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Active Control on Surface Free Energy of DLC Films

Research Project

Project/Area Number 25420095
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Design engineering/Machine functional elements/Tribology
Research InstitutionNippon Institute of Technology

Principal Investigator

WATANABE Shuichi  日本工業大学, 工学部, 教授 (60220886)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2013: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
KeywordsDLC膜 / 表面自由エネルギー / プラズマ処理 / 表面改質 / 生体適合性 / 摩擦係数
Outline of Final Research Achievements

DLC films can be used in numerous industrial applications, including biomedical modified-surfaces with biocompatible and wetting properties. It is important to understand the surface properties of DLC thin films for these applications. In this study, O2 and CF4 plasma treatment on DLC film surfaces is studied. The results indicate that the oxygen plasma-treated DLC films exhibit a hydrophilic surface due to the introduction of some hydroxyl and carbonyl groups. Surface roughness increased with the addition of CF4 to the O2 plasma, whereas oxygen- and fluorinated-based functional groups were generated on the surface of the DLC films. The surface energy also decreased with increasing CF4 fraction, causing the surface of the films to be hydrophobic. It is concluded that oxygen plasma treatment can be used to make hydrophilic DLC, making it a favorable wetting surface for biomedical applications.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (18 results)

All 2016 2015 2014 2013 Other

All Journal Article (7 results) (of which Peer Reviewed: 6 results,  Open Access: 2 results,  Acknowledgement Compliant: 2 results) Presentation (11 results) (of which Int'l Joint Research: 1 results)

  • [Journal Article] Study on the Applications of Functionally-developed Diamond-like Carbon (DLC) Films “Heat resistant properties of Si-O-DLC and Si-N-DLC films2016

    • Author(s)
      Nutthanun MOOLSRADOO, Anak KHANTACHAWANA, Chavin JONGWANNASIRI and Shuichi WATANABE
    • Journal Title

      日本工業大学研究報告

      Volume: 45 Pages: 15-18

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Improvement of Hydrophilic Stability of Diamond-like Carbon Films by O2/CF4 Plasma Post-treatment2015

    • Author(s)
      Chavin JONGWANNASIRI and Shuichi WATANABE
    • Journal Title

      Advanced Materials Research

      Volume: 1125 Pages: 38-44

    • DOI

      10.4028/www.scientific.net/amr.1125.38

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Heat Resistant Properties of Some Elements-Incorporated Diamond-like Carbon Films and Their Trial Applications for Micro End Mill Coatings2015

    • Author(s)
      Chavin Jongwannasiri, Nutthanun Moolsradoo and Shuichi Watanabe
    • Journal Title

      Materials Sciences and Applications

      Volume: 6 Issue: 01 Pages: 9-15

    • DOI

      10.4236/msa.2015.61002

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of Plasma Treatment on Friction Coefficient of Diamond-like Carbon Films2014

    • Author(s)
      Chavin Jongwannasiri and Shuichi Watanabe
    • Journal Title

      表面技術

      Volume: 65 Pages: 621-624

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Si-N-DLC系コンポジット膜の高温摩擦特性2014

    • Author(s)
      メレーアナス ムハンマド、チャウイン ジョンワンナシリ、渡部修一
    • Journal Title

      表面技術

      Volume: 65 Pages: 631-632

    • NAID

      130005112197

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effects of RF Power and Treatment Time on Wettability of Oxygen Plasma-Treated Diamond-Like Carbon Thin Films2014

    • Author(s)
      Chavin Jongwannasiri and Shuichi Watanabe
    • Journal Title

      International Journal of Chemical Engineering and Applications

      Volume: Vol. 5 Issue: 1 Pages: 13-16

    • DOI

      10.7763/ijcea.2014.v5.342

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Improvement of Thermal Stability and Tribological Performance of Diamond-Like Carbon Composite Thin Films2013

    • Author(s)
      Chavin Jongwannasiri, Xianghui Li and Shuichi Watanabe
    • Journal Title

      Materials Science and Applications

      Volume: Vol. 4 Issue: 10 Pages: 630-636

    • DOI

      10.4236/msa.2013.410077

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] Tribological Behavior of O2 and CF4 Plasma Post-treated Diamond-like Carbon Films in Dry Air and High Humidity Environments2015

    • Author(s)
      Chavin Jongwannnasiri, Shuichi Watanabe
    • Organizer
      19th International Conference on Surface Modification of Materials by Ion Beams
    • Place of Presentation
      Chiang Mai, Thailand
    • Year and Date
      2015-11-20
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Friction Characteristics of O2 and CF4 Plasma Post-Treated DLC Films2015

    • Author(s)
      Chavin JONGWANNASIRI and Shuichi WATANABE
    • Organizer
      表面技術協会第132回講演大会
    • Place of Presentation
      信州大学(長野県 長野市)
    • Year and Date
      2015-09-09
    • Related Report
      2015 Annual Research Report
  • [Presentation] Heat Resistant Properties of Some Elements-Incorporated Diamond-like Carbon Films and Their Trial Applications for Micro End Mill2015

    • Author(s)
      チャウイン ジョンワンナシリ、ナッタナン ムルサラドゥ、渡部修一
    • Organizer
      表面技術協会第131回講演大会
    • Place of Presentation
      関東学院大学 横浜・金沢八景キャンパス
    • Year and Date
      2015-03-05
    • Related Report
      2014 Research-status Report
  • [Presentation] Surface Characteristics of Plasma Post-treated DLC Films Using O2/CF4 Gas Mixture2015

    • Author(s)
      チャウイン ジョンワンナシリ、渡部修一
    • Organizer
      表面技術協会第131回講演大会
    • Place of Presentation
      関東学院大学 横浜・金沢八景キャンパス
    • Year and Date
      2015-03-04
    • Related Report
      2014 Research-status Report
  • [Presentation] Biocompatible Properties of Plasma Treatment of Diamond-like Carbon Thin Films2014

    • Author(s)
      チャウイン ジョンワンナシリ、アナック カンタチャワナ、渡部修一
    • Organizer
      表面技術協会第130回講演大会
    • Place of Presentation
      京都大学 吉田キャンパス
    • Year and Date
      2014-09-22
    • Related Report
      2014 Research-status Report
  • [Presentation] Si-N-DLC系コンポジット膜の高温摩擦特性2014

    • Author(s)
      メレーアナス ムハンマド、チャウイン ジョンワンナシリ、渡部修一
    • Organizer
      表面技術協会第130回講演大会
    • Place of Presentation
      京都大学 吉田キャンパス
    • Year and Date
      2014-09-22
    • Related Report
      2014 Research-status Report
  • [Presentation] Wetting and Biocompatible Properties of Oxygen Plasma Tratemnt on Diamond-like Carbon Thin Films2014

    • Author(s)
      Chavin Jongwannasiri, Anuk Khantachawana and Shuichi Watanabe
    • Organizer
      41st International Conference on Metallurgical Coatings and Thin Films
    • Place of Presentation
      Town & Country Hotel & Convention Center, San Diego USA
    • Year and Date
      2014-04-28
    • Related Report
      2014 Research-status Report
  • [Presentation] Thermal Stability of S-N-DLC Films

    • Author(s)
      Chavin Jongwannasiri, Melih Anas Mohammed and Shuichi Watanabe
    • Organizer
      表面技術協会第128回講演大会
    • Place of Presentation
      福岡工業大学
    • Related Report
      2013 Research-status Report
  • [Presentation] Evaluation of Thermal Durability of Si-N-DLC Films Deposited by PBII

    • Author(s)
      Melih Anas Mohammed, Chavin Jongwannasiri and Shuichi Watanabe
    • Organizer
      ニューダイヤモンドフォーラム第27回ダイヤモンドシンポジウム
    • Place of Presentation
      日本工業大学
    • Related Report
      2013 Research-status Report
  • [Presentation] Thermal Stability and Tribological Performance of Silicon/Nitrogen Co-incorporated Diamond-like Carbon Thin Films

    • Author(s)
      Chavin Jongwannasiri and Shuichi Watanabe
    • Organizer
      The International Conference on Experimental Mechanics 2013 & the 12th Asian Conference on Experimental Mechanics
    • Place of Presentation
      Swissotel Le Concorde, Bangkok
    • Related Report
      2013 Research-status Report
  • [Presentation] Effects on Surface Energy of DLC Films by means of Oxygen Plasma Treatmen

    • Author(s)
      Chavin Jongwannasiri, Anak Khantachawana and Shuichi Watanabe
    • Organizer
      表面技術協会第129回講演大会
    • Place of Presentation
      東京理科大学(野田キャンパス)
    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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