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Development of an industrial evaluation technique for vacancy behavior using muon spin relaxation method

Research Project

Project/Area Number 25289260
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Material processing/Microstructural control engineering
Research InstitutionUniversity of Toyama

Principal Investigator

Nishimura Katsuhiko  富山大学, 大学院理工学研究部(工学), 教授 (70218189)

Co-Investigator(Kenkyū-buntansha) MATSUDA Kenji  富山大学, 大学院理工学研究部, 教授 (00209553)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥14,950,000 (Direct Cost: ¥11,500,000、Indirect Cost: ¥3,450,000)
Fiscal Year 2015: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2014: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2013: ¥11,440,000 (Direct Cost: ¥8,800,000、Indirect Cost: ¥2,640,000)
Keywords金属生産工学 / アルミニウム合金 / 原子空孔 / ミュオン / スピン緩和 / クラスター / 電子密度計算 / 電子湿度計算 / 「国際情報交換」ノルウェイ / 「国際情報交換」連合王国 / 「国際情報交換」ノルウエイ
Outline of Final Research Achievements

Zero field muon spin relaxation experiments were carried out for Al-Mg-Si, Al-0.5%Mg and Al-0.5%Si alloys under various heat treatments, which have demonstrated that the muon trapping rates (νt) depended on the heat treatment on the sample and solute concentrations: (1) the concentration of dissolved Mg dominates the νt values at lower temperatures below 120 K; (2) the νt values around 200 K reflect a number of clusters; (3) the vacancy trapping is obvious around room temperature; (4) the natural aging effect is clearly observed with Al-0.5%Si. The isothermal time dependence of spin relaxation rates with the sample of Al-1.6%Mg2Si at 280, 290 and 300K showed that the spin relaxation rates at 280 K did not change for the first about 100 minutes after the solution heat treatment and quenching, then decreased with time in the logarithmic scale. Those at 290 and 300 K decreased with time from the beginning. Thus, muons clearly monitored kinetic behavior of vacancies.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (24 results)

All 2016 2015 2014 2013 Other

All Int'l Joint Research (4 results) Journal Article (9 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 7 results,  Open Access: 5 results,  Acknowledgement Compliant: 4 results) Presentation (11 results) (of which Int'l Joint Research: 1 results)

  • [Int'l Joint Research] ノルウェー科学技術大学(ノルウェー)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] ラザフォード・アップルトン研究所(英国)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] ニュー・サウス・ウェールズ大学(オーストラリア)

    • Related Report
      2015 Annual Research Report
  • [Int'l Joint Research] 理化学研究所(日本)

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Early Stage Clustering Behavior in Al-Mg-Si Alloys Observed via Time Dependent Magnetization2016

    • Author(s)
      Katsuhiko Nishimura, Kenji Matsuda, Qiankun Lei, Takahiro Namiki, Seungwon Lee, Norio Nunomra, Teiichiro Matsuzaki, Wayne D. Hutchison
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 57 Issue: 5 Pages: 627-630

    • DOI

      10.2320/matertrans.M2015474

    • NAID

      130005146676

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Solute-Vacancy Clustering In Al-Mg-Si Alloys Studied By Muon Spin Relaxation Technique2015

    • Author(s)
      K. NISHIMURA, K. MATSUDA, R. KOMAKI, N. NUNOMRA, S. WENNER, R. HOLMESTAD,T. MATSUZAKI, I. WATANABE, F.L. PRATT
    • Journal Title

      Archives of Metallurgy and Materials

      Volume: 60 Issue: 2 Pages: 925-929

    • DOI

      10.1515/amm-2015-0231

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Solute-vacancy clustering in Al-Mg-Si alloys studied by muon spin relaxation technique2015

    • Author(s)
      Katsuhiko Nishimura, Kenji Matsuda, Ryota Komaki, Norio Nunomra, Sigurd Wenner, Randi Holmestad, Teiichiro Matsuzaki, Isao Watanabe, Francis L. Pratt
    • Journal Title

      Archives of Metallurgy and Materials

      Volume: 1 Pages: 1-6

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] muSR study of Al-0.67%Mg-0.77%Si alloys2014

    • Author(s)
      K Nishimura, K Matsuda, R Komaki, N Nunomura, S Wenner, R Holmestad, T Matsuzaki, I Watanabe, F L Pratt and C D Marioara
    • Journal Title

      Journal of Physics

      Volume: 551 Pages: 012031-012031

    • DOI

      10.1088/1742-6596/551/1/012031

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Clustering and vacancy behavior in high- and low-solute Al-Mg-Si alloys2014

    • Author(s)
      S. Wenner, K. Nishimura, K. Matsuda, T. Matsuzaki, D. Tomono, F. L. Pratt, C. D. Marioara, R. Holmestad
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS

      Volume: 45A Issue: 12 Pages: 5777-5781

    • DOI

      10.1007/s11661-014-2527-3

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ミュオンスピン緩和スペクトル法の応用研究部2014

    • Author(s)
      西村克彦、櫻井健夫、松崎禎市郎、松田健二
    • Journal Title

      軽金属

      Volume: 64 Pages: 393-395

    • Related Report
      2014 Annual Research Report
    • Open Access
  • [Journal Article] ミュオンスピン緩和を利用した6000系Al合金の原子空孔挙動2014

    • Author(s)
      西村克彦、松田健二、小牧亮太、布村紀男、松崎禎市郎、渡邊功雄、里達雄、フランシス プラット、ランディ ホルメシュタット、シグード ウェナー、カリン マリオアラ
    • Journal Title

      KURRI-KR-195

      Volume: 195 Pages: 55-58

    • Related Report
      2013 Annual Research Report
  • [Journal Article] muSR study of Al-Mg, Al-Si and Al-Mg-Si alloys2014

    • Author(s)
      K. Matsuda, K. Nishimura, S. Wenner, R. Holmestad, T. Matsuzaki, F. L. Pratt, C. D. Marioara
    • Journal Title

      RIKEN Accelerator Progress Repor

      Volume: 47 Pages: 5-5

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Muon kinetics in heat treated Al (–Mg)(–Si) alloys2013

    • Author(s)
      Sigurd Wenner, Katsuhiko Nishimura, Kenji Matsuda, Teiichiro Matsuzaki, Dai Tomono, Francis L. Pratt,Calin D. Marioara, Randi Holmestad
    • Journal Title

      Acta Materialia

      Volume: 61 Issue: 16 Pages: 6082-6092

    • DOI

      10.1016/j.actamat.2013.06.050

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Presentation] Al-Mg-Si合金の磁化の時間変化2016

    • Author(s)
      畠山大智、西村克彦、並木孝洋、松田健二、吉野太規、布村紀男、松崎禎市郎
    • Organizer
      軽金属学会
    • Place of Presentation
      大阪大学
    • Year and Date
      2016-05-28
    • Related Report
      2015 Annual Research Report
  • [Presentation] Al-Mg-Si合金の自然時効とミュオンスピン緩和率・磁化の時間変化2016

    • Author(s)
      西村克彦,松田健二,並木孝洋,李昇原,布村紀男,松崎禎市郎,渡邉功雄,Majed Abdel-Jawad, Sungwon Yoon, F. L. Pratt
    • Organizer
      日本金属学会
    • Place of Presentation
      東京理科大学
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] Al-1.6%Mg2Siの磁化の時間変化2015

    • Author(s)
      畠山大智、西村克彦、並木孝洋、松田健二、吉野太規、布村紀男、松崎禎市郎
    • Organizer
      軽金属学会
    • Place of Presentation
      日本大学
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] ミュオンスピン緩和法によるAl-Mg-Si合金の自然時効の研究2015

    • Author(s)
      西村克彦,松田健二,並木孝洋,李昇原,布村紀男,松崎禎市郎,渡邉功雄,里達雄
    • Organizer
      軽金属学会
    • Place of Presentation
      日本大学
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] Kinetics of Natural Aging in Al-1.6%Mg2Si Alloy Studied by Muon Spin Relaxation2015

    • Author(s)
      Katsuhiko Nishimura, Kenji Matsuda, Takahiro Namiki, Seungwon Lee, Norio Nunomura, Teiichiro Matsuzaki, Isao Watababe, Majed Abdel-Jawad, Sungwon Yoon, F. L. Pratt
    • Organizer
      10th International Conference on the Physical Properties and Application of Advanced MATerials (ICPMAT2015)
    • Place of Presentation
      チェンマイ(タイ)
    • Year and Date
      2015-11-17
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] ミュオンスピン緩和法を用いたAl-Mg-Si 合金の研究2014

    • Author(s)
      小牧亮太,西村克彦,松田健二,並木孝洋
    • Organizer
      2014年度 日本物理学会北陸支部 定例学術講演会
    • Place of Presentation
      福井大学
    • Year and Date
      2014-12-13
    • Related Report
      2014 Annual Research Report
  • [Presentation] Muon Spin Relaxation Study of Al-Mg-Si alloys2014

    • Author(s)
      Katsuhiko Nishimura, Kenji Matsuda, Teiichiro Matsuzaki, Sigurd Wenner, Randi Holmestad
    • Organizer
      10th Japanese-Polish Joint Seminar on Micro and Nano Analysis
    • Place of Presentation
      札幌
    • Year and Date
      2014-10-24 – 2014-10-26
    • Related Report
      2014 Annual Research Report
  • [Presentation] Solute-vacancy clustering in Al-Mg-Si alloys studied by muon spin relaxation technique2014

    • Author(s)
      Katsuhiko Nishimura, Kenji Matsuda, Ryota Komaki, Norio Nunomra, Sigurd Wenner, Randi Holmestad, Teiichiro Matsuzaki, Isao Watanabe, Francis L. Pratt
    • Organizer
      The 9th International Conference on the Physical Properties and Application of Advanced Materials (ICPMAT2014)
    • Place of Presentation
      Krakow, Poland
    • Year and Date
      2014-09-14 – 2014-09-18
    • Related Report
      2014 Annual Research Report
  • [Presentation] ミュオンスピン緩和を利用した6000系Al合金の自然時効の研究2014

    • Author(s)
      西村克彦、松田健二、小牧亮太、布村紀男、松崎禎市郎、渡邊功雄、里達雄、Francis Pratt、Randi Holmestad、Sigurd Wenner
    • Organizer
      日本金属学会2014年度春期大会
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] muSR study of Al-0.67%Mg-0.77%Si alloys2014

    • Author(s)
      K Nishimura, K Matsuda, R Komaki, N Nunomura, S Wenner, R Holmestad, T Matsuzaki, I Watanabe, F L Pratt, C D Marioara
    • Organizer
      The 13th International Conference on Muon Spin Rotation, Relaxation and Resonance
    • Place of Presentation
      Grindelwald, Switzerland
    • Related Report
      2013 Annual Research Report
  • [Presentation] ミュオンスピン緩和を利用した6000系Al合金の原子空孔挙動2013

    • Author(s)
      西村克彦、松田健二、小牧亮太、布村紀男、松崎禎市郎、渡邊功雄、里達雄、フランシス プラット、ランディ ホルメシュタット、シグード ウェナー、カリン マリオアラ
    • Organizer
      「不安定原子核の理工学と物性応用研究III」専門研究会
    • Place of Presentation
      京都大学原子炉実験所
    • Related Report
      2013 Annual Research Report

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Published: 2013-05-21   Modified: 2022-01-31  

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