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Elucidation of the relationship between resistance to hydrogen embrittlement and the structure of surface oxide film

Research Project

Project/Area Number 25420750
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Structural/Functional materials
Research InstitutionIbaraki University

Principal Investigator

Itoh Goroh  茨城大学, 工学部, 教授 (80158758)

Co-Investigator(Kenkyū-buntansha) ITOH NOBUHIDE  茨城大学, 工学部, 教授 (70203156)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2013: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords表面酸化皮膜 / 水素 / アルミニウム合金 / 塑性変形 / 粒界 / すべり線 / 段差 / 無析出帯 / 酸化皮膜 / 金属材料 / 水素脆化 / 水素挙動 / 第2相 / 金属間化合物
Outline of Final Research Achievements

In ferritic steels, it was found that the surface oxide film is not a crucial barrier for hydrogen emission. In an Al-9%Mg alloy, hydrogen emission was observed in some of the grain boundaries as well as slip bands when specimen was deformed in tension. At the grain boundaries where hydrogen was emitted, it was presumed that the hydrogen was transported with slipping in a neighboring grain, with a formation of the surface step causing the fracture of the surface oxide film, and then emitted. In an Al-Zn-Mg alloy, similar result was obtained but the deformation was localized near the grain boundaries because of the presence of the precipitate free zones, and hence hydrogen was emitted at grain boundaries with more variety. Therefore, it was concluded that the surface oxide film plays an important role in hydrogen intrusion and emission.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (9 results)

All 2015 2014 2013

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (7 results) (of which Int'l Joint Research: 1 results,  Invited: 2 results) Book (1 results)

  • [Journal Article] Behavior of Hydrogen in a Tensile-Deformed Al-Mg Alloy2015

    • Author(s)
      真中俊明, 伊藤吾朗, 小山僚人
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 79 Issue: 3 Pages: 137-141

    • DOI

      10.2320/jinstmet.JC201411

    • NAID

      130004786487

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] BEHAVIOR OF HYDROGEN IN AN AL-ZN-MG ALLOY INVESTIGATED BY MEANS OF HYDROGEN MICROPRINT TECHNIQUE2015

    • Author(s)
      T. Manaka and G. Itoh
    • Organizer
      54th Annual Conference of Metallurgists
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Al-Zn-Mg合金の水素挙動に及ぼす応力負荷の影響2015

    • Author(s)
      真中俊明、伊藤吾朗、中井学
    • Organizer
      軽金属学会第129回秋期大会
    • Related Report
      2015 Annual Research Report
  • [Presentation] アルミニウム合金の水素挙動に及ぼす応力負荷や調質の影響2015

    • Author(s)
      真中俊明、小塚健司、伊藤吾朗、波多野雄治
    • Organizer
      軽金属学会第128回春期大会
    • Related Report
      2015 Annual Research Report
  • [Presentation] Hydrogen behavior in tensile-deformed Al-Zn-Mg alloy and Al-Mg alloy2014

    • Author(s)
      T. Manaka and G. Itoh
    • Organizer
      APCFS/SIF-2014 International Congress
    • Place of Presentation
      The University of Sydney
    • Year and Date
      2014-12-09 – 2014-12-12
    • Related Report
      2014 Research-status Report
  • [Presentation] アルミニウムの水素分析に及ぼす表面状態の影響,2014

    • Author(s)
      伊藤吾朗, 中川雄嗣, 寺田将也, 國井健生
    • Organizer
      軽金属学会第127回秋期大会
    • Place of Presentation
      東京工業大学大岡山キャンパス
    • Year and Date
      2014-11-15 – 2014-11-16
    • Related Report
      2014 Research-status Report
  • [Presentation] Hydrogen Embrittlement in 7000 Series Aluminum Alloys2013

    • Author(s)
      伊藤吾朗
    • Organizer
      1st Asian Conference on Aluminum Alloys
    • Place of Presentation
      中国、北京
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] Hydrogen behavior in aluminum alloys and steels2013

    • Author(s)
      伊藤吾朗
    • Organizer
      8th International Conference on Processing & Manufacturing of Advanced Materials
    • Place of Presentation
      アメリカ合衆国、ラスベガス
    • Related Report
      2013 Research-status Report
    • Invited
  • [Book] アルミニウム中の水素量の分析技術2015

    • Author(s)
      伊藤吾朗(分担執筆)
    • Total Pages
      56
    • Publisher
      一般社団法人軽金属学会
    • Related Report
      2014 Research-status Report

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Published: 2014-07-25   Modified: 2021-12-27  

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