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In-situ study of deformation and fracture dynamics of functional ceramics

Research Project

Project/Area Number 24760532
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Physical properties of metals
Research InstitutionTohoku University

Principal Investigator

CHEN Chunlin  東北大学, 原子分子材料科学高等研究機構, 助手 (50614989)

Project Period (FY) 2012-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2013: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Fiscal Year 2012: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywords表面 / 界面 / 粒界物性 / 動的ナノ計測 / 変形破壊力学
Research Abstract

Understanding of origin of materials fracture is the key point to prevent their damages, and also is an important subject of materials science. Through a combined study of in-situ TEM nanoindentation and advanced microscopy, we investigate the microstructure evolution of ceramics during nano-deformation, and study the mechanism of materials fracture.
There is no obvious plastic deformation during the nanoindentation of 4H-SiC. The emission of dislocation also cannot be seen. A micro-crack is formed and propagates along on the (0001) crystal plane. After unloading, dislocations are observed at the tip of the crack. It suggests that the dangling bonds on the surfaces of crack rebound and the healing of crack take place. Effects of grain boundaries on the mechanical properties of cubic BN have been studied. It is found that Sigma9 and sigma3 GBs of cubic BN are inclined to trap oxygen, which lowers the GB adhesion energies significantly, and greatly reduces the hardness of cubic BN.

Report

(3 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Research-status Report
  • Research Products

    (18 results)

All 2014 2013 2012

All Journal Article (11 results) (of which Peer Reviewed: 11 results,  Acknowledgement Compliant: 1 results) Presentation (7 results)

  • [Journal Article] Fluorine in Shark Teeth: Its Direct Atomic-Resolution Imaging and Strengthening Function2014

    • Author(s)
      Chen, Chunlin; Wang, Zhongchang; Saito, Mitsuhiro; Tohei, Tetsuya; Takano, Yoshiro; Ikuhara, Yuichi
    • Journal Title

      Angewandte Chemie

      Volume: 126 Issue: 6 Pages: 1569-1573

    • DOI

      10.1002/anie.201307689

    • Related Report
      2013 Annual Research Report 2013 Final Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Oxygen segregation at coherent grain boundaries of cubic born nitride2013

    • Author(s)
      C. Chen, S. Lv, Z. Wang, M. Saito, N. Shibada, T. Taniguchi, Y .Ikuhara
    • Journal Title

      Applied Physics Letters

      Volume: 102 Issue: 9 Pages: 91607-91607

    • DOI

      10.1063/1.4795300

    • Related Report
      2013 Final Research Report 2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effect of pretreatment and annealing on microstructure and mechanical properties of Mg–1.5Zn–0.25Gd (at%) alloys reinforced with quasicrystal2013

    • Author(s)
      H. Huang, C. L. Chen, Z. C. Wang, Y. P. Li, G. Y. Yuan
    • Journal Title

      Mater. Sci. Eng. A

      Volume: 581 Pages: 73-82

    • DOI

      10.1016/j.msea.2013.06.003

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Atomic-scale Structure and Electronic Property of the La_2FeCrO_6/SrTiO_3 Interface2013

    • Author(s)
      S. Lv, M. Saito, Z. Wang, C. Chen, S. Chakraverty, M. Kawasaki, Y. Ikuhara
    • Journal Title

      Journal of Applied Physics

      Volume: 114 Issue: 11 Pages: 113705-113705

    • DOI

      10.1063/1.4821795

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Excellent mechanical properties of an ultrafine-grained quasicrystalline strengthened magnesium alloy with multi-modal microstructure2013

    • Author(s)
      H. Huang, G. Y. Yuan, C. L. Chen, W. J. Ding, Z. C. Wang
    • Journal Title

      Materials Letters

      Volume: 107 Pages: 181-184

    • DOI

      10.1016/j.matlet.2013.06.006

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis and Characterization of CeO_2 Nano-rods2013

    • Author(s)
      Y. Chen, ... Z. C. Wang
    • Journal Title

      Ceramics International

      Volume: (掲載確定)(On line) Issue: 6 Pages: 6607-6610

    • DOI

      10.1016/j.ceramint.2013.01.096

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Icosahedral Quasicrystalline Fraction and Extrusion Ratio on Microstructure, Mechanical Properties, and Anisotropy of Mg-Zn-Gd-Based Alloys2013

    • Author(s)
      H. Huang, G. Y. Yuan, Z. C. Wang, 他2名
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 44 Issue: 6 Pages: 2725-2734

    • DOI

      10.1007/s11661-013-1609-y

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Facile synthesis of hybrid hexagonal CeF3 nano・disks on Ce02 frustum pyramids2013

    • Author(s)
      Y. Chen, T. Liu, C. Chen, R. Sun, S. Lv, M. Saito, S. Tsukimoto, Z. Wang
    • Journal Title

      Materials Letters

      Volume: 92 Pages: 7-10

    • DOI

      10.1016/j.matlet.2012.10.068

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Hydrothermal Synthesis of Ceria Hybrid Architectures of Nano-rods and Nano-octahedrons2013

    • Author(s)
      Y. Chen, Z. C. Wang,
    • Journal Title

      Materials Letters

      Volume: 96 Pages: 210-213

    • DOI

      10.1016/j.matlet.2013.01.069

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Impact of NaF Mineralizer on Cerium-containing Nanoparticles Synthesized by Hydrothermal Process2013

    • Author(s)
      Y. Chen,...Z. C. Wang
    • Journal Title

      Physica E

      Volume: 48 Pages: 181-186

    • DOI

      10.1016/j.physe.2013.01.006

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Microstructures and grain boundaries of cubic boron nitrides2012

    • Author(s)
      CL. Chen
    • Journal Title

      Diamond and Relates Materials

      Volume: 32 Pages: 27-31

    • DOI

      10.1016/j.diamond.2012.11.011

    • Related Report
      2013 Final Research Report 2012 Research-status Report
    • Peer Reviewed
  • [Presentation] TEM Investigation of Microstructure of Shark Enameloid2013

    • Author(s)
      C. L. Chen, Z. C. Wang, M. Saito, T. Tohei, Y. Takano, Y. Ikuhara
    • Organizer
      The 1st East-Asia Microscopy Conference (EAMC-1)
    • Place of Presentation
      Chongqing, China
    • Year and Date
      2013-10-15
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] Segregation of oxygen at coherent cubic boron nitride grain boundaries2013

    • Author(s)
      C. L. Chen, S. H. Lv, Z. C. Wang, M. Saito, S. Tsukimoto, N. Shibata, T. Taniguchi, Y. Ikuhara
    • Organizer
      iib2013, XIV International Conference on Intergranular and Interphase Boundaries in Materials
    • Place of Presentation
      Halkidiki, Greece
    • Year and Date
      2013-06-24
    • Related Report
      2013 Annual Research Report 2013 Final Research Report
  • [Presentation] Atomic-Level Characterization of the Enameloid of Shark teeth2013

    • Author(s)
      C. L. Chen, M. Saito, Z. C. Wang, T. Tohei, Y. Takano, Y. Ikuhara
    • Organizer
      The 69th Annual Meeting of the Japanese Society of Microscopy
    • Place of Presentation
      大阪
    • Year and Date
      2013-05-21
    • Related Report
      2013 Final Research Report
  • [Presentation] Microstructural Characterization of the Enameloid of Shark teeth2013

    • Author(s)
      ChunLin Chen, Susumu Tsukimoto, Yuichi Ikuhara, Tetsuya Tohei, Yoshiro Takano
    • Organizer
      日本セラミックス協会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2013-03-17
    • Related Report
      2013 Final Research Report 2012 Research-status Report
  • [Presentation] Microstructures and grain boundaries of cubic boron nitrides2013

    • Author(s)
      C. L. Chen, Z. C. Wang, S. H. Lv, M. Saito, S. Tsukimoto, T. Taniguchi
    • Organizer
      The Joint Symposium on Intercommunity, Platform and Characterization 2013
    • Place of Presentation
      筑波
    • Year and Date
      2013-02-27
    • Related Report
      2013 Final Research Report
  • [Presentation] Atomic-Level Characterization of the Enameloid of Shark teeth2013

    • Author(s)
      C. L. Chen, M. Saito, Z. C. Wang, T. Tohei, Y. Takano, Y. Ikuhara
    • Organizer
      The 69th Annual Meeting of the Japanese Society of Microscopy
    • Place of Presentation
      大阪府吹田市、ホテル阪急エキスポパーク
    • Related Report
      2013 Annual Research Report
  • [Presentation] Microstructure and Mechanical Property in HP-sintered Cubic Boron Nitrides2012

    • Author(s)
      C. L. Chen, Z. C. Wang, R. Huang, S. Tsukimoto, N. Shibata, T. Taniguchi, Y. Ikuhara
    • Organizer
      日本セラミックス協会
    • Place of Presentation
      名古屋大学
    • Year and Date
      2012-09-20
    • Related Report
      2013 Final Research Report 2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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