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Micromechanical characterization of hydrogen embrittlement related to martensitic transformation

Research Project

Project/Area Number 25420758
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Structural/Functional materials
Research InstitutionKumamoto University

Principal Investigator

Mine Yoji  熊本大学, 自然科学研究科, 准教授 (90372755)

Co-Investigator(Kenkyū-buntansha) TAKASHIMA KAZUKI  熊本大学, 大学院自然科学研究科, 教授 (60163193)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2015: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2014: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2013: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Keywords水素脆化 / 変形誘起マルテンサイト変態 / ステンレス鋼 / マイクロ材料試験 / 構造・機能材料
Outline of Final Research Achievements

Micro-bending and micro-tensile testing was employed to clarify the effect of microstructure developed by deformation with hydrogen on hydrogen embrittlement of metastable austenitic steel. Micro-bending testing of microstructures developed at the crack tip revealed that cracking readily occurred in the specimen deformed with hydrogen. Micro-tensile testing of samples processed by high-pressure torsion revealed the effect of intermediate phase for martensitic transformation on plasticity. Deformation-twinning in the uncharged steel acts as an intermediate phase in the transformation to alpha prime martensite, which contributes to a good balance between strength and ductility. Hydrogen charging in the steel facilitates the formation of epsilon martensite as an intermediate phase in the transformation, thereby leading to the strain localization. However, dynamic alpha prime martensitic transformation in the presence of hydrogen is requisite for severe HE with quasi-cleavage.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (27 results)

All 2016 2015 2014 Other

All Int'l Joint Research (1 results) Journal Article (4 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 4 results,  Open Access: 2 results,  Acknowledgement Compliant: 4 results) Presentation (20 results) (of which Int'l Joint Research: 4 results,  Invited: 2 results) Remarks (2 results)

  • [Int'l Joint Research] Karlsruhe Institute of Technology(Germany)

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Hydrogen embrittlement of ultrafine-grained stainless steels with different stabilities of the austenitic phase2016

    • Author(s)
      Yoji Mine, Daisuke Haraguchi, Takahiro Ideguchi, Nobuaki Horita, Zenji Horita, Kazuki Takashima
    • Journal Title

      ISIJ International

      Volume: 56 Issue: 6 Pages: 1083-1090

    • DOI

      10.2355/isijinternational.isijint-2015-664

    • NAID

      130005164510

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Mechanical characterisation of microstructural evolution in 304 stainless steel subjected to high-pressure torsion with and without hydrogen pre-charging2016

    • Author(s)
      Yoji Mine, Kaoru Koga, Kazuki Takashima, Zenji Horita
    • Journal Title

      Materials Science and Engineering A

      Volume: 661 Pages: 87-95

    • DOI

      10.1016/j.msea.2016.03.018

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Mechanical characterisation of hydrogen-induced quasi-cleavage in a metastable austenitic steel using micro-tensile testing2016

    • Author(s)
      Yoji Mine, Kaoru Koga, Oliver Kraft, Kazuki Takashima
    • Journal Title

      Scripta Materialia

      Volume: 113 Pages: 176-179

    • DOI

      10.1016/j.scriptamat.2015.11.013

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] High-pressure torsion of metastable austenitic stainless steel at moderate temperatures2015

    • Author(s)
      Y. Mine, D. Haraguchi, Z. Horita, K. Takashima
    • Journal Title

      Philosophical Magazine Letters

      Volume: 95 Issue: 5 Pages: 269-276

    • DOI

      10.1080/09500839.2015.1051602

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] ステンレス鋼SUS304における双晶界面が関与した水素誘起き裂進展挙動2016

    • Author(s)
      植木翔平,古賀 薫,峯 洋二,高島和希
    • Organizer
      日本鉄鋼協会第171回春季講演大会
    • Place of Presentation
      東京・東京理科大
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] オーステナイト系ステンレス鋼SUS304超微細粒材の水素脆化2016

    • Author(s)
      峯 洋二,高島和希,堀田伸明,堀田善治
    • Organizer
      日本鉄鋼協会第171回春季講演大会
    • Place of Presentation
      東京・東京理科大
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] Characterization of hydrogen embrittlement related to martensitic transformation in a type 304 austenitic stainless steel2015

    • Author(s)
      Yoji Mine, Ryo Matsuoka, Kaoru Koga, Kazuki Takashima, Oliver Kraft
    • Organizer
      2015 MRS Fall Meeting & Exhibit
    • Place of Presentation
      Boston, USA
    • Year and Date
      2015-11-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 超微細粒SUS304水素脆化挙動に及ぼす結晶粒径の影響2015

    • Author(s)
      堀田伸明,峯 洋二,高島和希,堀田善治
    • Organizer
      日本金属学会2015年秋期講演大会
    • Place of Presentation
      福岡・九大
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] Characterization of hydrogen embrittlement of ultrafine-grained 304 austenitic stainless steel using microtension testing2015

    • Author(s)
      Nobuaki Horita, Yoji Mine, Kazuki Takashima, Zenji Horita
    • Organizer
      17th International Conference on the Strength of Materials
    • Place of Presentation
      Brno, Czech Republic
    • Year and Date
      2015-08-09
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Microtension testing of single-crystalline austenitic stainless steel with mechanical twins2015

    • Author(s)
      Yoji Mine, Kaoru Koga, Shoki Nakamichi, Kazuki Takashima, Zenji Horita
    • Organizer
      17th International Conference on the Strength of Materials
    • Place of Presentation
      Brno, Czech Republic
    • Year and Date
      2015-08-09
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Microtension behavior of hydrogen-containing metastable austenitic stainless steel2015

    • Author(s)
      Ryo Matsuoka, Kaoru Koga, Yoji Mine, Kazuki Takashima
    • Organizer
      12th International Conference on the Mechanical Behavior of Materials
    • Place of Presentation
      Karlsruhe, Germany
    • Year and Date
      2015-05-10
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] マイクロ引張試験によるSUS304超微細粒材の水素脆化挙動の解析2015

    • Author(s)
      堀田伸明, 峯 洋二, 高島和希,堀田善治
    • Organizer
      日本鉄鋼協会第169回春季講演大会
    • Place of Presentation
      東京・東京大学
    • Year and Date
      2015-03-19
    • Related Report
      2014 Research-status Report
  • [Presentation] Microtension Behavior of Single Crystals with Mechanical Twins in Stable Austenitic Stainless Steel2014

    • Author(s)
      Yoji Mine, Shoki Nakamichi, Kaoru Koga, Kazuki Takashima, Zenji Horita
    • Organizer
      2015 MRS Fall Meeting and Exhibits
    • Place of Presentation
      Boston, USA
    • Year and Date
      2014-12-01
    • Related Report
      2014 Research-status Report
  • [Presentation] Micromechanical characterization of hierarchical micro/nano structures in steels2014

    • Author(s)
      Yoji Mine, Kazuki Takashima
    • Organizer
      The 4th International Symposium on Steel Science
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2014-11-06
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] 鉄鋼材料を構成する微視組織要素のマイクロ引張挙動2014

    • Author(s)
      峯洋二, 高島和希
    • Organizer
      日本鉄鋼協会第168回秋季講演大会
    • Place of Presentation
      名古屋・名古屋大学
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] 変形双晶を有するオーステナイト系ステンレス鋼単結晶のマイクロ引張試験2014

    • Author(s)
      古賀薫,峯洋二,高島和希,堀田善治
    • Organizer
      日本金属学会2014年秋期講演大会
    • Place of Presentation
      名古屋・名古屋大学
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] 温間HPT加工による準安定オーステナイト系ステンレス鋼における組織の発達と引張変形挙動の観察2014

    • Author(s)
      原口大佑, 峯洋二, 堀田善治
    • Organizer
      日本金属学会2014年秋期講演大会
    • Place of Presentation
      名古屋・名古屋大学
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] Hydrogen effect on deformation behaviour of type 304 austenitic stainless steel processed by high-pressure torsion at warm temperature2014

    • Author(s)
      Yoji Mine, Takahiro Ideguchi, Kazuki Takashima, Zenji Horita, Jean-Marc Olive
    • Organizer
      The 6th International Conference on Nanomaterials by Severe Plastic Deformation
    • Place of Presentation
      Metz, France
    • Year and Date
      2014-07-01
    • Related Report
      2014 Research-status Report
  • [Presentation] Microtension behavior of heterogeneous microstructures of type 304 stainless steel formed by high-pressure torsion in the presence of hydrogen

    • Author(s)
      Yoji Mine, Kaoru Koga, Kazuki Takashima, Zenji Horita
    • Organizer
      THERMEC' 2013
    • Place of Presentation
      ラスベガス(米国)
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] HPT加工を施した準安定オーステナイト系ステンレス鋼の疲労き裂進展挙動に及ぼす水素の影響

    • Author(s)
      原口大佑,峯 洋二,高島和希,堀田善治
    • Organizer
      日本金属学会九州支部・日本鉄鋼協会九州支部・軽金属学会九州支部 平成25年度 合同学術講演大会
    • Place of Presentation
      熊本
    • Related Report
      2013 Research-status Report
  • [Presentation] 水素存在下で高圧ねじり加工を施した304型ステンレス鋼のマイクロ引張挙動

    • Author(s)
      古賀 薫,峯 洋二,高島和希,堀田善治
    • Organizer
      日本金属学会2013年秋期講演大会
    • Place of Presentation
      金沢
    • Related Report
      2013 Research-status Report
  • [Presentation] マイクロ引張試験による準安定オーステナイト鋼の水素脆化挙動の評価

    • Author(s)
      峯 洋二,古賀 薫,高島和希,堀田善治
    • Organizer
      日本金属学会2013年秋期講演大会
    • Place of Presentation
      金沢
    • Related Report
      2013 Research-status Report
  • [Presentation] 温間HPT加工による準安定オーステナイト系ステンレス鋼の結晶粒微細化

    • Author(s)
      原口大佑,峯 洋二,堀田善治
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京
    • Related Report
      2013 Research-status Report
  • [Presentation] 温間高圧ねじり加工により作製した超微細粒SUS304の引張変形挙動

    • Author(s)
      峯 洋二,井手口貴弘,高島和希,堀田善治,Jean-Marc Olive
    • Organizer
      日本金属学会2014年春期講演大会
    • Place of Presentation
      東京
    • Related Report
      2013 Research-status Report
  • [Remarks] http://www.msre.kumamoto-u.ac.jp/~sentan/

    • Related Report
      2015 Annual Research Report
  • [Remarks] http://www.msre.kumamoto-u.ac.jp/~sentan/

    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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