sensor's Response2012

    • Author(s)
      Toshihiro Tsuji, Satoshi Hagihara, Toru Oizumi, Nobuo Takeda, Shingo Akao, Kosuke Takayanagi, Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      第33回超音波エレクトロニクスの基礎と応用に関するシンポジウム
    • Place of Presentation
      千葉
    • Year and Date
      2012-11-13
    • Related Report
      2012 Annual Research Report
  • [Presentation] Measurement of Trace Moisture by Differential Operation of Dual Ball SAW Sensors2012

    • Author(s)
      Toshihiro Tsuji, Satoshi Hagihara, Shingo Akao, Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      2012 IEEE International Ultrasonic Symposium (IUS)
    • Place of Presentation
      ドイツ、ドレスデン
    • Year and Date
      2012-10-09
    • Related Report
      2012 Annual Research Report
  • [Presentation] Continuous Monitoring of Multiple-Gas Concentrations Using Ball SAW Gas2012

    • Author(s)
      Satoshi Hagihara, Tosihiro Tsuji, Toru Oizumi, Shingo Akao, Kosuke Takayanagi Tsuneo Ohgi, Takayuki Yanagisawa, Noritaka Nakaso, Kazushi Yamanaka
    • Organizer
      2012 IEEE International Ultrasonic Symposium (IUS)
    • Place of Presentation
      ドイツ、ドレスデン
    • Year and Date
      2012-10-09
    • Related Report
      2012 Annual Research Report
  • [Book] Advance in Acoustic Microscory and High Resolution Imaging 12 Ultrasonic atomic force microscopy2013

    • Author(s)
      Kazushi Yamanaka, Toshihiro Tsuji
    • Publisher
      Wiley-VCH
    • Related Report
      2012 Annual Research Report
  • [Book] ULTRASONIC ATOMIC FORCE MICROSCOPY Characterization of MATERIALS vol.3 (2012)2012

    • Author(s)
      Kazushi Yamanaka, Toshihiro Tsuji
    • Publisher
      Springer
    • Related Report
      2012 Annual Research Report
  • [Book] Acoustic Scanning Probe Microscopy Chapter6 Ultrasonic Atomic Force Microscopy2012

    • Author(s)
      Kazushi Yamanaka, Toshihiro Tsuji
    • Publisher
      Springer
    • Related Report
      2012 Annual Research Report
  • [Remarks] http://www.material.tohoku.ac.jp/~hyoka/lab.html

    • Related Report
      2013 Annual Research Report
  • [Remarks]

    • URL

      http://www.material.tohoku.ac.jp~hyoka/database_year_j.html

    • Related Report
      2012 Annual Research Report
  • [Patent(Industrial Property Rights)] 簡易型電気信号処理装置2014

    • Inventor(s)
      山中一司、辻俊宏、大泉透
    • Industrial Property Rights Holder
      山中一司、辻俊宏、大泉透
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-241817
    • Filing Date
      2014-11-28
    • Related Report
      2014 Annual Research Report
  • [Patent(Industrial Property Rights)] 水分濃度センサ2013

    • Inventor(s)
      高柳浩介、塚原祐輔、山中一司、辻俊宏
    • Industrial Property Rights Holder
      凸版印刷株式会社、国立大学法人東北大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2013-130728
    • Filing Date
      2013-06-21
    • Related Report
      2013 Annual Research Report
  • [Patent(Industrial Property Rights)] ガスセンサ2012

    • Inventor(s)
      辻俊宏、山中一司、小原良和、坂本俊宏、岩谷隆光
    • Industrial Property Rights Holder
      国立大学法人東北大学
    • Filing Date
      2012-12-06
    • Related Report
      2012 Annual Research Report

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Published: 2012-04-24   Modified: 2019-07-29  

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