Towards the high-resolution neutron imaging under high pressure and temperature

• Project/Area Number: 25610158
• Research Category: Grant-in-Aid for Challenging Exploratory Research
• Allocation Type: Multi-year Fund
• Research Field: Petrology/Mineralogy/Economic geology
• Research Institution: Ehime University
• Principal Investigator: INOUE Toru 愛媛大学, 地球深部ダイナミクス研究センター, 教授 (00291500)
• Project Period (FY): 2013-04-01 – 2015-03-31
• Project Status: Completed (Fiscal Year 2014)
• Budget Amount: ¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000); Fiscal Year 2014: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000); Fiscal Year 2013: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
• Keywords: 中性子 / イメージング / 水素 / 水 / マグマ / 流体 / 含水相 / 高圧 / neutron / imaging / hydrogen / water / magma / fluid / hydrous phase / high pressure

Outline of Final Research Achievements

I have conducted the various kinds of test-experiments and the improvements to aim for the high-resolution imaging of our neutron camera installed by our Grant-in-Aid for Scientific Research on Innovative Areas in BL11 at J-PARC. By using the most optimized optical system, I have finally succeeded the hydrogen imaging of the hydrous sample within Pt capsule in high pressure cell assembly made by ZrO2 pressure medium, while it is impossible to see the hydrogen by X-ray. This result implies that the neutron imaging under high pressure and temperature will become possible under high pressure and temperature in nature future. We have already published the part of this research in an international journal (Hattori et al., 2015).

Research Products

• [Journal Article] In Situ Observation of Pressure-induced Crystallization from Amorphous Calcium Carbonate by Time-resolved X-ray Diffraction (2015)
  • Author(s): Maruyama K., Kagi H., Inoue T., Ohfuji H. and Yoshino T.
  • Journal Title: Chemistry Letters Volume: 44 Issue: 4 Pages: 434-436
  • DOI: 10.1246/cl.141062
  • NAID: 130005062153
  • ISSN: 0366-7022, 1348-0715
  • Peer Reviewed / Open Access / Acknowledgement Compliant
• [Journal Article] Design and Performance of High-Pressure PLANET Beamline at Pulsed Neutron Source at J-PARC (2015)
  • Author(s): Hattori, T., A. Sano-Furukawa, H. Arima, K. Komatsu, A. Yamada, Y. Inamura, T. Nakatani, Y. Seto, T. Nagai, W. Utsumi, T. Iitaka, H. Kagi, Y. Katayama, T. Inoue, T. Otomo, K. Suzuya, T. Kamiyama, M. Arai T. Yagi
  • Journal Title: Nuclear Instruments and Methods in Physics Research Section A Volume: 780 Pages: 55-67
  • DOI: 10.1016/j.nima.2015.01.059
  • Peer Reviewed / Open Access / Acknowledgement Compliant
• [Journal Article] A Possible New Al-bearing hydrous Mg-silicate (23 Å; phase) in the deep upper mantle (2015)
  • Author(s): Cai, N., T. Inoue, K. Fujino, H. Ohfuji and H. Yurimoto
  • Journal Title: Am. Mineral. Volume: -
  • Peer Reviewed / Acknowledgement Compliant
• [Journal Article] Equation of state and phase transition of antigorite under high pressure and high temperature (2014)
  • Author(s): Yang, C., T. Inoue, A. Yamada, T. Kikegawa, J. Ando
  • Journal Title: Phys. Earth Planet. Inter. Volume: 228 Pages: 56-62
  • DOI: 10.1016/j.pepi.2013.07.008
  • Peer Reviewed / Open Access / Acknowledgement Compliant
• [Journal Article] B-site deficiencies in A-site-ordered perovskite LaCu3Pt3.75O12 (2013)
  • Author(s): Ochi,M., Yamada, I., Ohgushi, K., Kusano, Y., Mizumaki, Takahashi, R., Nishiyama, N., Inoue, T., Irifune, T.
  • Journal Title: Inorg. Chem. Volume: 52 Issue: 7 Pages: 3985-3989
  • DOI: 10.1021/ic302809v
  • Peer Reviewed
• [Journal Article] Synthesis of tungsten trioxide nanoparticles by microwave plasma in liquid and analysis of physical properties (2013)
  • Author(s): Hattori, Y., S. Nomura, S. Mukasa, H. Toyota, T. Inoue, T. Kasahara
  • Journal Title: J. Alloys and Compounds, Volume: 560 Pages: 105-110
  • DOI: 10.1016/j.jallcom.2013.01.137
  • Peer Reviewed
• [Journal Article] Synthesis of tungsten oxide, silver, and gold nanoparticles by radio frequency plasma in water (2013)
  • Author(s): Hattori, Y., Nomura, S., Mukasa, S., Toyota, H., Inoue, T., and Usui, T.
  • Journal Title: J. Alloys and Compdounds Volume: 578 Pages: 148-152
  • DOI: 10.1016/j.jallcom.2013.05.032
  • Peer Reviewed
• [Journal Article] NMR study of successive magnetic transitions in the A-site ordered perovskite LaMn3Cr4O12 (2013)
  • Author(s): Kawasaki, Y., Takase, S., Kishimoto, Y., Ohno, T., Yamada, I., Shiro, K., Takahashi, R., Ohgushi, K., Nishiyama, N., Inoue, T. and Irifune, T.
  • Journal Title: J. Korean Phys. Soc. Volume: 63 Issue: 3 Pages: 640-643
  • DOI: 10.3938/jkps.63.640
  • Peer Reviewed
• [Journal Article] Suppression of Intersite Charge Transfer in Charge-Disproportionated Perovskite YCu3Fe4O12 (2013)
  • Author(s): Etani, H., Yamada, I., Ohgushi, K., Hayashi, N., Kusano, Y., Mizumaki, M., Kim, J., Tsuji, N., Takahashi, R., Nishiyama, N., Inoue, T., Irifune, T., Takano, M.
  • Journal Title: Journal of the American Chemical Society Volume: 52 Issue: 16 Pages: 3985-3989
  • DOI: 10.1021/ja312015j
  • Peer Reviewed
• [Journal Article] Control of Bond-Strain-Induced Electronic Phase Transitions in Iron Perovskites (2013)
  • Author(s): Ikuya Yamada, Hidenobu Etani, Kazuki Tsuchida, Shohei Marukawa, Naoaki Hayashi, Takateru Kawakami, Masaichiro Mizumaki, Kenya Ohgushi, Yoshihiro Kusano, Jungeun Kim, Naruki Tsuji, Ryoji Takahashi, Norimasa Nishiyama, Toru Inoue, Tetsuo Irifune, and Mikio Takano
  • Journal Title: Inorganic Chemistry Volume: 52 Issue: 23 Pages: 13751-13761
  • DOI: 10.1021/ic402344m
  • Peer Reviewed
• [Presentation] In situ X-ray observation of dehydration and EoS of chlorite under high pressure and temperature (2014)
  • Author(s): Inoue, T., Suenami, H. and Kikegawa, T.
  • Organizer: 2014 AGU Fall Meeting
  • Place of Presentation: San Francisco, USA
  • Year and Date: 2014-12-15 – 2014-12-19
• [Presentation] New Al-bearing hydrous Mg-silicate in the deep upper mantle (2014)
  • Author(s): Cai, N., Inoue, T., Fujino, K., Ohfuji, H. and Yurimoto, H.
  • Organizer: 2014 AGU Fall Meeting
  • Place of Presentation: San Francisco, USA
  • Year and Date: 2014-12-15 – 2014-12-19
• [Presentation] 含水bridgmaniteの合成とキャラクタリゼーション (2014)
  • Author(s): 井上徹，矢吹智実，柿澤翔，藤野清志，圦本尚義，栗林貴弘，長瀬敬郎
  • Organizer: 第55回高圧討論会
  • Place of Presentation: 徳島大学（徳島市、徳島県）
  • Year and Date: 2014-11-22
• [Presentation] ラジオグラフィーによるケイ酸塩-鉄分離過程のその場観察 (2014)
  • Author(s): 八木健彦，後藤弘匡，飯塚理子，鈴木昭夫，井上徹
  • Organizer: 第55回高圧討論会
  • Place of Presentation: 徳島大学（徳島市、徳島県）
  • Year and Date: 2014-11-22
• [Presentation] AlとHに富むMg-bridgmaniteの合成とキャラクタリゼーション (2014)
  • Author(s): 井上徹，矢吹智実，柿澤翔，藤野清志，圦本尚義，栗林貴弘，長瀬敏郎
  • Organizer: 日本鉱物科学会2014年年会・総会
  • Place of Presentation: 熊本大学（熊本市、熊本県）
  • Year and Date: 2014-09-18
• [Presentation] 緑泥石の脱水分解反応境界とその状態方程式 (2014)
  • Author(s): 井上徹，末次秀規，柿澤翔，亀卦川卓美
  • Organizer: 日本鉱物科学会2014年年会・総会
  • Place of Presentation: 熊本大学（徳島市、徳島県）
  • Year and Date: 2014-09-18
• [Presentation] 非晶質炭酸カルシウムの圧力誘起結晶化その場観察 (2014)
  • Author(s): 丸山浩司，鍵裕之，井上徹，吉野徹
  • Organizer: 日本鉱物科学会2014年年会・総会
  • Place of Presentation: 熊本大学 （熊本市、熊本県）
  • Year and Date: 2014-09-17
• [Presentation] Al incorporation in dense hydrous magnesium silicates (2014)
  • Author(s): Inoue, T., Hayashi, K. and Yurimoto, H.
  • Organizer: IMA 2014
  • Place of Presentation: South Africa, Santon
  • Year and Date: 2014-09-03
• [Presentation] Coupled substitution of H+ and Al3+ into deep mantle minerals (2014)
  • Author(s): Inoue, T., Cai, N., Hayashi, K. and Yurimoto, H.
  • Organizer: Asia Oceania Geosciences Society
  • Place of Presentation: Sapporo, Hokkaido
  • Year and Date: 2014-08-01
• [Presentation] 地球内部の「水」を見るツール～超高圧中性子ビームラインPLANET～ (2014)
  • Author(s): 服部高典，佐野亜沙美，有馬寛，井上徹，鍵裕之，八木健彦
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: パシフィコ横浜（横浜市、神奈川県）
  • Year and Date: 2014-05-02
• [Presentation] J-PARC高圧中性子ビームライン(PLANET)の地球惑星科学への応用 (2014)
  • Author(s): 鍵裕之，飯塚理子，小松一生，八木健彦，永井隆哉，井上徹，佐野亜沙美，服部高典
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: パシフィコ横浜（横浜市、神奈川県）
  • Year and Date: 2014-05-02
• [Presentation] Aluminum incorporation into phase A - a new hydrous silicate in the deep upper mantle (2014)
  • Author(s): Cai, N., Inoue, T., Fujino, K., Ohfuji, H., Kuribayashi, T. and Yurimoto, H.
  • Organizer: Japan Geoscience Union Meeting 2014
  • Place of Presentation: Pacifico Yokohama (Yokohama, Kanagawa)
  • Year and Date: 2014-04-29
• [Presentation] Dehydration boundary and the EoS of chlorite under high pressure and temperature (2014)
  • Author(s): Suenami, H., Inoue, T.*, Kakizawa, S. and Kikegawa, T.
  • Organizer: Japan Geoscience Union Meeting 2014
  • Place of Presentation: Pacifico Yokohama (Yokohama, Kanagawa)
  • Year and Date: 2014-04-28
  • Invited
• [Presentation] 熱力学的手法によるMg2SiO4のポストスピネル相転移境界の再決定
  • Author(s): 糀谷浩，井上徹，赤荻正樹
  • Organizer: 日本地球惑星科学連合2013
  • Place of Presentation: 千葉
• [Presentation] J-PARC, PLANETにおける無水及び含水アルバイトガラスの高圧下中性子回折実験と中性子イメージング予備実験
  • Author(s): 井上徹，山田明寛，浦川啓，鈴木昭夫，有馬寛，寺崎英紀，大高理，服部高典，佐野亜沙美
  • Organizer: 日本地球惑星科学連合2013
  • Place of Presentation: 千葉
• [Presentation] 超高圧中性子回折装置PLANETの性能と現状
  • Author(s): 服部高典，佐野亜沙美，有馬寛，小松一生，山田明寛，永井隆哉，片山芳則，井上徹，内海渉，鍵裕之，八木健彦
  • Organizer: 日本地球惑星科学連合2013
  • Place of Presentation: 千葉
• [Presentation] X線その場観察を用いた高圧下における緑泥石の脱水分解反応
  • Author(s): 末次秀規，井上徹
  • Organizer: 日本地球惑星科学連合2013
  • Place of Presentation: 千葉
• [Presentation] 上部マントル条件下におけるMgCO3+SiO2=MgSiO3+CO2反応境界の決定
  • Author(s): 柿澤翔，井上徹，山田明寛，末次秀規
  • Organizer: 日本地球惑星科学連合2013
  • Place of Presentation: 千葉
• [Presentation] Re-determination of high-temperature heat capacity and thermal expansivity of Mg2SiO4 ringwoodite: Implication for clapeyron slope of post-spinel transition
  • Author(s): Kojitani, H., Ohhata, M., Shimada, H., Inoue, T., and Akaogi, M.
  • Organizer: Asia Oceania Geosciences Society
  • Place of Presentation: Brisbane, Australia
  • Invited
• [Presentation] 熱力学的手法によるMg2SiO4のポストスピネル相転移境界の再決定
  • Author(s): 糀谷 浩，井上徹，赤荻正樹
  • Organizer: 日本鉱物科学会2013年年会・総会
  • Place of Presentation: 筑波大学
• [Presentation] 下部マントル条件下で安定なAlに富む高圧含水鉱物
  • Author(s): 井上徹，林晃平，圦本 尚義
  • Organizer: 日本鉱物科学会2013年年会・総会
  • Place of Presentation: 筑波大学
• [Presentation] 下部マントル最上部におけるAlに富む高圧含水鉱物
  • Author(s): 井上徹，林晃平，圦本尚義
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] 高温高圧下におけるMgCO3 + SiO2系の反応と溶融
  • Author(s): 柿澤翔，井上徹，末次秀規，CAI Nao，山田明寛，亀卦川卓美
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] Thermal equation of state of lawsonite under high pressure and high temperature
  • Author(s): Nao CAI, Toru INOUE, Takumi KIKEGAWA
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] 高圧下におけるNaAlSi3O8ガラスの局所構造変化
  • Author(s): 山田明寛，井上徹，亀卦川卓美
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] ポストスピネル相境界から制約されるMg2SiO4リングウッダイト中の陽イオン無秩序
  • Author(s): 糀谷浩，井上徹，赤荻正樹
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] 室温圧縮下の含水石英ガラスのX線回折実験
  • Author(s): 浦川啓，井上徹，亀卦川卓美
  • Organizer: 第54回高圧討論会
  • Place of Presentation: 新潟コンベンションセンター
• [Presentation] Al-bearing dense hydrous minerals under mantle transition zone and uppermost lower mantle conditions
  • Author(s): Inoue, T., Hayashi, K. and Yurimoto, H.
  • Organizer: AGU Fall Meeting 2013
  • Place of Presentation: San Francisco, USA
• [Presentation] New high-pressure neutron beamline PLANET at J-PARC
  • Author(s): Hattori, T., Sano-Furukawa, A., Arima, H., Inamura, Y., Nahgai, T., Katayama, Y., Inoue, T., Kagi, H. and Yagi, T.
  • Organizer: International conference on neutron scattering (ICNS2013)
  • Place of Presentation: Edinburgh, UK
• [Presentation] New Tool for Investigating High-Pressure and High-Temperature States of Matter at Intense Pulsed Neutron Source J-PARC
  • Author(s): Hattori, T., Sano-Furukawa, A., Arima, H., Inamura, Y., Yamada, A., Komatsu, K., Nahgai, T., Katayama, Y., Inoue, T., Kagi, H. and Yagi, T.
  • Organizer: THERMEC 2013 (the 8th international conference on advanced materials)
  • Place of Presentation: Las Vegas, USA
• [Presentation] 地球内部の「水」を見るツール～超高圧中性子ビームラインPLANET～
  • Author(s): 服部高典，佐野亜沙美，有馬寛，井上徹，鍵裕之，八木健彦
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: 横浜
• [Presentation] J-PARC高圧中性子ビームライン(PLANET)の地球惑星科学への応用
  • Author(s): 鍵裕之，飯塚理子，小松一生，八木健彦，永井隆哉，井上徹，佐野亜沙美，服部高典
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: 横浜
• [Presentation] 沈み込む堆積岩層中の含水相topaz-OHの高温高圧下における状態方程式の決定
  • Author(s): 新里 美月，井上 徹，蔡 閙，末次秀規，亀卦川卓美
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: 横浜
• [Presentation] Aluminum incorporation into phase A - a new hydrous silicate in the deep upper mantle
  • Author(s): Cai, N., Inoue, T., Fujino, K., Ohfuji, H., Kuribayashi, T., H. Yurimoto
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: 横浜
• [Presentation] Dehydration boundary and the EoS of chlorite under high pressure and temperature
  • Author(s): Suenami, H., Inoue, T., Kakizawa, S., Kikegawa, T.
  • Organizer: 日本地球惑星科学連合2014
  • Place of Presentation: 横浜
  • Invited
• [Book] 地球ダイナミクス：山本明彦編 (2014)
  • Author(s): 井上徹
  • Total Pages: 229
  • Publisher: 朝倉書店
• [Book] 地球内部の物質科学. In 地球ダイナミクス(山本明彦編） (2014)
  • Author(s): 井上徹
  • Publisher: 朝倉書店
• [Remarks] 愛媛大学地球深部ダイナミクス研究センター
  • URL: http://www.grc.ehime-u.ac.jp/
• [Remarks] 愛媛大学地球深部ダイナミクス研究センター
  • URL: http://www.ehime-u.ac.jp/~grc/