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Search for aluminum-based hydride using various quantum-beam in-situ observation techniques

Research Project

Project/Area Number 25420725
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionJapan Atomic Energy Agency

Principal Investigator

Saitoh Hiroyuki  国立研究開発法人日本原子力研究開発機構, 原子力科学研究部門 量子ビーム応用研究センター, 研究主幹 (20373243)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2015: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2014: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2013: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Keywords高温高圧 / 水素化物 / 放射光 / 中性子 / アルミニウム合金 / アルミニウム水素化物 / 放射光その場観察 / アルミニウム合金水素化物 / 中性子線回折その場観察
Outline of Final Research Achievements

High-pressure technique is effective for realizing novel materials that cannot be obtained around ambient pressure. We explored novel aluminum-based hydrides using the technique to develop light-weight, compact, and safe hydrogen storage method. To explore these materials, various quantum-beam in-situ observation techniques have been developed.
We have succeeded in synthesis of aluminum-based hydride by hydrogenating Al2Cu alloy at 10 GPa and 800°C. Hydrogenation reactions of metals have been observed in situ using x-ray absorption fine structure and neutron diffraction measurements.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (37 results)

All 2016 2015 2014 2013

All Journal Article (13 results) (of which Peer Reviewed: 9 results,  Acknowledgement Compliant: 10 results,  Open Access: 2 results) Presentation (23 results) (of which Int'l Joint Research: 2 results,  Invited: 8 results) Book (1 results)

  • [Journal Article] 新規金属水素化物の高温高圧合成2016

    • Author(s)
      齋藤 寛之, 高木 成幸, 折茂 慎一, 青木 勝敏
    • Journal Title

      粉体および粉末冶金

      Volume: 63

    • NAID

      130005156351

    • Related Report
      2015 Annual Research Report
    • Acknowledgement Compliant
  • [Journal Article] 高温高圧下における鉄の重水素化反応のその場観察2016

    • Author(s)
      齋藤 寛之, 町田 晃彦, 青木 勝敏
    • Journal Title

      高圧力の科学と技術

      Volume: 26

    • NAID

      130005158541

    • Related Report
      2015 Annual Research Report
    • Acknowledgement Compliant
  • [Journal Article] Hydrogenation of L12-type AlNi3 alloy at high pressure and temperature2015

    • Author(s)
      N. Endo, H. Saitoh, A. Machida, Y. Katayama
    • Journal Title

      Journal Alloys and Compounds

      Volume: 印刷中 Pages: S61-S63

    • DOI

      10.1016/j.jallcom.2015.01.200

    • Related Report
      2015 Annual Research Report 2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] fcc Fe 中の重水素原子のサイト占有状態2015

    • Author(s)
      青木勝敏,町田晃彦,齋藤寛之,服部高典,佐野亜沙美
    • Journal Title

      波紋

      Volume: 25 Pages: 26-31

    • NAID

      130007510577

    • Related Report
      2015 Annual Research Report
  • [Journal Article] True boundary for the formation of homoleptic transition-metal hydride complexes2015

    • Author(s)
      S. Takagi, Y. Iijima, T. Sato, H. Saitoh, K. Ikeda, T. Otomo, K. Miwa, T. Ikeshoji, K. Aoki, S. Orimo
    • Journal Title

      Angewandte Chemie International Edition

      Volume: 54 Issue: 19 Pages: 5650-5653

    • DOI

      10.1002/anie.201500792

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Phase diagram of the Eu–H system at high temperatures and high hydrogen pressures2015

    • Author(s)
      H. Saitoh, A. Machida, T. Matsuoka, K. Aoki
    • Journal Title

      Solid State Communications

      Volume: 205 Pages: 24-27

    • DOI

      10.1016/j.ssc.2014.12.019

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Hydrogenation of a TiFe-based alloy at high pressures and temperatures2015

    • Author(s)
      N. Endo, I. Saita, Y. Nakamura, H. Saitoh, A. Machida
    • Journal Title

      International Journal of Hydrogen Energy

      Volume: 40 Issue: 8 Pages: 3283-3287

    • DOI

      10.1016/j.ijhydene.2015.01.015

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Hydrogenation of Anodized Aluminum and Crystal Growth of Formed Hydride at High Pressure and High Temperature2014

    • Author(s)
      H. Saitoh, S. Kato, M. Katagiri
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 55 Issue: 8 Pages: 1114-1116

    • DOI

      10.2320/matertrans.MG201411

    • NAID

      130004825215

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Li4FeH6: iron-containing complex hydride with high gravimetric hydrogen density2014

    • Author(s)
      H. Saitoh, S. Takagi, M. Matsuo, Y. Iijima, N. Endo, K. Aoki, S. Orimo
    • Journal Title

      APL Materials

      Volume: 2 Issue: 7 Pages: 076103-076103

    • DOI

      10.1063/1.4886219

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Synchrotron X-ray diffraction techniques for in situ measurement of hydride formation under several gigapascals of hydrogen pressure2014

    • Author(s)
      H. Saitoh, A. Machida, K. Aoki
    • Journal Title

      Chinese Science Bulletin

      Volume: 59 Issue: 36 Pages: 5290-5301

    • DOI

      10.1007/s11434-014-0543-8

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Site occupancy of interstitial deuterium atoms in face-centred cubic iron2014

    • Author(s)
      A. Machida, H. Saitoh, H. Sugimoto, T. Hattori, A. Sano-Furukawa, N. Endo, Y. Katayama, R. Iizuka, T. Sato, M. Matsuo, S. Orimo, K. Aoki
    • Journal Title

      Nature Communications

      Volume: 5 Issue: 1 Pages: 5063-5063

    • DOI

      10.1038/ncomms6063

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] 放射光その場観察を用いた高温高圧下での新規金属水素化物合成2014

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Journal Title

      放射光

      Volume: 27 Pages: 10-19

    • NAID

      40019965794

    • Related Report
      2013 Research-status Report
  • [Journal Article] Synthesis and formation process of Al2CuHx: A new class of interstitial aluminum-based alloy hydride2013

    • Author(s)
      H. Saitoh, S. Takagi, N. Endo, A. Machida, K. Aoki, S. Orimo, Y. Katayama
    • Journal Title

      APL Materials

      Volume: 1 Issue: 3

    • DOI

      10.1063/1.4821632

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] Syntheses of novel hydrides under high pressure and high temperature2016

    • Author(s)
      H. Saitoh, S.Takagi, K.Aoki, S.Orimo
    • Organizer
      THERMEC'2016
    • Place of Presentation
      Graz, Austria
    • Year and Date
      2016-05-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] TiCo3合金の高温高圧での水素化2016

    • Author(s)
      齋藤寛之, 森本勝太
    • Organizer
      日本金属学会2016年春期(第158回)大会, 東京理科大葛飾キャンパス
    • Place of Presentation
      東京理科大葛飾キャンパス(東京)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 放射光を利用した金属水素化物の高温高圧合成2016

    • Author(s)
      齋藤寛之
    • Organizer
      フロンティア機能物質創製センター第2回シンポジウム
    • Place of Presentation
      兵庫県立先端科学技術支援センター(上郡)
    • Year and Date
      2016-03-05
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] 放射光と高温高圧法を利用した新しい水素貯蔵材料の探索2016

    • Author(s)
      齋藤寛之
    • Organizer
      第2回放射光設備利用講習会
    • Place of Presentation
      津山高専(津山)
    • Year and Date
      2016-02-29
    • Related Report
      2015 Annual Research Report
  • [Presentation] SYNTHESES OF NOVEL HYDRIDES UNDER HIGH PRESSURE2016

    • Author(s)
      H. Saitoh, S.Takagi, K.Aoki, S.Orimo
    • Organizer
      10th Int. Symposium "Hydrogen & Energy"
    • Place of Presentation
      ラフォーレ蔵王(蔵王)
    • Year and Date
      2016-02-21
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 新規金属水素化物の高温高圧合成2015

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Organizer
      粉体粉末冶金協会 平成27年度秋季大会
    • Place of Presentation
      京都大学吉田キャンパス(京都)
    • Year and Date
      2015-11-11
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] 放射光その場観察を利用した金属錯体水素化物の高温高圧合成研究2015

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Organizer
      第56回高圧討論会
    • Place of Presentation
      JMSアステールプラザ(広島)
    • Year and Date
      2015-11-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高温高圧法による新規水素化物の合成研究22015

    • Author(s)
      齋藤 寛之, 高木 成幸, 折茂 慎一
    • Organizer
      第2回 「公益社団法人日本金属学会研究会 水素化物に関わる次世代学術・応用展開研究会」
    • Place of Presentation
      金沢大学角間キャンパス(金沢)
    • Year and Date
      2015-10-22
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高密度水素化物実現を目指した高温高圧合成研究2015

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Organizer
      日本金属学会 2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学伊都キャンパス(博多)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] アルミニウムを主原料とする新しい水素貯蔵合金の合成2015

    • Author(s)
      齋藤寛之
    • Organizer
      SPring-8シンポジウム2015
    • Place of Presentation
      九州大学伊都キャンパス(博多)
    • Year and Date
      2015-09-13
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] 高温高圧法を利用した新規水素貯蔵材料開発2015

    • Author(s)
      齋藤寛之
    • Organizer
      平成27年度 第10回水素若手研究会
    • Place of Presentation
      産総研福島再生可能エネルギー研究所(郡山)
    • Year and Date
      2015-08-24
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] CsCl型構造アルミニウム合金 AlFe, AlCo, AlNiの高温高圧下での水素化2015

    • Author(s)
      遠藤成輝, 齋藤寛之, 町田晃彦
    • Organizer
      日本金属学会2015年春期講演大会
    • Place of Presentation
      東京大学 (東京都目黒区)
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] 新規金属水素化物の合成研究2015

    • Author(s)
      齋藤寛之
    • Organizer
      第2回愛媛大学先進超高圧科学研究拠点(PRIUS)シンポジウム
    • Place of Presentation
      愛媛大学 (愛媛県松山市)
    • Year and Date
      2015-02-23 – 2015-02-24
    • Related Report
      2014 Research-status Report
  • [Presentation] [ONSA賞受賞講演]放射光その場観察を利用した新しい水素貯蔵合金開発2015

    • Author(s)
      齋藤寛之
    • Organizer
      一般社団法人大阪ニュークリアサイエンス協会 第23回 放射線利用総合シンポジウム
    • Place of Presentation
      大阪大学中之島センター(大阪府大阪市)
    • Year and Date
      2015-01-26
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] Li4FeH6の高温高圧合成2014

    • Author(s)
      齋藤寛之, 高木成幸, 松尾元彰, 飯島祐樹, 遠藤成輝, 青木勝敏, 折茂慎一
    • Organizer
      第55回高圧討論会
    • Place of Presentation
      徳島大学 (徳島県徳島市)
    • Year and Date
      2014-11-22 – 2014-11-24
    • Related Report
      2014 Research-status Report
  • [Presentation] 放射光その場観察を利用した新規水素化物の探索2014

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Organizer
      第12回 水素量子アトミクス研究会
    • Place of Presentation
      東北大学金属材料研究所 (宮城県仙台市)
    • Year and Date
      2014-10-22 – 2014-10-23
    • Related Report
      2014 Research-status Report
  • [Presentation] 高温高圧法による新規水素化物の合成研究2014

    • Author(s)
      齋藤寛之, 高木成幸, 青木勝敏, 折茂慎一
    • Organizer
      金属学会研究会「水素化物に関わる次世代学術・応用展開研究会」
    • Place of Presentation
      東北大学金属材料研究所 (宮城県仙台市)
    • Year and Date
      2014-10-21 – 2014-10-22
    • Related Report
      2014 Research-status Report
  • [Presentation] 高温高圧下でのAlNi3合金の水素化2014

    • Author(s)
      遠藤成輝, 齋藤寛之, 町田晃彦
    • Organizer
      日本金属学会2014年秋期講演大会
    • Place of Presentation
      名古屋大学 (愛知県名古屋市)
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Research-status Report
  • [Presentation] Aluminum-based Interstitial Hydride, Al2CuHx2014

    • Author(s)
      H. Saitoh, S. Takagi, N. Endo, A. Machida, K. Aoki, S. Orimo, and Y. Katayama
    • Organizer
      14th International Symposium on Metal-Hydrogen Systems
    • Place of Presentation
      Manchester (UK)
    • Year and Date
      2014-07-20 – 2014-07-25
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] 新規鉄錯体水素化物Li4FeH6の高温高圧合成2014

    • Author(s)
      齋藤寛之、高木成幸、松尾元彰、飯島祐樹、遠藤成輝、青木勝敏、折茂慎一
    • Organizer
      日本金属学会 2014年春期(第154回)講演大会
    • Place of Presentation
      東京
    • Related Report
      2013 Research-status Report
  • [Presentation] Synthesis of novel Al-based alloy hydrides under high pressure and high temperature2013

    • Author(s)
      Hiroyuki Saitoh, Naruki Endo, Akihiko Machida, Yoshinori Katayama, and Katsutoshi Aoki
    • Organizer
      17th International Conference on Crystal Growth and Epitaxy
    • Place of Presentation
      Warsaw, Poland
    • Related Report
      2013 Research-status Report
  • [Presentation] 齋藤寛之、高木成幸、遠藤成輝、町田晃彦、青木勝敏、折茂慎一、片山芳則2013

    • Author(s)
      侵入型水素化物Al2CuHx (x~1)の結晶構造
    • Organizer
      日本金属学会 2013年秋期(第153回)講演大会
    • Place of Presentation
      金沢
    • Related Report
      2013 Research-status Report
  • [Presentation] 侵入型アルミニウム合金水素化物, Al2CuHx2013

    • Author(s)
      齋藤寛之、高木成幸、遠藤成輝、町田晃彦、青木勝敏、折茂慎一、片山芳則
    • Organizer
      第54回高圧討論会
    • Place of Presentation
      新潟
    • Related Report
      2013 Research-status Report
  • [Book] The Lightest Metals2015

    • Author(s)
      Timothy P. Hanusa
    • Total Pages
      496
    • Publisher
      Wiley
    • Related Report
      2015 Annual Research Report

URL: 

Published: 2014-07-25   Modified: 2019-07-29  

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