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Deposition of Ideally-oriented PZT Monocrystalline Thin Film on Si Substrate and Feasibility Study of Its Application to MEMS

Research Project

Project/Area Number 25286033
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Nano/Microsystems
Research InstitutionTohoku University

Principal Investigator

Tanaka Shuji  東北大学, 工学(系)研究科(研究院), 教授 (00312611)

Co-Investigator(Kenkyū-buntansha) YOSHIDA Shinya  東北大学, 大学院工学研究科, 特任准教授 (30509691)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥18,850,000 (Direct Cost: ¥14,500,000、Indirect Cost: ¥4,350,000)
Fiscal Year 2015: ¥7,020,000 (Direct Cost: ¥5,400,000、Indirect Cost: ¥1,620,000)
Fiscal Year 2014: ¥7,020,000 (Direct Cost: ¥5,400,000、Indirect Cost: ¥1,620,000)
Fiscal Year 2013: ¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
KeywordsPZT / エピタキシャル成長 / 単結晶圧電薄膜 / 急冷法 / 誘電率 / MEMS / 圧電薄膜 / バッファ層 / キュリー点 / スパッタリング / チタン酸ジルコン酸鉛 / スパッタ成膜 / 単結晶膜 / シリコン基板 / 圧電定数
Outline of Final Research Achievements

In this study, PZT family monocrystalline thin films with the ideal orientation were epitaxially grown on a Si substrate. The deposition method is sputtering, and by a fast cooling method, the ideal polarization, i.e. c-axis polarization of tetragonal crystal, has been first realized on a Si substrate. As a result, we obtained excellent characteristics for applications such as high piezoelectric constant, low dielectric constant, very large figure of merit derived from them and Curie point significantly higher than that of the bulk. A metal buffer layer with low resistivity was also successfully deposited. In addition, MEMS structures were fabricated using the deposited PZT family monocrystalline thin films to confirm that they were free from process damages.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (16 results)

All 2016 2015 2014

All Journal Article (3 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 2 results) Presentation (13 results) (of which Int'l Joint Research: 6 results,  Invited: 5 results)

  • [Journal Article] Fabrication and characterization of large figure-of-merit epitaxialPMnN-PZT/Si transducer for piezoelectric MEMS sensors2016

    • Author(s)
      Shinya Yoshida, Hiroaki Hanzawa, Kiyotaka Wasa, Shuji Tanaka
    • Journal Title

      Sensors and Actuators A

      Volume: 239 Pages: 201-208

    • DOI

      10.1016/j.sna.2016.01.031

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] PZT薄膜とPZT MEMS2015

    • Author(s)
      吉田慎哉, 森山雅昭
    • Journal Title

      金属

      Volume: 85 Pages: 701-707

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Highly c-Axis Oriented Monocrystalline Pb(Zr, Ti)O3 Thin Films on Si Wafer Prepared by Fast Cooling Immediately after Sputter Deposition2014

    • Author(s)
      Shinya Yoshida, Hiroaki Hanzawa, Kiyotaka Wasa, Masayosh Esashi, Shuji Tanaka
    • Journal Title

      IEEE Transactions on Ultrasonics, Feroelectrics, and Frequency Control

      Volume: 61 Issue: 9 Pages: 1552-1558

    • DOI

      10.1109/tuffc.2014.3069

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Advanced Piezoelectric Films for MEMS and Acoustic Wave Devices2015

    • Author(s)
      S. Tanaka, S. Yoshida, M. Kadota, K. Wasa
    • Organizer
      Sixth International Symposium on Acoustic Wave Devices for Future Mobile Communication Systems
    • Place of Presentation
      千葉, 千葉大学
    • Year and Date
      2015-11-24
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] MEMSの最新動向と圧電応用2015

    • Author(s)
      田中秀治
    • Organizer
      第153回電子セラミック・プロセス研究会
    • Place of Presentation
      横浜, 横浜港湾福利厚生協会波止場会館
    • Year and Date
      2015-10-17
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] MEMS研究者から見た見た圧電MEMS と圧電材料2015

    • Author(s)
      吉田慎哉, 田中秀治
    • Organizer
      応用物理学会春季講演会
    • Place of Presentation
      名古屋, 名古屋国際会議場
    • Year and Date
      2015-09-13
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] Advanced Piezoelectric Thin Films and Devices2015

    • Author(s)
      Shuji Tanaka
    • Organizer
      19th Nano Engineering and Microsystem Technology Conference
    • Place of Presentation
      台北, 台湾
    • Year and Date
      2015-08-13
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] LARGE FIGURE-OF-MERIT EPITAXIAL PB(MN,NB)O3-PB(ZR,TI)O3/SI TRANSDUCER FOR PIEZOELECTRIC MEMS SENSORS2015

    • Author(s)
      Hiroaki Hanzawa, Shinya Yoshida, Kiyotaka Wasa, and Shuji Tanaka
    • Organizer
      18th International Conference on Solid-State Sensors, Actuators and Microsystems, Transducers 2015
    • Place of Presentation
      Anchorage, Alaska, USA
    • Year and Date
      2015-06-21
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Sputter Deposition of Epitaxial Yttria-Stabilized Zirconia (YSZ) Buffer Layer on Large Diameter Si Wafer for Epitaxial PZT Thin Film Transducer2015

    • Author(s)
      S. Yoshida, S. Nishizawa, T. Hayasaka, K. Wasa and S. Tanaka
    • Organizer
      IEEE International Symposium on Applications of Ferroelectric (ISAF)
    • Place of Presentation
      Singapore
    • Year and Date
      2015-05-24
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Epitaxial Growth of (100)/(001) PZT-Based Thin Film on (111) Si Wafer Using SrRuO3/LaNiO3/Pt/CeO2 Buffer Layer2015

    • Author(s)
      Takeshi Hayasaka, Shinya Yoshida, Shuji Tanaka
    • Organizer
      IEEE International Symposium on Applications of Ferroelectric (ISAF)
    • Place of Presentation
      Singapore
    • Year and Date
      2015-05-24
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] K. Wasa, H. Hanzawa, S. Yoshida, S. Tanaka, H. Adachi, T. Matsunaga, Structure and Ferroelectric Properties of High TcBi(Me)O3-PbTiO3 Single Crystal Thin Films2015

    • Author(s)
      K. Wasa, H. Hanzawa, S. Yoshida, S. Tanaka, H. Adachi, T. Matsunaga
    • Organizer
      IEEE International Symposium on Applications of Ferroelectric (ISAF)
    • Place of Presentation
      Singapore
    • Year and Date
      2015-05-24
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 急冷法によってc軸配向させたSi基板上のPMnN-PZT単結晶薄膜の高温特性2015

    • Author(s)
      半澤弘明, 吉田慎哉, 和佐清孝, 田中秀治
    • Organizer
      第62回応用物理学会春季学術講演会
    • Place of Presentation
      東海大学湘南キャンパス,平塚,神奈川
    • Year and Date
      2015-03-11 – 2015-03-14
    • Related Report
      2014 Annual Research Report
  • [Presentation] 圧電MEMSのためのスパッタ堆積による大口径Si基板上へのYSZバッファ層のエピタキシャル成長2015

    • Author(s)
      西澤信典, 吉田慎哉, 和佐清孝, 田中秀治
    • Organizer
      第62回応用物理学会春季学術講演会
    • Place of Presentation
      東海大学湘南キャンパス,平塚,神奈川
    • Year and Date
      2015-03-11 – 2015-03-14
    • Related Report
      2014 Annual Research Report
  • [Presentation] 高性能圧電MEMSセンサのためのc軸配向PMnN-PZTエピタキシャル薄膜のSi基板上への形成2015

    • Author(s)
      吉田慎哉, 半澤弘明, 和佐清孝, 田中秀治
    • Organizer
      圧電材料・デバイスシンポジウム2015
    • Place of Presentation
      東北大学,仙台,宮城
    • Year and Date
      2015-02-18 – 2015-02-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] Advanced Piezoeletric Thin Film and Devices2014

    • Author(s)
      Shuji Tanaka
    • Organizer
      10th Fraunhofer Symposium in Sendai
    • Place of Presentation
      東北大学,仙台,宮城
    • Year and Date
      2014-11-26
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Highly c-Axis Oriented Monocrystalline Pb(Zr, Ti)O3 based Thin Film on Si Wafer by Sputter Deposition with Fast Cooling Process2014

    • Author(s)
      Hiroaki Hanzawa, Shinya Yoshida, Kiyotaka Wasa and Shuji Tanaka
    • Organizer
      2014 IEEE International Ultrasonics Symposium
    • Place of Presentation
      Chicago, Illinois, USA
    • Year and Date
      2014-09-03 – 2014-09-06
    • Related Report
      2014 Annual Research Report

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Published: 2013-05-21   Modified: 2019-07-29  

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