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Anomalous small-angle scattering at K absorption edge of Al for visualization of nanoclusters in Al-Mg based alloys

Research Project

Project/Area Number 25286085
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Quantum beam science
Research InstitutionKyoto University

Principal Investigator

OKUDA Hiroshi  京都大学, 工学(系)研究科(研究院), 准教授 (50214060)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥17,550,000 (Direct Cost: ¥13,500,000、Indirect Cost: ¥4,050,000)
Fiscal Year 2015: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Fiscal Year 2014: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2013: ¥12,740,000 (Direct Cost: ¥9,800,000、Indirect Cost: ¥2,940,000)
Keywords異常小角散乱法 / 軟X線 / 軽合金 / アルミニウム合金 / ナノ析出物 / 軟X線 / 異常分散効果 / 異常小角散乱 / 2次元測定 / 軟X線小角散乱法 / AlMgSi合金 / Al-Mg-X合金 / 軟X線共鳴散乱 / クラスター
Outline of Final Research Achievements

Anomalous small-angle X-ray scattering system for contrast change using resonant effect at K absorption edges of Aluminum and Magnesium has been designed and constructed for realizing contrast enhancement to measure small-angle scattering from low-Z aluminum alloys, i.e., Al-Mg and Al-Mg-Si. To visualize Fourier transform of the scattering patterns by strengthening nanoclusters and nanoprecipitates, establishing quantitative measurements at the tender X-ray region is a new and technically difficult requirements.
We have shown that resonant small-angle scattering at the K absorption edge of Aluminum by Alumina nanoparticles and precipitates in Al alloy systems agreed with theoretical prediction given by Cromer-Liberman calculations.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (16 results)

All 2016 2015 2014 2013 Other

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (14 results) (of which Int'l Joint Research: 2 results,  Invited: 4 results) Remarks (1 results)

  • [Journal Article] Normalization of grazing-incidence small angle scattering of phospholipid alloy systems2014

    • Author(s)
      H.Okuda, T.Yamamoto,K.Takshita, M.Hirai, K.Senoo, H.Ogawa and Y.Kitajima
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: 53 Issue: 5S1 Pages: 1-5

    • DOI

      10.7567/jjap.53.05fh02

    • Related Report
      2014 Annual Research Report 2013 Annual Research Report
    • Peer Reviewed
  • [Presentation] 1keVから100keVまで 小角散乱の金属材料への応用2016

    • Author(s)
      奥田浩司、浴畑嶺、北島義典、為則祐介
    • Organizer
      PF研究会
    • Place of Presentation
      筑波 高エネルギー研
    • Year and Date
      2016-03-30
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] 軟X線二次元小角散乱法の開発とAl合金への応用2016

    • Author(s)
      浴畑嶺、西澤勇樹、奥田浩司、北島義典
    • Organizer
      物性工学談話会
    • Place of Presentation
      京都大学
    • Year and Date
      2016-01-27
    • Related Report
      2015 Annual Research Report
  • [Presentation] Al K吸収端での異常小角散乱の試み2016

    • Author(s)
      奥田浩司,北島義典
    • Organizer
      日本放射光学会年会
    • Place of Presentation
      柏 東京大学サテライト
    • Year and Date
      2016-01-09
    • Related Report
      2015 Annual Research Report
  • [Presentation] EXTENSIONS OF GISAXS MEASUREMENTS IN TENDER X-RAY REGION2015

    • Author(s)
      H.Okuda,T.Yamamoto, M.Hirai,Y.Kitajima,N.Shimizu and N.Igarashi
    • Organizer
      GISAS2015
    • Place of Presentation
      Nice, France
    • Year and Date
      2015-09-08
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Microstructure evolution of thin films examined by GISAXS2015

    • Author(s)
      H.Okuda, T.Yamamoto, Y.Kitajima, S.Sakurai, H.OPgawa, N.Shimizu, N.Igarashi
    • Organizer
      American Crystallographic Association, annual meeting
    • Place of Presentation
      Philadelphia,USA
    • Year and Date
      2015-07-26
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Early stage of precipitation in Al-Mg-Si and related alloys examined by small-angle scattering2015

    • Author(s)
      H.Okuda, Y.Nishizawa, Y. Kitajima,T.Sato, M.Mihara
    • Organizer
      TMS2015
    • Place of Presentation
      Orlando, FL,USA
    • Year and Date
      2015-03-15 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] GISAXSの軟X線領域への展開2015

    • Author(s)
      奥田浩司
    • Organizer
      光・量⼦融合連携研究講演会
    • Place of Presentation
      九州大学伊都C
    • Year and Date
      2015-03-10
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] GISAXS measurements near the absorption edge of P2014

    • Author(s)
      H.Okuda,T.Yamamoto,K.Takeshita,M.Hirai,S.Sakurai,Y.Kitajima,N.Igarashi,N.Shimizu,H.Ogawa
    • Organizer
      ALS workshop
    • Place of Presentation
      ALS,Berkeley, CA,USA
    • Year and Date
      2014-10-07 – 2014-10-08
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Al-Mg-Cu-Ag合金析出過程の放射光小角散乱法による検討2014

    • Author(s)
      西澤勇希、奥田浩司、里達雄k三原麻未
    • Organizer
      金属学会秋季大会
    • Place of Presentation
      名古屋大東山C
    • Year and Date
      2014-09-23 – 2014-09-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] 6000系Al合金の析出過程評価のためのAlK吸収端を用いた透過軟X線小角散乱法の開発2014

    • Author(s)
      西澤勇樹 奥田浩司 白井涼 北島義典
    • Organizer
      放射光学会
    • Place of Presentation
      広島
    • Related Report
      2013 Annual Research Report
  • [Presentation] Anomalous small-angle scattering with soft X-rays at Al and Si K absorption edges2014

    • Author(s)
      H.Okuda, T.Yamamoto,Y.Nishizawa,Y.Kitajima
    • Organizer
      TMS2014
    • Place of Presentation
      SanDiego, USA
    • Related Report
      2013 Annual Research Report
  • [Presentation] 1.5-2keV領域での透過軟X線小角散乱法の検討2014

    • Author(s)
      西澤勇希 奥田浩司 白井涼 北島義典
    • Organizer
      日本金属学会春季大会
    • Place of Presentation
      東京
    • Related Report
      2013 Annual Research Report
  • [Presentation] Alの K吸収端を利用した異常小角散乱測定の検討2013

    • Author(s)
      奥田浩司、白井涼 山本崇善、西澤勇希、宍戸久郎l北原周、北島義典
    • Organizer
      日本金属学会秋季大会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] 6000系Alの析出過程解明のためのAlK吸収端を用いた透過軟X線小角散乱法の開発

    • Author(s)
      西澤勇樹 奥田浩司 白井涼 北島義典
    • Organizer
      軽金属学会関西支部若手院生研究会
    • Place of Presentation
      姫路
    • Related Report
      2013 Annual Research Report
  • [Remarks] 奥田GrHP

    • URL

      http://mcmd.mtl.kyoto-u.ac.jp/

    • Related Report
      2014 Annual Research Report

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Published: 2013-05-21   Modified: 2019-07-29  

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