Development of Stress-Mapping Technique with Sub-Microscale Spatial Resolution by Angular dispersive Micro-Raman spectroscopy
Project/Area Number |
24760088
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Research Category |
Grant-in-Aid for Young Scientists (B)
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Allocation Type | Multi-year Fund |
Research Field |
Materials/Mechanics of materials
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Research Institution | Meijo University |
Principal Investigator |
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Project Period (FY) |
2012-04-01 – 2014-03-31
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Project Status |
Completed (Fiscal Year 2013)
|
Budget Amount *help |
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2013: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2012: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
|
Keywords | 顕微ラマン分光法 / 角度分散 / 結晶方位 / 応力マッピング測定 / サブミクロン空間分解能 / 結晶方位測定 |
Research Abstract |
In this study, angular-dispersive-type micro-Raman spectroscopy was developed. In this instrument, the angular dispersive optical system that laser light was made incident from three directions (0, 50, and 100 degree) and detection was in the direction of 0 degree, was constructed. It was successful to determine the crystallographic orientation of Alumina by using angular dispersive properties. Especially, the directions of a-axis and c-axis were determined. Finally, for polycrystalline partially stabilized zirconia (PSZ), the possibility of stress measurement by angular dispersive properties was examined. The amount of Raman shift of PSZ under mechanical loading changed with the incidence angle, and the angular dispersion property was confirmed to be useful for stress measurement of polycrystalline material.
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Report
(3 results)
Research Products
(10 results)