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Combined Measurement of Translational and Rotational Motion of Nanocrystals using Coherent X-rays

Research Project

Project/Area Number 24710092
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Quantum beam science
Research InstitutionThe University of Tokyo

Principal Investigator

SHINOHARA YUYA  東京大学, 新領域創成科学研究科, 助教 (60451861)

Project Period (FY) 2012-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2013: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2012: ¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
KeywordsX線光子相関分光法 / ダイナミクス / コヒーレントX線 / X線光子相関分光法 / コヒーレントX線 / マイクロレオロジー
Research Abstract

In this research project, we have developed an experimental technique for the observation of translational and rotational motion of nanocrystals in soft matter by using quasi-monochromatic and quasi-coherent X-rays. When coherent X-rays illuminates samples, granular scattering patterns called speckle are observed. By analyzing temporal fluctuation of the speckle intensity, information on the translational motion of nanocrystals can be obtained. Rotational motion of nanocrystals is analyzed by tracking the movement of diffraction spots from nanocrystals. By combining these techniques, we have successfully analyzed complex dynamics of crystalline carbon black nanoparticles in styrene-butadiene rubber. This study opens up the possibility of using X-rays as a probe of microrheology.

Report

(3 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Research-status Report
  • Research Products

    (21 results)

All 2014 2013 2012

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (20 results) (of which Invited: 7 results)

  • [Journal Article] Combined Measurement of X-ray Photon Correlation Spectroscopy and Diffracted X-ray Tracking using Pink Beam X-rays2013

    • Author(s)
      Yuya Shinohara, Akira Watanabe, Hiroyuki Kishimoto, and Yoshiyuki Amemiya
    • Journal Title

      Journal of Synchrotron Radiation

      Volume: 20 Issue: 5 Pages: 801-804

    • DOI

      10.1107/s090904951301844x

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed
  • [Presentation] Observation of Rotational and Translational Motion of Nanocrystals using Pink-beam X-rays2014

    • Author(s)
      篠原佑也,渡部慧,岸本浩通,雨宮慶幸
    • Organizer
      The 6^<th> Japan-Taiwan Joint Meeting on Neutron and X-ray Scattering
    • Place of Presentation
      台北、台湾
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Translational and Rotational Motion of Nanocrystals in Rubber2014

    • Author(s)
      篠原佑也,渡部慧,岸本浩通,雨宮慶幸
    • Organizer
      APS March Meeting 2014
    • Place of Presentation
      Denver USA
    • Related Report
      2013 Final Research Report
  • [Presentation] ゴム中のナノ粒子の並進及び回転運動の同時測定2014

    • Author(s)
      渡部慧、篠原佑也、岸本浩通、雨宮慶幸
    • Organizer
      日本放射光学会年会
    • Place of Presentation
      広島国際会議場
    • Related Report
      2013 Final Research Report
  • [Presentation] ゴム中のナノ粒子の並進運動及び回転運動の同時計測2014

    • Author(s)
      渡部慧
    • Organizer
      日本放射光学会年会・合同シンポジウム
    • Place of Presentation
      広島国際会議場
    • Related Report
      2013 Annual Research Report
  • [Presentation] Translational and Rotational Motion of Nanocrystals in Rubber2014

    • Author(s)
      篠原佑也
    • Organizer
      APS March Meeting 2014
    • Place of Presentation
      Denver, USA
    • Related Report
      2013 Annual Research Report
  • [Presentation] Observation of Rotational and Translational Motion of Nanocrystals2014

    • Author(s)
      篠原佑也
    • Organizer
      The 6th Taiwan-Japan Joint Meeting on X-ray and Neutron Scattering
    • Place of Presentation
      台北、台湾
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 小角X線散乱法を用いたタイヤゴム中でのナノ粒子構造・ダイナミクスの観察2013

    • Author(s)
      篠原佑也
    • Organizer
      SPring-8利用推進評議会
    • Place of Presentation
      神戸クリスタルタワー
    • Year and Date
      2013-04-16
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] 準単色コヒーレントX線を用いたナノ結晶の並進・回転運動の観察2013

    • Author(s)
      篠原佑也、渡部慧、岸本浩通、雨宮慶幸
    • Organizer
      第62回高分子討論会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Final Research Report
  • [Presentation] Observation of Translational and Rotational Motion of Nanocrystals with Coherent X-rays2013

    • Author(s)
      篠原佑也,渡部慧,岸本浩通,雨宮慶幸
    • Organizer
      Light and Particle Beams in Materials Science 2013
    • Place of Presentation
      つくば国際会議場
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] コヒーレントX線を用いたナノ結晶の並進運動と回転運動の同時測定2013

    • Author(s)
      渡部慧、篠原佑也、岸本浩通、雨宮慶幸
    • Organizer
      日本放射光学会年会
    • Place of Presentation
      名古屋大学
    • Related Report
      2013 Final Research Report
  • [Presentation] 準単色コヒーレントX線を用いたナノ結晶の並進・回転運動の観察2013

    • Author(s)
      篠原佑也
    • Organizer
      高分子討論会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] 小角散乱を用いたタイヤゴム中でのナノ粒子構造・ダイナミクスの観察2013

    • Author(s)
      篠原佑也
    • Organizer
      SPring-8利用推進協議会
    • Place of Presentation
      神戸クリスタルタワー
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Observation of Transkational and Rotational Motion of Nanocrystals with Coherent X-rays2013

    • Author(s)
      篠原佑也
    • Organizer
      Light and Particle Beams in Materials Science 2013
    • Place of Presentation
      つくば国際会議場
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] コヒーレントX線を用いたナノ結晶の並進運動と回転運動の同時測定2013

    • Author(s)
      渡部慧
    • Organizer
      日本放射光学会年会
    • Place of Presentation
      名古屋大学
    • Related Report
      2012 Research-status Report
  • [Presentation] Translational-Rotational Motion of Nanocrystals with Coherent X-rays2012

    • Author(s)
      篠原佑也,渡部慧,岸本浩通,雨宮慶幸
    • Organizer
      SAS2012
    • Place of Presentation
      Sydney, Australia
    • Related Report
      2013 Final Research Report
  • [Presentation] Dynamics of Nanoparticles in Rubber Observed with Coherent X-rays2012

    • Author(s)
      篠原佑也
    • Organizer
      SAS2012
    • Place of Presentation
      ydney, Australia, plenary
    • Related Report
      2013 Final Research Report
  • [Presentation] コヒーレントX線を用いたナノ結晶の並進・回転運動の同時測定法2012

    • Author(s)
      篠原佑也
    • Organizer
      第61回高分子討論会
    • Place of Presentation
      名古屋工業大学
    • Related Report
      2013 Final Research Report
  • [Presentation] コヒーレントX線を用いたナノ結晶の並進・回転運動の同時測定法2012

    • Author(s)
      篠原佑也
    • Organizer
      高分子討論会
    • Place of Presentation
      名古屋工業大学
    • Related Report
      2012 Research-status Report
  • [Presentation] Combined Measurement of Translational-Rotational Motion of Nanocrystals with Coherent X-rays2012

    • Author(s)
      篠原佑也
    • Organizer
      SAS2012
    • Place of Presentation
      Sydney, Australia
    • Related Report
      2012 Research-status Report
  • [Presentation] Dynamics of Nanoparticles in Rubber Observed with Coherent X-rays2012

    • Author(s)
      篠原佑也
    • Organizer
      SAS2012
    • Place of Presentation
      Sydney, Australia
    • Related Report
      2012 Research-status Report
    • Invited

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Published: 2013-05-31   Modified: 2019-07-29  

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