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Surface scrubbing by superhydrophilic PVA brushes and its cleaning mechanism

Research Project

Project/Area Number 25420112
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Fluid engineering
Research InstitutionShizuoka University

Principal Investigator

Sanada Toshiyuki  静岡大学, 工学部, 准教授 (50403978)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2014: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2013: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
KeywordsPVAブラシ / 摩擦 / 表面濡れ性 / 洗浄 / 濡れ性 / 半導体洗浄
Outline of Final Research Achievements

To gain insight into the mechanisms of PVA roller brush cleaning in semiconductor device fabrication, we measure the shear force between PVA brushes and several surfaces. PVA brushes have a sponge-like structure and contain a large amount of water. The contact state between the brush and surface is very complex because of the soft nature of the brush, the asperities on the brush surfaces, and the porous structure of the brush surface. The shear force between the brush and surface is affected by the surface wettability, and the COF is found to decrease and approach 0.5 as the brush rotation speed increases. These results imply that the brush directly makes contact with the surface and that the real contact area of the PVA brush increases with the contact time. Furthermore, we developed a cleaning sample with particles that have optimal adhesive force with the aim of evaluating wet cleaning. Finally, the cleaning performance of PVA brush cleaning was demonstrated.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (18 results)

All 2016 2015 2014 2013 Other

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 1 results) Presentation (16 results) (of which Int'l Joint Research: 1 results,  Invited: 2 results)

  • [Journal Article] Effect of surface wettability on frictional conditions during scrubbing using polyvinyl acetal brush2015

    • Author(s)
      Y. Hara, T. Sanada, A. Fukunaga, H. Hiyama
    • Journal Title

      ECS Journal of Solid State Science and Technology

      Volume: 4 Issue: 5 Pages: 141-148

    • DOI

      10.1149/2.0111505jss

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Frictional Analysis of PVA Brush for Post CMP Cleaning: Effects of Rotation Speed, Compression Distance, and Fluid Viscosity2013

    • Author(s)
      Takashi Fujiwara, Toshiyuki Sanada, Akira Fukunaga, Hirokuni Hiyama
    • Journal Title

      Solid State Phenomena

      Volume: 195 Pages: 213-216

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] 各種膜付半導体ウェーハのPVAロールブラシとの摩擦力測定2016

    • Author(s)
      西尾賢哉
    • Organizer
      応用物理学会界面ナノ電子化学研究会第2回ポスター展
    • Place of Presentation
      慶應義塾大学(横浜市、神奈川県)
    • Year and Date
      2016-03-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 洗浄用高付着力サンプルの作成とPVAブラシや液滴列による除去率評価2016

    • Author(s)
      徳田絵夢,真田俊之,岩田太,高東智佳子,檜山浩國,福永明
    • Organizer
      日本機械学会 関東支部第22期講演会
    • Place of Presentation
      東京工業大学(目黒区、東京都)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] 洗浄液浸漬下におけるPVAロールブラシと各種膜付半導体ウェーハとの摩擦力測定2016

    • Author(s)
      西尾賢哉,真田俊之,浜田聡美,檜山浩國,福永明
    • Organizer
      日本機械学会 関東支部第22期講演会
    • Place of Presentation
      東京工業大学(目黒区、東京都)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] Normal force and behavior of containing water during the compression of PVA brush2015

    • Author(s)
      K. Nishio, T. Sanada, A. Fukunaga, H. Hiyama
    • Organizer
      2015 International Conference on Planarization/CMP Technology
    • Place of Presentation
      アリゾナ州、アメリカ合衆国
    • Year and Date
      2015-09-30
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 表面濡れ性の違いによるPVAロールブラシの摩擦力と水のしみ出し挙動2015

    • Author(s)
      西尾賢哉,真田俊之,檜山浩國,福永明
    • Organizer
      第76回応用物理学会秋季学術講演会
    • Place of Presentation
      名古屋国際会議場(名古屋市、愛知県)
    • Year and Date
      2015-09-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] PVAロールブラシの摩擦特性に及ぼす表面濡れ性の影響2015

    • Author(s)
      西尾賢哉,原義高,真田俊之,福永明,檜山浩國
    • Organizer
      機械学会関東支部第21期講演会
    • Place of Presentation
      横浜国立大学, 横浜市, 神奈川県, 日本
    • Year and Date
      2015-03-20 – 2015-03-21
    • Related Report
      2014 Research-status Report
  • [Presentation] Measurements of Normal and friction forces during brush cleaning2014

    • Author(s)
      K. Nishio, Y. Hara, T. Sanada, A. Fukunaga, H. Hiyama
    • Organizer
      International Conference on Planarization/CMP Technology (ICPT2014)
    • Place of Presentation
      神戸国際会議場, 神戸, 兵庫県, 日本
    • Year and Date
      2014-11-19 – 2014-11-21
    • Related Report
      2014 Research-status Report
  • [Presentation] Viscoelasticity behavior of PVA brush and its impact on friction: A Guideline for Nodule Configuration2014

    • Author(s)
      Y. Hara, T. Sanada, A. Fukunaga, H. Hiyama
    • Organizer
      12th International Symposium on Ultra Clean Processing of Semiconductor Surfaces(UCPSS2014)
    • Place of Presentation
      Brussels44Center, Brussels, ベルギー王国
    • Year and Date
      2014-09-21 – 2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] PVAブラシ粘弾性と摩擦特性2014

    • Author(s)
      真田俊之,原義高,福永明,檜山浩國
    • Organizer
      応用物理学会シンポジウム
    • Place of Presentation
      北海道大学, 札幌市, 北海道, 日本
    • Year and Date
      2014-09-17
    • Related Report
      2014 Research-status Report
  • [Presentation] Viscoelasticity behavior of PVA brush and its impact on friction2014

    • Author(s)
      T. Sanada, Y. Hara, A. Fukunaga, H. Hiyama
    • Organizer
      19th International Symposium on Chemical-Mechanical Planarization
    • Place of Presentation
      Albany Marriott Hotel, Albany, New York, アメリカ合衆国
    • Year and Date
      2014-08-10 – 2014-08-13
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] Influence of traverse speed and surface wettability on the friction of PVA brush for post CMP cleaning

    • Author(s)
      T. Sanada, A. Fukunaga, H. Hiyama
    • Organizer
      18th International Symposium on Chemical-Mechanical Planarization
    • Place of Presentation
      Lake Placid (USA)
    • Related Report
      2013 Research-status Report
  • [Presentation] The effect of surface wettability on the frictional condition for PVA roll brush

    • Author(s)
      Y. Hara, T. Sanada, A. Fukunaga, H. Hiyama
    • Organizer
      13th International Symposium on Semiconductor Cleaning Science and Technology (SCST13)
    • Place of Presentation
      San Fransico (USA)
    • Related Report
      2013 Research-status Report
  • [Presentation] A Frictional Analysis of PVA Brush for Post CMP Cleaning

    • Author(s)
      T. Sanada
    • Organizer
      SEMICON Korea SEMI Technology Symposiumu S5 Contamination-free Manufacturing and CMP Technology
    • Place of Presentation
      Seoul (Korea)
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] PVAロールブラシの摩擦特性

    • Author(s)
      原義高,真田俊之,福永明,檜山浩國
    • Organizer
      混相流シンポジウム2013
    • Place of Presentation
      長野
    • Related Report
      2013 Research-status Report
  • [Presentation] 洗浄用超親水性PVAブラシの摩擦特性

    • Author(s)
      真田俊之,原義高,福永明,檜山浩國
    • Organizer
      日本機械学会年次大会
    • Place of Presentation
      岡山
    • Related Report
      2013 Research-status Report
  • [Presentation] CMP後洗浄用PVAブラシの摩擦特性

    • Author(s)
      真田俊之,原義高,福永明,檜山浩國
    • Organizer
      応用物理学会シンポジウム
    • Place of Presentation
      京都
    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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