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Study of charging phenomena by electric field visualization and secondary electron detection

Research Project

Project/Area Number 25249093
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Surface and interface engineering
Research InstitutionTohoku University

Principal Investigator

Shindo Daisuke  東北大学, 多元物質科学研究所, 教授 (20154396)

Co-Investigator(Kenkyū-buntansha) MURAKAMI YASUKAZU  東北大学, 多元物質科学研究所, 准教授 (30281992)
AKASE ZENTARO  東北大学, 多元物質科学研究所, 講師 (90372317)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥44,460,000 (Direct Cost: ¥34,200,000、Indirect Cost: ¥10,260,000)
Fiscal Year 2015: ¥7,930,000 (Direct Cost: ¥6,100,000、Indirect Cost: ¥1,830,000)
Fiscal Year 2014: ¥26,260,000 (Direct Cost: ¥20,200,000、Indirect Cost: ¥6,060,000)
Fiscal Year 2013: ¥10,270,000 (Direct Cost: ¥7,900,000、Indirect Cost: ¥2,370,000)
Keywords電子線ホログラフィー / 帯電 / 電子顕微鏡 / 二次電子 / 検出器 / エポキシ樹脂 / チタン酸バリウム / 集団運動 / 絶縁体 / 生体試料 / トナー
Outline of Final Research Achievements

The purpose of this study is to analyze the charging phenomena under the electron irradiation and clarify the motion of secondary electrons emitted from a specimen. First, by utilizing the phase reconstruction process of electron holography, the charging state of the specimen was quantitatively evaluated. On the other hand, by carrying out the amplitude reconstruction process and detecting the electric field variations due to the motion of electrons, accumulation and collective motion of electrons could be visualized. Furthermore, by developing and introducing an analytical instrument of secondary electrons for a transmission electron microscope, the energy spectra of secondary electrons were obtained and the correlation between the change of the energy spectra of secondary electrons and the charging state of charged insulating specimens was successfully analyzed.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (40 results)

All 2016 2015 2014 2013 Other

All Journal Article (10 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 10 results,  Open Access: 9 results,  Acknowledgement Compliant: 2 results) Presentation (26 results) (of which Int'l Joint Research: 3 results,  Invited: 7 results) Book (2 results) Remarks (2 results)

  • [Journal Article] Spontaneous Polarization and Bulk Photovoltaic Effect Driven by Polar Discontinuity in LaFeO3/SrTiO3 Heterojunctions2016

    • Author(s)
      M. Nakamura, F. Kagawa, T.Tanigaki, H. S. Park, T. Matsuda, D. Shindo, Y. Tokura, and M. Kawasaki
    • Journal Title

      PHYSICAL REVIEW LETTERS

      Volume: in press Issue: 15

    • DOI

      10.1103/physrevlett.116.156801

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Application of strain to orbital-spin-coupled system MnV2O4 at cryogenic temperatures within a transmission electron microscope2016

    • Author(s)
      Y. Murakami, T. Suzuki, Y. Nii, S.Murai, T. Arima, R. Kainuma, and D. Shindo
    • Journal Title

      Microscopy

      Volume: in press Issue: 3 Pages: 223-232

    • DOI

      10.1093/jmicro/dfv377

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Electrostatic-Potential Analysis of Charged Particles by Split-Illumination Electron Holography2015

    • Author(s)
      Toshiaki Tanigaki, Zentaro Akase, Shinji Aizawa, Hyun Soon Park, Yasukazu Murakami, Daisuke Shindo, Hiromitsu Kawase
    • Journal Title

      Microscopy and Microanalysis

      Volume: 21(Supplement S3 ) Issue: S3 Pages: 1969-1970

    • DOI

      10.1017/s1431927615010624

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Real-Space Observation of Short-Period Cubic Lattice of Skyrmions in MnGe2015

    • Author(s)
      Toshiaki Tanigaki, Kiyou Shibata, Naoya Kanazawa, Xiuzhen Yu, Yoshinori Onose, Hyun Soon Park, Daisuke Shindo, Yoshinori Tokura
    • Journal Title

      Nano Letters

      Volume: 15(8) Issue: 8 Pages: 5438-5442

    • DOI

      10.1021/acs.nanolett.5b02653

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Large anisotropic deformation of skyrmions in strained crystal2015

    • Author(s)
      K. Shibata, J. Iwasaki, N. Kanazawa, S. Aizawa, T. Tanigaki, M. Shirai, T. Nakajima, M. Kubota, M. Kawasaki, H. S. Park, D.Shindo, N. Nagaosa, Y. Tokura
    • Journal Title

      Nature Nanotechnology

      Volume: 10 Issue: 7 Pages: 589-589

    • DOI

      10.1038/nnano.2015.113

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Three-Dimensional Magnetic Vortex Cores Visualized by Electron Holographic Vector Field Tomography2015

    • Author(s)
      Toshiaki Tanigaki, Yoshio Takahashi, Tomokazu Shimakura, Tetsuya Akashi, Ruriko Tsuneta, Akira Sugawara, Daisuke Shindo
    • Journal Title

      Microscopy and Microanalysis

      Volume: 21(Supplement S3 ) Issue: S3 Pages: 2149-2150

    • DOI

      10.1017/s1431927615011526

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Split-illumination electron holography for improved evaluation of electrostatic potential associated with electrophotography2014

    • Author(s)
      Toshiaki Tanigaki, Kuniaki Sato, Zentaro Akase, Shinji Aizawa, Hyun Soon Park, Tsuyoshi Matsuda, Yasukazu Murakami, Daisuke Shindo, Hiromitsu Kawase
    • Journal Title

      Applied Physics Letters

      Volume: 104 Issue: 13

    • DOI

      10.1063/1.4869830

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Electron Holography Visualization of Collective Motion of Electrons Through Electric Field Variation2014

    • Author(s)
      D. Shindo et al.
    • Journal Title

      Microscopy and Microanalysis

      Volume: in press Issue: 4 Pages: 1015-1021

    • DOI

      10.1017/s1431927614000786

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Advanced split-illumination electron holography without Fresnel fringes2014

    • Author(s)
      Toshiaki Tanigaki, Shinji Aizawa, Hyun Soon Park, Tsuyoshi Matsuda, Ken Harada, Daisuke Shindo
    • Journal Title

      Ultramicroscopy

      Volume: 137 Pages: 7-11

    • DOI

      10.1016/j.ultramic.2013.11.002

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] In situ electron holographic study of Ionic liquid2014

    • Author(s)
      Manabu Shirai, Tohiaki Tanigaki, Shinji Aizawa, Hyun Soon Park, Tsuyoshi Matsuda, Daisuke Shindo
    • Journal Title

      Ultramicroscopy

      Volume: 146 Pages: 125-129

    • DOI

      10.1016/j.ultramic.2014.08.003

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 電子線ホログラフィーによるナノ結晶軟磁性材料の定量的磁場解析の検討2016

    • Author(s)
      木村 健太, 赤瀬 善太郎, 進藤 大輔, 新津 甲大, 谷垣 俊明, Parmanand Sharma, 牧野 彰宏
    • Organizer
      日本金属学会第158回春期講演大会
    • Place of Presentation
      東京都(東京理科大学葛飾キャンパス)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによる形状を制御した誘電体の帯電現象の解析2016

    • Author(s)
      神明前 功, 真柄 英之, 赤瀬 善太郎, 佐藤 隆文, 進藤 大輔
    • Organizer
      日本金属学会第158回春期講演大会
    • Place of Presentation
      東京都(東京理科大学葛飾キャンパス)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによる絶縁体試料間の電場観察2016

    • Author(s)
      肥後 光暁, 真柄 英之, 赤瀬 善太郎, 進藤 大輔, 嶌田 恵子, 大野 伸彦
    • Organizer
      日本金属学会第158回春期講演大会
    • Place of Presentation
      東京都(東京理科大学葛飾キャンパス)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] Disturbance-free, electron holographic observation of electrons’ motion by electric field variations2016

    • Author(s)
      Daisuke Shindo
    • Organizer
      CEMS International Symposium on Dynamics in Artificial Quantum Systems
    • Place of Presentation
      東京都(東京大学先端科学技術研究セン ター)
    • Year and Date
      2016-01-12
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Spontaneous polarization and bulk photovoltaic effect induced in designed interface of oxide heterojunctions2015

    • Author(s)
      M. Nakamura, F. Kagawa, T. Tanigaki, H.S. Park, T. Matsuda, D. Shindo, Y. Tokura, M. Kawasaki
    • Organizer
      CEMS Topical Meeting on Oxide Interfaces 2015
    • Place of Presentation
      埼玉県和光市(理化学研究所 )
    • Year and Date
      2015-11-05
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 暗視野電子線ホログラフィーを用いたNd2Fe14B結晶粒の歪分布の評価2015

    • Author(s)
      金子 修平, 村上 恭和, 新津 甲大, 赤瀬 善太郎, 進藤 大輔, 谷垣 俊明, 佐々木 泰祐, 大久保 忠勝, 宝野 和博
    • Organizer
      日本金属学会第157回秋期講演大会
    • Place of Presentation
      福岡市(九州大学伊都キャンパス)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによるオーステナイト系ステンレス鋼中の強磁性領域の電磁場解析2015

    • Author(s)
      佐藤 雄亮, 赤瀬 善太郎, 進藤 大輔, 谷山 明
    • Organizer
      日本金属学会第157回秋期講演大会
    • Place of Presentation
      福岡市(九州大学伊都キャンパス)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによる形状を制御した非導電性試料周囲の電場解析2015

    • Author(s)
      築田 直也, 真柄 英之, 赤瀬 善太郎, 進藤 大輔
    • Organizer
      日本金属学会第157回秋期講演大会
    • Place of Presentation
      福岡市(九州大学伊都キャンパス)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] Ni50Mn20In30ホイスラー合金における逆位相界面を介した磁区構造の幾何学的転移2015

    • Author(s)
      新津 甲大, 谷垣 俊明, 許 皛, 村上 恭和, 貝沼 亮介, 進藤 大輔
    • Organizer
      日本金属学会第157回秋期講演大会
    • Place of Presentation
      福岡市(九州大学伊都キャンパス)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] らせん磁性体FeGeにおける一軸引張応力によるスキルミオン変形2015

    • Author(s)
      柴田基洋, 岩崎惇一, 金澤直也, 会沢真二, 谷垣俊明, 白井学, 中島多朗, 久保田将司, 川崎雅司, 朴賢洵, 進藤大輔, 永長直人, 十倉好紀
    • Organizer
      日本物理学会2015秋季大会
    • Place of Presentation
      大阪府吹田市(関西大学千里山キャンパス)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] Electron Holography of Topological Magnets2015

    • Author(s)
      Daisuke Shindo
    • Organizer
      2015 Workshop on "Topological Magnets"
    • Place of Presentation
      埼玉県和光市(理化学研究所 )
    • Year and Date
      2015-05-25
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 逆位相境界で増強される強磁性 (Ferromagnetism developed by antiphase boundaries)2015

    • Author(s)
      村上恭和, 新津甲大, 谷垣俊明, 貝沼亮介, 朴賢洵, 進藤大輔
    • Organizer
      日本顕微鏡学会第71回学術講演会
    • Place of Presentation
      京都市(国立京都国際会館)
    • Year and Date
      2015-05-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによるFe-Si-B-P-Cuナノ結晶軟磁性材料の磁場解析 (Electron Holography Study of Magnetic Flux Distribution in Fe-rich Nanocrystalline Soft Magnetic Material Fe85Si2B8P4Cu1)2015

    • Author(s)
      赤瀬善太郎, 齋藤智広, 会沢真二, 進藤大輔, Sharma Parmanand, 牧野彰宏
    • Organizer
      日本顕微鏡学会第71回学術講演会
    • Place of Presentation
      京都市(国立京都国際会館)
    • Year and Date
      2015-05-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによるLixCoO2粒子の帯電状態の観察 (Observation of electric charging in LixCoO2 particles by electron holography)2015

    • Author(s)
      上石正樹, 赤瀬善太郎, 村上恭和, 進藤大輔, 桑田直明, 河村純一
    • Organizer
      日本顕微鏡学会第71回学術講演会
    • Place of Presentation
      京都市(国立京都国際会館)
    • Year and Date
      2015-05-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによる磁気渦の三次元解析 (Tree-dimensional analysis of magnetic vortices by electron holography)2015

    • Author(s)
      谷垣俊明, 高橋由夫, 島倉智一, 明石哲也, 常田るり子, 菅原昭, 進藤大輔
    • Organizer
      日本顕微鏡学会第71回学術講演会
    • Place of Presentation
      京都市(国立京都国際会館)
    • Year and Date
      2015-05-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] 分離照射電子線ホログラフィーによる帯電粒子の電位解析 (Electrostatic potential analysis of charged particles by split-illumination electron holography)2015

    • Author(s)
      谷垣俊明, 赤瀬善太郎, 会沢真二, Park Hyun Soon, 村上恭和, 進藤大輔, 川瀬広光
    • Organizer
      日本顕微鏡学会第71回学術講演会
    • Place of Presentation
      京都市(国立京都国際会館)
    • Year and Date
      2015-05-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子線ホログラフィーによる形状を制御した非導電性試料周囲の電場観察2015

    • Author(s)
      築田 直也, 真柄 英之, 赤瀬 善太郎, 進藤 大輔, 会沢 真二
    • Organizer
      日本金属学会第156回大会
    • Place of Presentation
      東京
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] 電子線ホログラフィーにより可視化された2次電子の集団運動に対するシミュレーション2014

    • Author(s)
      真柄英之, 赤瀬善太郎, 進藤大輔
    • Organizer
      日本金属学会第155回大会
    • Place of Presentation
      名古屋
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] 電子線ホログラフィーによるSiO2微粒子の帯電効果の解析2014

    • Author(s)
      鈴木浩晃, 赤瀬善太郎, 会沢真二, 谷垣俊明, 新津甲大, 進藤大輔
    • Organizer
      日本金属学会第155回大会
    • Place of Presentation
      名古屋
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] 電子線ホログラフィーによるVO2薄膜の金属-絶縁体相転移の観察2014

    • Author(s)
      木下晃一, 新津甲大, 会沢真二, 村上恭和, 進藤大輔, 神吉輝夫, 田中秀和
    • Organizer
      日本金属学会第155回大会
    • Place of Presentation
      名古屋
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] Split-illumination electron holography2014

    • Author(s)
      Toshiaki Tanigaki, Shinji Aizawa, Hyun Soon Park, Tsuyoshi Matsuda, Ken Harada, Yasukazu Murakami, Daisuke Shindo
    • Organizer
      18th International Microscopy Congress
    • Place of Presentation
      Czech Republic, Prague
    • Year and Date
      2014-09-07 – 2014-09-12
    • Related Report
      2014 Annual Research Report
  • [Presentation] Collective Motion of Secondary Electrons Visualized by Electron Holography2014

    • Author(s)
      Daisuke Shindo, Zentaro Akase, Hyun Soon Park
    • Organizer
      Microscopy & microanalysis 2014
    • Place of Presentation
      U. S. A., Hartford
    • Year and Date
      2014-08-03 – 2014-08-07
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Collective Motion of Electrons Visualized by Electron Holography2014

    • Author(s)
      D. Shindo
    • Organizer
      FIRST International Symposium on Topological Quantum Technology
    • Place of Presentation
      Tokyo
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] 電子線ホログラフィーによるSiO2微粒子の帯電効果の観察2014

    • Author(s)
      鈴木浩晃他
    • Organizer
      日本金属学会春期大会
    • Place of Presentation
      東京
    • Related Report
      2013 Annual Research Report
  • [Presentation] Dynamic Motion of Electrons Observed through Electric Field Variation2013

    • Author(s)
      D. Shindo et al.
    • Organizer
      Frontiers of Electron Microscopy in Materials Science
    • Place of Presentation
      Lorne, Australia
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Electron Holography Study of Magnetic Nanostructures in Functional Materials2013

    • Author(s)
      D. Shindo et al.
    • Organizer
      2013 MRS Fall Meeting & Exhibit
    • Place of Presentation
      Boston, USA
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Book] 磁気便覧2016

    • Author(s)
      進藤 大輔
    • Total Pages
      888
    • Publisher
      丸善出版
    • Related Report
      2015 Annual Research Report
  • [Book] in-situ測定/その場観察 実例集 ~各種計測技術の実践テクニックおよび材料デバイス別分析例~2013

    • Author(s)
      進藤大輔
    • Total Pages
      315
    • Publisher
      (株)情報機構
    • Related Report
      2013 Annual Research Report
  • [Remarks] TAGEN FOREFRONT 01

    • URL

      http://www.tagen.tohoku.ac.jp/general/publish/forefront/ebook_01/

    • Related Report
      2015 Annual Research Report
  • [Remarks] 東北大学 多元物質科学研究所 先端計測開発センター 電子線干渉計測研究分野

    • URL

      http://www.tagen.tohoku.ac.jp/modules/laboratory/index.php?laboid=57

    • Related Report
      2015 Annual Research Report

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Published: 2013-05-15   Modified: 2019-07-29  

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