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Strength of Low-dimensional Materials in Detrimental Environment

Research Project

Project/Area Number 25630014
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Research InstitutionKobe University

Principal Investigator

Nakai Yoshikazu  神戸大学, 工学(系)研究科(研究院), 教授 (90155656)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2014: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2013: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords薄膜 / ナノ結晶 / 環境強度 / 疲労 / ナノ結晶材料 / 疲労強度 / 疲労き裂伝ぱ / Hall-Petchの関係
Outline of Final Research Achievements

In the present project, the effect of grain size on the mechanical strength of electrodeposited nickel thin film was studied. By EBSD analysis, grain boundaries in the material were found to be large twist angle boundaries. In the measurement of grain size by EBSD, the step size should be less than tenth part of grain size.
Either relation between 0.2% proof strength, tensile strength, or fatigue limit and grain size of electro deposited nickel thin film is different from that of bulk nickel plate with conventional grain size, and this difference is large for smaller grain size thin film. This is considered to come from the fact that grain boundary has area with volume, not a face with no thickness. For the consideration of Hall-Petch relationship, mean free path of dislocation should be considered, that is actual grain size minus grain boundary area size.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (51 results)

All 2016 2015 2014 2013 Other

All Journal Article (10 results) (of which Peer Reviewed: 10 results,  Open Access: 7 results,  Acknowledgement Compliant: 3 results) Presentation (36 results) (of which Int'l Joint Research: 3 results,  Invited: 1 results) Book (3 results) Remarks (2 results)

  • [Journal Article] 4D evaluation of grain shape and fatigue damage of individual grains in polycrystalline alloys by diffraction contrast tomography using ultrabright synchrotron radiation2016

    • Author(s)
      D. Shiozawa, Y. Nakai, R. Miura, N. Masada, S. Matsuda, R. Nakao
    • Journal Title

      Int. J. of Fatigue

      Volume: 64 Pages: 668-674

    • DOI

      10.1016/j.ijfatigue.2015.07.014

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] In situ Observation of Rolling Contact Fatigue Cracks by Laminography Using Ultra-bright Synchrotron Radiation2015

    • Author(s)
      Y. Nakai, D. Shiozawa, S. Kikuchi, K. Sato, T. Obama, T. Makino, Y. Neishi
    • Journal Title

      Frattura ed Integrita Strutturale

      Volume: 34 Issue: 34 Pages: 267-275

    • DOI

      10.3221/igf-esis.34.28

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Evaluation of near-threshold fatigue crack propagation in Ti-6Al-4V alloy with harmonic structure created by mechanical milling and spark plasma sintering2015

    • Author(s)
      S. Kikuchi, T. Imai, H. Kubozono, Y. Nakai, A. Ueno and K. Ameyama
    • Journal Title

      Fracture and Structural Integrity

      Volume: 34 Issue: 34 Pages: 261-270

    • DOI

      10.3221/igf-esis.34.30

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Evaluation of Fatigue Damage by Diffraction Contrast Tomography Using Synchrotron Radiation2014

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Ryotaro Miura, and Shota Matsuda
    • Journal Title

      Materials Science Forum

      Volume: 783-786 Pages: 2359-2364

    • DOI

      10.4028/www.scientific.net/msf.783-786.2359

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Observation of rolling contact fatigue cracks by laminography using ultra-bright synchrotron radiation2014

    • Author(s)
      D. Shiozawa, T. Makino, Y. Neishi, and Y. Nakai
    • Journal Title

      Procedia Materials Science

      Volume: 3 Pages: 154-164

    • DOI

      10.1016/j.mspro.2014.06.030

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Evaluation of Rolling Contact Fatigue Crack Path in High Strength Steel with Artificial Defects2014

    • Author(s)
      T.Makino, Y.Neishi, D.Shiozawa, Y.Fukuda, K.Kajiwara and Y.Nakai
    • Journal Title

      International Journal of Fatigue

      Volume: 68 Pages: 168-177

    • DOI

      10.1016/j.ijfatigue.2014.05.006

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] 4D analysis of pit growth and crack initiation in aluminum alloy under corrosion fatigue using synchrotron radiation micro CT imaging2014

    • Author(s)
      塩澤大輝,岡田宗大,中井善一
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 64 Issue: 11 Pages: 564-569

    • DOI

      10.2464/jilm.64.564

    • NAID

      130004775045

    • ISSN
      0451-5994, 1880-8018
    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Evaluation of Fatigue Damage by Diffraction Contrast Imaging using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Ryotaro Miura, and Shota Matsuda
    • Journal Title

      Advanced Materials Research

      Volume: 891-892 Pages: 600-605

    • DOI

      10.4028/www.scientific.net/amr.891-892.600

    • Related Report
      2013 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Fatigue of ultra-fine grained α-brass2014

    • Author(s)
      Yoshikazu Nakai, Takuto Imanaka and Daiki Shiozawa
    • Journal Title

      Advanced Materials Research

      Volume: 891-892 Pages: 1125-1130

    • DOI

      10.4028/www.scientific.net/amr.891-892.1125

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Observation of 3D shape and propagation mode transition of fatigue cracks in Ti-6Al-4V under cyclic torsion using CT imaging with ultra-bright synchrotron radiation2013

    • Author(s)
      Daiki Shiozawa, Y. Nakai, T. Murakami and H. Nosho
    • Journal Title

      International Journal of Fatigue

      Volume: (in press) Pages: 158-165

    • DOI

      10.1016/j.ijfatigue.2013.02.018

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] ナノ結晶電着ニッケル薄膜の微視組織および機械的特性に及ぼす光沢剤添加の影響2016

    • Author(s)
      榎本 寛之,竹重 亮 汰,中塚 悠太,中井 善一,菊池 将一
    • Organizer
      日本機械学会関西支部 第91期定時総会講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-11
    • Related Report
      2015 Annual Research Report
  • [Presentation] 調和組織を有する工業用純チタンの下限界近傍における疲労き裂伝ぱ特性2016

    • Author(s)
      森徹也,久 保薗宏樹,今井貴文,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] AFM によるマグネシウム合金 AZ31 の疲労き裂発生挙動の観察2016

    • Author(s)
      坂昌彦,岡江秀樹, 菊池将一,中井善一
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] TiNi 超弾性合金の疲労寿命に及ぼす水素環境の影響2016

    • Author(s)
      松本高明,中井善一,田中拓, 足立瞳,池山隆宏
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] ナノ結晶電着ニッケル薄膜の作製とその疲労き裂伝ぱ特性評価2016

    • Author(s)
      竹重亮汰,榎本寛之, 中塚悠太,中井善一,菊池将一
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] ナノ結晶電着ニッケル薄膜の疲労特性に及ぼす光沢剤添加の影響2016

    • Author(s)
      中塚悠太,榎本寛之, 竹重亮汰,中井善一,菊池将一
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高輝度放射光によるオーステナイト系ステンレス鋼の疲労過程におけるミスオリエンテーション変 化の観察2016

    • Author(s)
      野中謙次,中尾亮太,淺川直也,塩澤大輝,菊池将一,中井善一
    • Organizer
      平成27年度関西学生会学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高輝度放射光によるステンレス鋼の疲労におけるミスオリエンテーション評価2015

    • Author(s)
      中尾亮太, 淺川直也, 松田翔太, 塩澤大輝, 菊池将一, 中井善一
    • Organizer
      日本機械学会 M&M2015材料力学カンファレンス
    • Place of Presentation
      慶應義塾大学(神奈川県横浜市)
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] 水素環境下における形状記憶合金細線の疲労寿命2015

    • Author(s)
      足立瞳, 田中拓, 河野久晃, 中井善一
    • Organizer
      日本機械学会 M&M2015材料力学カンファレンス
    • Place of Presentation
      慶應義塾大学(神奈川県横浜市)
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] 調和組織を有するTi-6Al-4V合金の疲労き裂伝ぱ特性に及ぼす応力比の影響2015

    • Author(s)
      今井貴文, 久保薗宏樹, 菊池将一, 中井善一, 上野明, 飴山惠
    • Organizer
      日本機械学会 M&M2015材料力学カンファレンス
    • Place of Presentation
      慶應義塾大学(神奈川県横浜市)
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] Evaluation of High Cycle Fatigue Damage for Austenitic Stainless Steel by Diffraction Contrast Tomography Using Ultra-bright Synchrotron Radiation2015

    • Author(s)
      Naoya Asakawa, Daiki Shiozawa, Syoichi Kikuchi, Shota Matsuda, Yoshikazu Nakai
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2015
    • Place of Presentation
      LOISIR HOTEL(愛知県豊橋市)
    • Year and Date
      2015-10-04
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effects of Harmonic Structure and Grain Size on Fatigue Crack Propagation of Ti-6Al-4V Alloy2015

    • Author(s)
      Shoichi Kikuch, Takafumi Imai, Hiroki Kubozono, Yoshikazu Nakai, Mie Ota, Akira Ueno, Kei Ameyamaazu
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2015 (ATEM’15)
    • Place of Presentation
      LOISIR HOTEL(愛知県豊橋市)
    • Year and Date
      2015-10-04
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Evaluation of near-threshold fatigue crack propagation in Ti-6Al-4V alloy with harmonic structure created by mechanical milling and spark plasma sintering2015

    • Author(s)
      Shoichi Kikuchi, Takafumi Imai, Hiroki Kubozono, Yoshikazu Nakai, Akira Ueno, Kei Ameyama
    • Organizer
      The 5th International Conference on CRACK PATHS (CP 2015)
    • Place of Presentation
      Ferrara, Italy
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Ti-6Al-4V合金の疲労き裂伝ぱ特性に及ぼす調和組織の影響2015

    • Author(s)
      久保薗宏樹,今井貴文,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本材料学会第64期学術講演会
    • Place of Presentation
      山形大学(山形県米沢市)
    • Year and Date
      2015-05-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高輝度放射光を用いた回折コントラストトモグラフィによるSUS316L鋼の高サイクル疲労損傷の評価2015

    • Author(s)
      淺川直也,松田翔太,中尾亮太,塩澤大輝,菊池将一,中井善一
    • Organizer
      日本材料学会第64期学術講演会
    • Place of Presentation
      山形大学(山形県米沢市)
    • Year and Date
      2015-05-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] ナノ結晶電着薄膜平滑材の疲労強度に関する研究2015

    • Author(s)
      堤 湧貴,榎本 寛之,前川 将悟,中井 善一
    • Organizer
      日本機械学会関西支部 第90 期定時総会講演会
    • Place of Presentation
      京都大学,京都市
    • Year and Date
      2015-03-16 – 2015-03-17
    • Related Report
      2014 Research-status Report
  • [Presentation] TiNi 形状記憶合金細線の水素環境下における疲労寿命に及ぼす応力波形の影響2015

    • Author(s)
      池山隆宏,田中拓,河野久晃,足立瞳,中井善一
    • Organizer
      日本機械学会関西学生会平成26 年度学生員卒業研究発表講演会
    • Place of Presentation
      京都大学,京都市
    • Year and Date
      2015-03-14
    • Related Report
      2014 Research-status Report
  • [Presentation] ナノ結晶ニッケル電着薄膜の作成とその強度評価2015

    • Author(s)
      前川将悟,中井善一,堤湧貴,榎本寛之
    • Organizer
      日本機械学会関西学生会平成26 年度学生員卒業研究発表講演会
    • Place of Presentation
      京都大学,京都市
    • Year and Date
      2015-03-14
    • Related Report
      2014 Research-status Report
  • [Presentation] 調和組織を有するチタン合金の疲労き裂伝ぱに関する研究2015

    • Author(s)
      久保薗宏樹,今井貴文,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本機械学会関西学生会平成26 年度学生員卒業研究発表講演会
    • Place of Presentation
      京都大学,京都市
    • Year and Date
      2015-03-14
    • Related Report
      2014 Research-status Report
  • [Presentation] Evaluation of Fatigue Damage in Polycrystalline Alloys by Diffraction Contrast Tomography using Ultra-bright Synchrotron Radiation2014

    • Author(s)
      . Shiozawa, Y. Nakai, R. Miura, and S. Matsuda
    • Organizer
      3rd Japan-China Joint Symposium on Fatigue of Engineering Materials and Structures
    • Place of Presentation
      高山市民文化会館,高山市
    • Year and Date
      2014-11-06 – 2014-11-08
    • Related Report
      2014 Research-status Report
  • [Presentation] 4D evaluation of grain shape and fatigue damage of individual grain in polycrystalline alloys by diffraction contrast tomography using ultra-bright synchrotron radiation2014

    • Author(s)
      D. Shiozawa, Y. Nakai, R. Miura, S. Matsuda
    • Organizer
      International Conference on Fatigue Damage of Structural Materials X
    • Place of Presentation
      Hyannis Conference Center, Hyannis, MA, USA
    • Year and Date
      2014-09-21 – 2014-09-26
    • Related Report
      2014 Research-status Report
  • [Presentation] 形状記憶合金細線の疲労寿命に及ぼす環境の影響2014

    • Author(s)
      足立 瞳,田中 拓,河野久晃,中井善一
    • Organizer
      日本機械学会材料力学カンファレンス(M&M2014)
    • Place of Presentation
      福島大学,福島市
    • Year and Date
      2014-07-19 – 2014-07-21
    • Related Report
      2014 Research-status Report
  • [Presentation] Observation of rolling contact fatigue cracks by laminography using ultra-bright synchrotron radiation2014

    • Author(s)
      D. Shiozawa, T. Makino, Y. Neishi, and Y. Nakai
    • Organizer
      20th European Conference on Fracture (ECF20)
    • Place of Presentation
      Norwegian University of Science and Technology, Trondheim, Norway
    • Year and Date
      2014-06-30 – 2014-07-04
    • Related Report
      2014 Research-status Report
  • [Presentation] 放射光回折コントラストトモグラフィによる低サイクル疲労の損傷評価2014

    • Author(s)
      中尾亮太,塩澤大輝,中井善一,政田尚也,松田翔太
    • Organizer
      日本材料学会第63期学術講演会
    • Place of Presentation
      福岡大学,福岡市
    • Year and Date
      2014-05-17 – 2014-05-18
    • Related Report
      2014 Research-status Report
  • [Presentation] ナノ結晶ニッケル電着薄膜の作成とその強度評価2014

    • Author(s)
      榎本寛之,中井善一,堤湧貴
    • Organizer
      日本機械学会関西学生会平成25年度学生員卒業研究発表講演会
    • Place of Presentation
      堺
    • Related Report
      2013 Research-status Report
  • [Presentation] TiNi 形状記憶合金細線の疲労寿命に及ぼす水素濃度の影響2014

    • Author(s)
      足立瞳,田中拓,河野久晃,中井善一
    • Organizer
      日本機械学会関西学生会平成25年度学生員卒業研究発表講演会
    • Place of Presentation
      堺
    • Related Report
      2013 Research-status Report
  • [Presentation] バルク金属ガラスの腐食環境下での下限界近傍における疲労き裂伝ぱに関する研究2014

    • Author(s)
      上野 晃平,中井 善一,今井 貴文
    • Organizer
      日本機械学会関西支部 第89期定時総会講演会
    • Place of Presentation
      堺
    • Related Report
      2013 Research-status Report
  • [Presentation] Threshold of Crack Propagation of Zr-based Bulk Metallic Glass in Sodium Chloride Solution2013

    • Author(s)
      Yoshikazu NAKAI, Toyohiko KOTAMA, Bo HE, and Kohei UENO
    • Organizer
      EUROMAT 2013
    • Place of Presentation
      セビリヤ
    • Related Report
      2013 Research-status Report
  • [Presentation] α黄銅超微細結晶粒材の疲労強度2013

    • Author(s)
      中井善一,今中拓人,塩澤大輝
    • Organizer
      M&M2013
    • Place of Presentation
      岐阜
    • Related Report
      2013 Research-status Report
  • [Presentation] 高輝度放射光を用いた回折コントラストトモグラフィによる疲労損傷評価に関する検討2013

    • Author(s)
      松田翔太,政田尚也,塩澤大輝,中井善一,三浦亮太郎
    • Organizer
      M&M2013
    • Place of Presentation
      岐阜
    • Related Report
      2013 Research-status Report
  • [Presentation] 水素環境下における繰返し応力がTiNi形状記憶合金の寿命に及ぼす影響2013

    • Author(s)
      河野久晃,田中拓,中井善一,西本匡志
    • Organizer
      M&M2013
    • Place of Presentation
      岐阜
    • Related Report
      2013 Research-status Report
  • [Presentation] 放射光μCT 及び小型転動疲労試験機を用いた転動疲労き裂進展過程の観察2013

    • Author(s)
      佐藤一矢,塩澤大輝,根石豊,牧野泰三,中井善一,岡田宗大,
    • Organizer
      M&M2013
    • Place of Presentation
      岐阜
    • Related Report
      2013 Research-status Report
  • [Presentation] Zr 基バルク金属ガラスの腐食環境中における下限界近傍の疲労き裂伝ぱ2013

    • Author(s)
      中井善一,小山豊彦, 何波, 上野晃平
    • Organizer
      日本材料学会第16回破壊力学シンポジウム
    • Place of Presentation
      阿蘇ファームランド
    • Related Report
      2013 Research-status Report
  • [Presentation] 高輝度放射光を用いた回折コントラストイメージによるき裂発生過程の結晶組織観察2013

    • Author(s)
      政田尚也, 松田翔太, 塩澤大輝, 中井善一
    • Organizer
      日本材料学会第16回破壊力学シンポジウム
    • Place of Presentation
      阿蘇ファームランド
    • Related Report
      2013 Research-status Report
  • [Presentation] 放射光μCTイメージングによる腐食疲労におけるピットの成長及びき裂発生過程の4D解析2013

    • Author(s)
      岡田宗大, 塩澤大輝, 中井善一
    • Organizer
      日本材料学会第16回破壊力学シンポジウム
    • Place of Presentation
      阿蘇ファームランド
    • Related Report
      2013 Research-status Report
  • [Presentation] Evaluation of Fatigue Damage by Diffraction Contrast Imaging using Ultra-bright Synchrotron Radiation2013

    • Author(s)
      Daiki Shiozawa, Yoshikazu Nakai, Ryotaro Miura, and Shota Matsuda
    • Organizer
      THERMEC 2013
    • Place of Presentation
      ラスベガス
    • Related Report
      2013 Research-status Report
    • Invited
  • [Book] 初心者のための疲労用語の解説2015

    • Author(s)
      曙紘之,塩澤大輝,柿内利文,牧野泰三,伊藤隆基,上野明,植松美彦,小川武史,小熊博幸,杵渕雅男,久保田祐信,黒島義人,小山敦弘,菅田淳,高橋学,田中和人,中井善一,中村孝,西川出,堀川教世,政木清孝
    • Publisher
      公益社団法人 日本材料学会 疲労部門委員会 疲労用語集小委員会
    • Related Report
      2015 Annual Research Report
  • [Book] 破壊力学2014

    • Author(s)
      中井善一,久保司郎
    • Total Pages
      184
    • Publisher
      朝倉書店
    • Related Report
      2014 Research-status Report
  • [Book] 材料力学2013

    • Author(s)
      中井善一,三村耕司,阪上隆英,多田直哉,岩本剛,田中拓
    • Total Pages
      204
    • Publisher
      朝倉書店
    • Related Report
      2013 Research-status Report
  • [Remarks] 破壊制御学研究室

    • URL

      http://www.research.kobe-u.ac.jp/eng-fracture/

    • Related Report
      2015 Annual Research Report 2014 Research-status Report
  • [Remarks] 破壊制御学研究室

    • URL

      http://www.research.kobe-u.ac.jp/eng-fracture/

    • Related Report
      2013 Research-status Report

URL: 

Published: 2014-07-25   Modified: 2019-07-29  

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