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Development of adhesive system of one-step self-etch adhesive with a high bond durability

Research Project

Project/Area Number 25462969
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Conservative dentistry
Research InstitutionNihon University

Principal Investigator

NISHIYAMA Norihiro  日本大学, 松戸歯学部, 教授 (90112953)

Co-Investigator(Kenkyū-buntansha) UCHIDA Ryoichiro  日本大学, 松戸歯学部, 助教 (10623960)
FUJITA Kou  日本大学, 松戸歯学部, 助教 (00147737)
AIDA Masahiro  日本大学, 松戸歯学部, 教授 (40147715)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2013: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywords接着 / ワンステップセルフエッチボンディング材 / MDP / MDPのカルシウム塩 / ワンステップボンディング材 / MDP / MDPのカルシウム塩 / NMR / XRD / 歯質接着 / 歯質接着性モノマー / カーブフィッティング / 酸性モノマーのカルシウム塩
Outline of Final Research Achievements

To determine the amount of calcium salt of MDP (MDP-Ca salt) developed during the adhesive application period to enamel or dentin, we designed a series of experimental MDP-based one-step adhesives with different amounts of MDP (EX adhesive). The effect of the concentration of MDP added in the EX adhesive on the types of the molecular species of MDP-Ca salts and their production amounts were examined. The enamel predominantly yielded mono-calcium salts of the MDP monomer and dimer, but in contrast, the dentin yielded di-calcium salts of the MDP monomer and dimer along with them. The amounts of MDP-Ca salt developed enamel and dentin increased with an increase in the amount of MDP added.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (3 results)

All 2016 2015

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Open Access: 2 results,  Acknowledgement Compliant: 2 results) Presentation (1 results)

  • [Journal Article] Quantitative evaluation of MDP-Ca salt and DCPD after application of MDP-based one-step self-etch adhesive on enamel and dentin2016

    • Author(s)
      Yoko Yokota, Kou Fujita (Nakajima), Ryoichiro Uchida, Etsuko Aida, Naoko Aoki (Tabei), Masahiro Aida, Norihiro Nishiyama
    • Journal Title

      Journal of Adhesive Dentistry

      Volume: なし

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Determination of molecular species of calcium salts of MDP produced through decalcification of enamel and dentin by MDP-based one-step adhesive2015

    • Author(s)
      Yokota Y, Nishiyama N.
    • Journal Title

      Dental Materials Journal

      Volume: 34 Issue: 2 Pages: 270-279

    • DOI

      10.4012/dmj.2014-260

    • NAID

      130005062401

    • ISSN
      0287-4547, 1881-1361
    • Related Report
      2015 Annual Research Report 2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] 31P NMR Analyses of Enamel and Dentin Reactants of MDP-based One-step Adhesive.2015

    • Author(s)
      Norihiro Nishiyama, Kou Fujita Nakajima, Yoko Yokota, Ryoichiro Uchida, Yasuhiro Tanimoto, and Hideki Teshima
    • Organizer
      93RD IADR GENERALSESSION
    • Place of Presentation
      BOSTON, MASS., USA
    • Year and Date
      2015-03-12
    • Related Report
      2014 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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