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High-strength and high-ductility mechanism of pure Ti sintered material using hydrogen and oxygen

Research Project

Project/Area Number 25249102
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/Microstructural control engineering
Research InstitutionOsaka University

Principal Investigator

Kondoh Katsuyoshi  大阪大学, 接合科学研究所, 教授 (50345138)

Co-Investigator(Kenkyū-buntansha) UMEDA JUNKO  大阪大学, 接合科学研究所, 助教 (50345162)
SUNADA SATOSHI  富山大学, 工学部, 教授 (00206575)
SASASE MASATO  若狭湾エネルギー研究センター, 研究員 (60359239)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥28,600,000 (Direct Cost: ¥22,000,000、Indirect Cost: ¥6,600,000)
Fiscal Year 2015: ¥8,060,000 (Direct Cost: ¥6,200,000、Indirect Cost: ¥1,860,000)
Fiscal Year 2014: ¥9,100,000 (Direct Cost: ¥7,000,000、Indirect Cost: ¥2,100,000)
Fiscal Year 2013: ¥11,440,000 (Direct Cost: ¥8,800,000、Indirect Cost: ¥2,640,000)
Keywords粉末冶金 / 純チタン / 相変態 / 残留水素 / 加工熱処理 / 集合組識 / 変形双晶 / ヤング率 / 集合組織
Outline of Final Research Achievements

To clarify high-strength and ductility mechanism of pure Ti material with small additive hydrogen, TiH2 raw powder was consolidated by sintering and hot extrusion. The residual hydrogen content depended on the sintering temperature, and affected on α/β phase transformation during extrusion. In case of 0.33 mass% hydrogen content, α→β phase transformation completely occurred at 1073 K, and resulted in <0001>α texture formation of extruded Ti material. This texture was never observed in the conventional extruded Ti materials (<10-10>α texture) with few hydrogen elements. The former indicated high tensile strength (σ) of 959 MPa and elongation (δ) of 27.6% compared to PM pure Ti materials with σ=634 MPa and δ=29.9%. In-situ SEM observation on the hydride dispersoids in PM Ti material indicated that they could be obviously deformed in tensile and had a ductile property at room temperature.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (17 results)

All 2016 2015 2014 2013 Other

All Int'l Joint Research (2 results) Journal Article (3 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 3 results,  Acknowledgement Compliant: 3 results) Presentation (7 results) (of which Int'l Joint Research: 2 results,  Invited: 2 results) Patent(Industrial Property Rights) (5 results) (of which Overseas: 2 results)

  • [Int'l Joint Research] ロイヤルメルボルン工科大学(オーストラリア)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] 西安理工大学(中国)

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Strengthening behavior of in situ-synthesized (TiC-TiB)/Ti composites by powder metallurgy and hot extrusion2016

    • Author(s)
      Shufeng LI, KatsuyoshiKondoh, HisashiImai, BiaoChen, LeiJia, JunkoUmeda
    • Journal Title

      Materials and Design

      Volume: 95 Pages: 127-132

    • DOI

      10.1016/j.matdes.2016.01.092

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Titanium Powders via Gas-Solid Direct Reaction Process and Mechanical Properties of Their Extruded Materials2015

    • Author(s)
      Takanori Mimoto, Junko Umeda, Katsuyoshi Kondoh
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 56 Issue: 8 Pages: 1153-1158

    • DOI

      10.2320/matertrans.L-M2015816

    • NAID

      130005088955

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Experimental and Theoretical Analysis of Nitrogen Solid-Solution Strengthening of PM Titanium2014

    • Author(s)
      Katsuyoshi Kondoh, Bin Sun, Shufeng Li, Hisashi Imai, Junko Umeda
    • Journal Title

      International Journal of Powder Metallurgy

      Volume: 50 Pages: 35-40

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] State-of-the-Art in Powder Metallurgy Materials with Atomic/Nano scale Microstructures2015

    • Author(s)
      Katsuyoshi Kondoh
    • Organizer
      Global Advanced Materials and Surfaces 2016
    • Place of Presentation
      ドバイ
    • Year and Date
      2015-12-07
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Novel Processing of High-strength & High-ductility PM Pure Titanium with Light Elements2015

    • Author(s)
      Katsuyoshi Kondoh
    • Organizer
      3rd International Conference on Powder Metallurgy in Asia
    • Place of Presentation
      京都
    • Year and Date
      2015-11-08
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Strengthening Behavior and Mechanisms of Extruded Powder Metallurgy Pure Ti Materials Reinforced with Ubiquitous Light Elements2015

    • Author(s)
      Takanori Mimoto, Junko Umeda, Katsuyoshi Kondoh
    • Organizer
      TMS2015
    • Place of Presentation
      オーランド(アメリカ)
    • Year and Date
      2015-03-15 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] Microstructures and Mechanical Properties of Extruded Powder Metallurgy Pure Ti Materials by Gas-Solid Reaction Process2014

    • Author(s)
      Takanori Mimoto, Junko Umeda, Katsuyoshi Kondoh
    • Organizer
      MS&T2014
    • Place of Presentation
      ピッツバーグ(アメリカ)
    • Year and Date
      2014-10-12 – 2014-10-16
    • Related Report
      2014 Annual Research Report
  • [Presentation] ユビキタス軽元素を利用した純チタン焼結材料の高次機能化2014

    • Author(s)
      近藤 勝義
    • Organizer
      日本鉄鋼協会 第52回 材質制御研究会
    • Place of Presentation
      鳥取大学(鳥取県鳥取市)
    • Year and Date
      2014-10-07
    • Related Report
      2014 Annual Research Report
  • [Presentation] 固気直接反応法による高濃度窒素固溶チタン粉末押出材の創製2014

    • Author(s)
      三本嵩哲,梅田純子,近藤勝義
    • Organizer
      日本金属学会2014年秋期(第155回)
    • Place of Presentation
      名古屋大学(愛知県名古屋市)
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] Pure Titanium with High Strength and Excellent Ductility by Solid Solute Oxygen Strengthening via Powder Metallurgy Route2013

    • Author(s)
      Katsuyoshi Kondoh
    • Organizer
      Materials Science & Technology 2013(MS&T2013)
    • Place of Presentation
      Montreal, Canada
    • Related Report
      2013 Annual Research Report
  • [Patent(Industrial Property Rights)] 酸素固溶チタン焼結体およびその製造方法2015

    • Inventor(s)
      近藤 勝義
    • Industrial Property Rights Holder
      近藤 勝義
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-215846
    • Filing Date
      2015-11-02
    • Related Report
      2015 Annual Research Report
  • [Patent(Industrial Property Rights)] チタン粉末材料、チタン素材及び酸素固溶チタン粉末材料の製造方法2014

    • Inventor(s)
      近藤 勝義
    • Industrial Property Rights Holder
      近藤 勝義
    • Industrial Property Rights Type
      特許
    • Filing Date
      2014-12-26
    • Related Report
      2014 Annual Research Report
    • Overseas
  • [Patent(Industrial Property Rights)] 窒素固溶チタン粉末材料、チタン素材及び窒素固溶チタン粉末材料の製造方法2014

    • Inventor(s)
      近藤 勝義
    • Industrial Property Rights Holder
      近藤 勝義
    • Industrial Property Rights Type
      特許
    • Filing Date
      2014-12-26
    • Related Report
      2014 Annual Research Report
    • Overseas
  • [Patent(Industrial Property Rights)] チタン粉末材料、チタン素材及び酸素固溶チタン粉末材料の製造方法2014

    • Inventor(s)
      近藤勝義
    • Industrial Property Rights Holder
      近藤勝義
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-003392
    • Filing Date
      2014-01-10
    • Related Report
      2013 Annual Research Report
  • [Patent(Industrial Property Rights)] 窒素固溶チタン粉末材料、チタン素材及び窒素固溶チタン粉末材料の製造方法2014

    • Inventor(s)
      近藤勝義
    • Industrial Property Rights Holder
      近藤勝義
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-011362
    • Filing Date
      2014-01-24
    • Related Report
      2013 Annual Research Report

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Published: 2013-05-15   Modified: 2019-07-29  

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