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Preparation of microreactor-type solid catalysts via immobilization of zeolite nanosheets

Research Project

Project/Area Number 24760626
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Reaction engineering/Process system
Research InstitutionHokkaido University

Principal Investigator

OGINO Isao  北海道大学, 工学(系)研究科(研究院), 准教授 (60625581)

Project Period (FY) 2012-04-01 – 2014-03-31
Project Status Completed (Fiscal Year 2013)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2013: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2012: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Keywords化学工学 / 反応・分離工学 / 触媒 / ゼオライト / ナノシート / マイクロリアクター
Research Abstract

This research aims to synthesize high-performance solid catalysts via immobilization of zeolite nanosheets or nanocrystals, which exhibit molecular recognition properties, on the microchannels of a solid support. We investigated the pre-treatment conditions of the solid support as well as immobilization methods and successfully prepared a solid catalyst, which potentially exhibits the aimed catalytic properties.

Report

(3 results)
  • 2013 Annual Research Report   Final Research Report ( PDF )
  • 2012 Research-status Report
  • Research Products

    (30 results)

All 2014 2013 2012 Other

All Journal Article (6 results) (of which Peer Reviewed: 6 results) Presentation (22 results) (of which Invited: 10 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Exfoliation of Graphite Oxide in Water without Sonication : Bridging Length Scales from Nanosheets to Macroscopic Materials2014

    • Author(s)
      Isao Ogino, Yuya Yokoyama, Shinichiro Iwamura, Shin R. Mukai
    • Journal Title

      Chem. Mater

      Volume: 26 Pages: 3334-3339

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Exfoliation of Graphite Oxide in Water without Sonication: Bridging Length Scales from Nanosheets to Macroscopic Materials2014

    • Author(s)
      荻野勲,横山裕也,岩村振一郎,向井紳
    • Journal Title

      Chemistry of Materials

      Volume: 00 Issue: 10 Pages: 0-0

    • DOI

      10.1021/cm501305c

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Hetero-Atom Tolerant Delamination of Layered Zeolite Precursor Materials2013

    • Author(s)
      Isao Ogino, Einar A. Eilertsen, Son-Jong Hwang, Thomas Rea, Dan Xie, Xiaoying Ouyang, Stacey I. Zones, Alexander Katz
    • Journal Title

      Chem. Mater

      Volume: 25 Pages: 1502-1509

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Immobilization of Magnesium Ammonium Phosphate Crystals within Microchannels for Efficient Ammonia Removal2013

    • Author(s)
      Takanobu Masuda, Isao Ogino, Shin R. Mukai
    • Journal Title

      Water Sci. Technol

      Volume: 67 Pages: 359-365

    • Related Report
      2013 Final Research Report
    • Peer Reviewed
  • [Journal Article] Heteroatom-Tolerant Delamination of Layered Zeolite Precursor Materials2013

    • Author(s)
      荻野 勲 他
    • Journal Title

      Chemistry of Materials

      Volume: in press Issue: 9 Pages: 1502-1509

    • DOI

      10.1021/cm3032785

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Journal Article] Immobilization of Magnesium Ammonium Phosphate Crystals within Microchannels for Efficient Ammonia Removal2013

    • Author(s)
      増田隆信、荻野勲、向井紳
    • Journal Title

      Water Science and Technology

      Volume: 67 Pages: 359-365

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] Synthesis of a Non-Conventional Monolithic Catalyst for Continuous Flow Reaction Systems2014

    • Author(s)
      Isao Ogino,Daiki Andoh,Yoshitaka Satoh,Shinichiro Iwamura,Shin R. Mukai
    • Organizer
      247th ACS National Meeting & Exposition
    • Place of Presentation
      Dallas,USA
    • Year and Date
      2014-03-19
    • Related Report
      2013 Final Research Report
  • [Presentation] 酸化グラフェンの新規調製法2013

    • Author(s)
      横山裕也,荻野勲,向井紳
    • Organizer
      第40回炭素材料学会
    • Place of Presentation
      京都教育文化センター,京都市
    • Year and Date
      2013-12-05
    • Related Report
      2013 Final Research Report
  • [Presentation] マイクロリアクター型固体触媒の合成2013

    • Author(s)
      安藤大輝,荻野勲,向井紳
    • Organizer
      第112回触媒討論会
    • Place of Presentation
      秋田大学,秋田
    • Year and Date
      2013-09-09
    • Related Report
      2013 Final Research Report
  • [Presentation] Microreactor-Type Catalytic Material Synthesized by Immobilizing Nanosheets of Mg-Al Layered Double Hydroxides in a Monolithic Silica2013

    • Author(s)
      Isao Ogino, Daiki Andoh, Shin R. Mukai
    • Organizer
      The Sixteenth International Symposium on Relations between Homogeneous and Heterogeneous Catalysts
    • Place of Presentation
      Sapporo, Japan
    • Year and Date
      2013-08-06
    • Related Report
      2013 Final Research Report
  • [Presentation] Synthesis of a Honeycomb-Type Carbon-Based Acid Catalyst for Flow Reaction Systems2013

    • Author(s)
      Isao Ogino, Kazuhiro Murakami, Yoshitaka Satoh, Shin R. Mukai
    • Organizer
      23rd North American Catalysis Society Meeting
    • Place of Presentation
      Louisville, USA
    • Year and Date
      2013-06-04
    • Related Report
      2013 Final Research Report
  • [Presentation] 二次元ゼオライトナノシートの合成2013

    • Author(s)
      荻野勲
    • Organizer
      JPIJS北海道・東北地区講演会
    • Place of Presentation
      北海道大学,札幌市
    • Year and Date
      2013-01-29
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Strengthening on Monolithic Silica with Microhoneycombs Synthesized Using Ice Templating Method2012

    • Author(s)
      Isao Ogino, Yuki Miyoshi, Yoshitaka Satoh, Shin R. Mukai
    • Organizer
      The 6th International Conference on Multi-Functional Materials and Applications
    • Place of Presentation
      Daejeon,Korea
    • Year and Date
      2012-11-23
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] Tuning the Hierarchical Pore Structure of Monolithic Silica Having Honeycomb Structure via the Ice Templating Method2012

    • Author(s)
      Yoshitaka Satoh,Isao Ogino,Shin R. Mukai
    • Organizer
      The 6th International Conference on Multi-Functional Materials and Applications
    • Place of Presentation
      Daejeon,Korea
    • Year and Date
      2012-11-23
    • Related Report
      2013 Final Research Report
  • [Presentation] Synthesis of Silica Microhoneycomb-Immobilized Heteropoly Acid Catalyst for Liquid-Phase Esterification Reaction2012

    • Author(s)
      Kazuhiro Murakami,Seiichiro Yoshida,Masatoshi Hashimoto,Isao Ogino,Shin R. Mukai
    • Organizer
      10th Japan-Korea Symposium on Materials & Interfaces
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2012-11-08
    • Related Report
      2013 Final Research Report
  • [Presentation] ゼオライト層状前駆体の層剥離によるゼオライトナノシートの合成2012

    • Author(s)
      荻野勲
    • Organizer
      トークインシャワー2012年
    • Place of Presentation
      直方いこいの村,直方市
    • Year and Date
      2012-09-09
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] ゼオライト層状前駆体の層剥離2012

    • Author(s)
      荻野勲
    • Organizer
      第52回オーロラセミナー
    • Place of Presentation
      十勝幕別温泉グランヴリオホテル,幕別町
    • Year and Date
      2012-08-07
    • Related Report
      2013 Final Research Report
    • Invited
  • [Presentation] General Heteroatom-Tolerant Method for Delamination of Layered Zeolite Precursors2012

    • Author(s)
      Isao Ogino, Stacey I. Zones, Alexander Katz
    • Organizer
      ZMPC2012
    • Place of Presentation
      Hiroshima, Japan
    • Year and Date
      2012-07-30
    • Related Report
      2013 Final Research Report
  • [Presentation] ゼオライト層状前駆体の層剥離によるゼオライトナノシートの合成2012

    • Author(s)
      荻野 勲
    • Organizer
      トークシャワーイン九州2012
    • Place of Presentation
      直方いこいの村,直方市
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] General Heteroatom-Tolerant Method for Delamination of Layered Zeolite Precursors2012

    • Author(s)
      荻野 勲,Stacey I. Zones,Alexander Katz
    • Organizer
      ZMPC2012
    • Place of Presentation
      アステールプラザ,広島市
    • Related Report
      2012 Research-status Report
  • [Presentation] Synthesis of a non-conventional monolithic catalyst for continuous flow reaction systems

    • Author(s)
      荻野勲,横山裕也,岩村振一郎,向井紳
    • Organizer
      American Chemical Society
    • Place of Presentation
      Dallas convention center,米国ダラス
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Micreactor-type catalytic material synthesized by immobilizing nanosheets of Mg-Al layered double hydroxides in a monolithic silica

    • Author(s)
      荻野勲,安藤大輝,向井紳
    • Organizer
      The Sixteenth International Symposium on Relations between Homogeneous and Heterogeneous Catalysis
    • Place of Presentation
      北海道大学,札幌市
    • Related Report
      2013 Annual Research Report
  • [Presentation] Synthesis of a Honeycomb-Type Carbon-Based Acid Catalyst for Flow Reaction Systems

    • Author(s)
      荻野勲,村上一博,佐藤慶孝,向井紳
    • Organizer
      23rd North American Catalysis Society Meeting
    • Place of Presentation
      The Galt House Hotel,米国ルイビル市
    • Related Report
      2013 Annual Research Report
  • [Presentation] 流通反応用カーボン系固体酸触媒の開発

    • Author(s)
      荻野勲
    • Organizer
      炭素材料第117委員会 第308回委員会
    • Place of Presentation
      産総研,東京江東区
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] マイクロリアクター型固体触媒の合成

    • Author(s)
      安藤大輝,荻野勲,向井紳
    • Organizer
      第112回触媒討論会
    • Place of Presentation
      秋田大学,秋田市
    • Related Report
      2013 Annual Research Report
  • [Presentation] ゼオライト層状前駆体の層剥離

    • Author(s)
      荻野 勲
    • Organizer
      第52回オーロラセミナー
    • Place of Presentation
      十 勝 幕 別 温 泉 グ ラ ン ヴ ィ リ オ ホ テ ル,幕別町
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] Strengthening of Monolithic Silica with Microhoneycombs Synthesized Using Ice Templating Method

    • Author(s)
      荻野勲、三好悠基、佐藤慶孝、向井紳
    • Organizer
      The 6th International Conference on Multi-Functional Materials and Applications
    • Place of Presentation
      ハンバット国立大学、大田市、韓国
    • Related Report
      2012 Research-status Report
    • Invited
  • [Presentation] 二次元ゼオライトナノシートの合成

    • Author(s)
      荻野 勲
    • Organizer
      JPIJS北海道・東北地区講演会
    • Place of Presentation
      北海道大学,札幌市
    • Related Report
      2012 Research-status Report
    • Invited
  • [Remarks]

    • URL

      http://mde-cp.eng.hokudai.ac.jp/

    • Related Report
      2013 Final Research Report
  • [Patent(Industrial Property Rights)] 酸化グラフェン含有液の製造方法及びその利用2013

    • Inventor(s)
      向井紳,荻野勲,横山裕也
    • Industrial Property Rights Holder
      北海道大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2013-079572
    • Filing Date
      2013-04-05
    • Related Report
      2013 Final Research Report

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Published: 2013-05-31   Modified: 2019-07-29  

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