Mechanistic Studies of Synthetic Organic Reactions Using Quantitative Mass Spectrometry
| Project/Area Number |
24750036
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| Research Category |
Grant-in-Aid for Young Scientists (B)
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| Allocation Type | Multi-year Fund |
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| Research Field |
Organic chemistry
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| Research Institution | University of Shizuoka |
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Principal Investigator |
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| Project Period (FY) |
2012-04-01 – 2014-03-31
|
| Project Status |
Completed (Fiscal Year 2013)
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| Budget Amount *help |
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2013: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Fiscal Year 2012: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
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| Keywords | 有機合成化学 / 質量分析 / 反応機構 / 触媒 / 反応中間体 / 有機合成 |
|---|
| Research Abstract |
In this study, mechanistic study using mass spectrometry was conducted by detecting trace amounts of unstable catalysts and reaction intermediates. Use of soft ionization method enabled detection of such species. In the same time, reaction monitoring by combining mass spectrometer and autosampler was tried to realize quantification of chemical species in the reaction.
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Report
(3 results)
Research Products
(38 results)
