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Surface functionalization of composite materials using soluble mold and imprinting lithography

Research Project

Project/Area Number 24760086
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Research InstitutionTokyo University of Science

Principal Investigator

MATSUZAKI Ryosuke  東京理科大学, 理工学部, 講師 (20452013)

Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2014: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2013: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywords複合材料 / CFRP / 表面処理 / ナノインプリント / 破壊靭性 / DCB試験 / 溶解性モールド / 表面修飾 / 接着 / インプリントリソグラフィ / インプリント / 接着強度
Outline of Final Research Achievements

To improve the adhesive strength, we performed surface modification of carbon fiber reinforced plastics (CFRP) using Nano-imprint lithography (NIL). Because a metal mold was used in the conventional process, the manufactured surface was limited to the 2.5 dimension. We propose an imprint process of three-dimensional shape with interlock structure using a soluble mold. We fabricated the soluble mold using negative photoresist by inclined exposure method, and investigated the fracture toughness of three-dimensional structures using DCB tests. As a result, it was found that the higher fracture toughness can be obtained by using imprint lithography compared with the conventional surface treatment using abrasive paper.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (16 results)

All 2015 2014 2013 Other

All Journal Article (4 results) (of which Peer Reviewed: 4 results) Presentation (10 results) Remarks (2 results)

  • [Journal Article] Effects of mixed-mode ratio and step-shaped micro pattern surface on crack-propagation resistance of carbon-fiber-reinforced plastic/adhesive interface2015

    • Author(s)
      Yoshikazu Yukimoto, Ryosuke Matsuzaki, Akira Todoroki
    • Journal Title

      Composites Part A

      Volume: 69 Pages: 139-149

    • DOI

      10.1016/j.compositesa.2014.11.014

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Mode II interfacial fracture toughness of composite/adhesive interfaces obtained by in-mold surface modification2014

    • Author(s)
      Yoshikazu Yukimoto, Ryosuke Matsuzaki and Akira Todoroki
    • Journal Title

      International Journal of Adhesives and Adhesion

      Volume: 50 Pages: 191-198

    • DOI

      10.1016/j.ijadhadh.2014.01.034

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Crack growth analysis of a composite/adhesive interface toughened by in-mold surface preparation2013

    • Author(s)
      Takuya Suzuki, Ryosuke Matsuzaki, Akira Todoroki, and Yoshihiro Mizutani
    • Journal Title

      International Journal of Adhesives and Adhesion

      Volume: 42 Pages: 36-43

    • DOI

      10.1016/j.ijadhadh.2013.01.008

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Enhancement of interfacial fracture toughness of carbon/epoxy composite adhesive joints by in-mold surface preparation2013

    • Author(s)
      Yuki Hikosaka, Ryosuke Matsuzaki, Akira Todoroki and Yoshihiro Mizutani
    • Journal Title

      eXPRESS Polymer Letters

      Volume: 7 Issue: 3 Pages: 293-303

    • DOI

      10.3144/expresspolymlett.2013.26

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] ナノカーボンと複合材料成形2015

    • Author(s)
      松崎亮介
    • Organizer
      ナノカーボン研究会
    • Place of Presentation
      東京理科大学神楽坂キャンパス(東京)
    • Year and Date
      2015-03-17
    • Related Report
      2014 Annual Research Report
  • [Presentation] 電極による電場印加を用いた熱硬化性樹脂の成形シミュレーション2015

    • Author(s)
      羽鳥伸哉, 松崎亮介
    • Organizer
      日本複合材料学会日本複合材料会議
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京)
    • Year and Date
      2015-03-04 – 2015-03-06
    • Related Report
      2014 Annual Research Report
  • [Presentation] インプリントによる溶解性モールドを用いた3次元表面複合材料の創製2014

    • Author(s)
      加藤秀昌, 松崎亮介
    • Organizer
      日本機械学会関東学生会第53回学生員卒業研究発表講演会
    • Place of Presentation
      東京農工大学 (東京)
    • Related Report
      2013 Research-status Report
  • [Presentation] Evaluation of the fracture toughenss of composite/adhesive interface applied by inmold surface modification under mode II loading2013

    • Author(s)
      Yoshikazu Yukimoto, Ryosuke Matsuzaki
    • Organizer
      Proceedings of 19th International Conference on Composite Materilas
    • Place of Presentation
      Montreal, Canada
    • Related Report
      2013 Research-status Report
  • [Presentation] インモールド表面処理を施した複合材接着界面モードII破壊靱性の実験的評価2013

    • Author(s)
      雪本善和, 松崎亮介, 轟 章
    • Organizer
      日本材料学会学術講演会
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Research-status Report
  • [Presentation] Evaluation of interfacial fracture toughness of CFRP/ adhesives treated by in-mold surface preparation2013

    • Author(s)
      Yoshikazu Yukimoto, Ryosuke Matsuzaki
    • Organizer
      Proceedings of 13th Japan International SAMPE Symposium and Exhibition (JISSE)
    • Place of Presentation
      Nagoya, Tokyo
    • Related Report
      2013 Research-status Report
  • [Presentation] Evaluation of The Fracture Toughness of CFRP/Adhesives Interface Treated by In-mold Surface Modification2013

    • Author(s)
      (164) Yoshikazu Yukimoto, Ryosuke Matsuzaki, Akira Todoroki
    • Organizer
      Proceedings of Japan-Korea Joint symposium on composite materials
    • Place of Presentation
      Kagoshima University, Kagoshima
    • Related Report
      2013 Research-status Report
  • [Presentation] 溶解性モールドを用いたインプリントによる3次元表面複合材料の創製2013

    • Author(s)
      橘和尚史, 松崎亮介
    • Organizer
      日本機械学会関東支部講演会講演論文集
    • Place of Presentation
      首都大学東京
    • Related Report
      2012 Research-status Report
  • [Presentation] インモールド表面処理を施したCFRP/接着剤界面の評価2013

    • Author(s)
      松崎亮介, 轟章, 水谷義弘
    • Organizer
      日本材料学会第106回フラクトグラフィ部門委員会
    • Place of Presentation
      埼玉大学東京ステーションカレッジ
    • Related Report
      2012 Research-status Report
  • [Presentation] インモールド表面処理を施した複合材のモードII接着界面破壊靱性の評価2013

    • Author(s)
      雪本善和, 松崎亮介, 轟 章
    • Organizer
      日本複合材料合同会議
    • Place of Presentation
      東京大学
    • Related Report
      2012 Research-status Report
  • [Remarks] Resarch | Matsuzaki Laboratory

    • URL

      http://www.rs.tus.ac.jp/rmatsuza/research.html

    • Related Report
      2013 Research-status Report
  • [Remarks] Matsuzaki Laboratory

    • URL

      http://www.rs.tus.ac.jp/rmatsuza/index.html

    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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