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Development of ex situ processed MgB2 condoctors with strong grain connectivity

Research Project

Project/Area Number 25420696
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Physical properties of metals/Metal-base materials
Research InstitutionNational Institute for Materials Science

Principal Investigator

FUJII Hiroki  国立研究開発法人物質・材料研究機構, 高温超伝導線材グループ, 主席研究員 (80354306)

Project Period (FY) 2013-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2014: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2013: ¥3,380,000 (Direct Cost: ¥2,600,000、Indirect Cost: ¥780,000)
Keywords二硼化マグネシウム / ex situ法線材 / 臨界電流密度特性 / 結晶粒間結合 / MgO層除去 / 高エネルギー粉砕処理 / ピン留め点 / 上部臨界磁界 / 高活性粉末 / 結晶子サイズ / 二硼化マグネシウム線材 / ex situ法 / 強結合 / 不活性ガス雰囲気 / 充填粉精製 / 超伝導線材 / 酸化マグネシウム除去 / 溶液処理
Outline of Final Research Achievements

In order to improve grain connectivity in ex situ processed MgB2 conductors,we have made attempt to remove MgO layers on the surface of MgB2 grains. Among three methods,the dissolution in weak acid solutions, reduction by the addition of Ca compounds and mechnical removal through ball milling process, the most effective method was the mechanical removal. Althohgh this method is already studied by several authors, with paying attention to the highly reactive milled powders, the Jc value at 4.2 K and 10 T was doubled and the optimized heat-treatment temerature decreased by more than 100 degree, compared with the previously reported values.

Report

(5 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (9 results)

All 2017 2016 2015 2014 2013

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 2 results,  Open Access: 1 results) Presentation (6 results)

  • [Journal Article] Improved critical current density in ex situ processed MgB2 tapes by the size reduction of grains and crystallites by high-energy ball milling2017

    • Author(s)
      H. Fujii, A. Ishitoya, S. Itoh, K. Ozawa, H. Kitaguchi
    • Journal Title

      Cryogenics

      Volume: 82 Pages: 15-24

    • DOI

      10.1016/j.cryogenics.2017.01.002

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effect of additions of Ca compounds to the filling powder on the reduction of MgO and the critical current density properties of ex situ processed MgB2 tapes2016

    • Author(s)
      H. Fujii, A. Ishitoya, S. Itoh, K. Ozawa and H. Kitaguchi
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 664 Pages: 650-656

    • DOI

      10.1016/j.jallcom.2016.01.027

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] The effect of refinement of carbon-substituted MgB2 filling powder using various starting powders on the microstructure and critical current density of ex situ processed superconducting tapes2014

    • Author(s)
      H. Fujii, K. Ozawa, and H. Kitaguchi
    • Journal Title

      Superconducting Science and Technology

      Volume: 27 Issue: 3 Pages: 035002-035002

    • DOI

      10.1088/0953-2048/27/3/035002

    • Related Report
      2013 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] 活性粉末を使用したex situ法MgB2線材の最適加熱処理温度2017

    • Author(s)
      藤井宏樹、石戸谷章、伊藤真二、北口仁
    • Organizer
      2017年春季低温工学・超電導学会
    • Place of Presentation
      タワーホール船堀
    • Year and Date
      2017-05-22
    • Related Report
      2016 Annual Research Report
  • [Presentation] 活性粉末を使用したex situ法MgB2線材の作製と臨界電流密度特性2016

    • Author(s)
      藤井宏樹、石戸谷章、伊藤真二、小澤清、北口仁
    • Organizer
      2016年春季低温工学・超電導学会
    • Place of Presentation
      タワーホール船堀
    • Year and Date
      2016-05-30
    • Related Report
      2016 Annual Research Report
  • [Presentation] 還元剤添加によるex situ法MgB2線材の臨界電流密度特性の改善2015

    • Author(s)
      藤井宏樹、石戸谷章、伊藤真二、小澤清、北口仁
    • Organizer
      2015年秋季低温工学・超電導学会
    • Place of Presentation
      姫路商工会議所(兵庫県姫路市)
    • Year and Date
      2015-12-02
    • Related Report
      2015 Research-status Report
  • [Presentation] ex situ法MgB2線材の臨界電流密度特性に及ぼす充填粉への還元剤添加効果2015

    • Author(s)
      藤井宏樹、小澤清、北口仁
    • Organizer
      2015年春季低温工学・超電導学会
    • Place of Presentation
      産業技術総合研究所つくばセンター共用講堂(茨城県つくば市)
    • Year and Date
      2015-05-27
    • Related Report
      2015 Research-status Report
  • [Presentation] 精製したMgB2-xCx粉を用いて作製したex situ法線材の超伝導特性2014

    • Author(s)
      藤井宏樹、小澤清、北口仁
    • Organizer
      2014年春季低温工学・超電導学会
    • Place of Presentation
      タワーホール船堀
    • Year and Date
      2014-05-26 – 2014-05-28
    • Related Report
      2014 Research-status Report
  • [Presentation] ex situ法炭素置換MgB2線材の作製と超伝導特性2013

    • Author(s)
      藤井 宏樹、小澤 清、北口 仁
    • Organizer
      低温工学・超電導学会
    • Place of Presentation
      タウンホール船堀
    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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