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Development of highly efficient and high precision figuring and finishing technique applying anodic oxidation for mold material made of SiC

Research Project

Project/Area Number 25630026
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Production engineering/Processing studies
Research InstitutionOsaka University

Principal Investigator

YAMAMURA Kazuya  大阪大学, 工学(系)研究科(研究院), 准教授 (60240074)

Project Period (FY) 2013-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2014: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2013: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords陽極酸化 / 反応焼結SiC / 金型材料 / 形状修正 / 数値制御加工 / 金型 / SiC / 研磨 / 非球面
Outline of Final Research Achievements

We proposed application of electrochemical mechanical polishing (ECMP), which is using a slurry as the electrolyte, for fabricating an ultraprecise glass lens mold made of reaction sintered silicon carbide (RS-SiC) material. RS-SiC is composed from SiC phase and Si phase, and SiC is easily oxidized anodically whereas Si is seldom oxidized. We have experimentally obtained optimal conditions in which oxidation rate of SiC and polishing rate of Si are same. By applying numerically controlled ECMP using optimal conditions for planarization of RS-SiC substrate, flatness and surface roughness are decreased from 808 nm to 184 nm and from 2.65 nm rms to 0.98 nm rms, respectively. Obtained result indicates that developed technique enables us to realize figure correction and smoothing of RS-SiC substrate simultaneously.

Report

(3 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • Research Products

    (17 results)

All 2015 2014 Other

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 3 results) Presentation (14 results)

  • [Journal Article] Figuring and finishing of reaction-sintered SiC by anodic oxidation assisted process2015

    • Author(s)
      N. Shimozono, X. Shen, H. Deng, K. Endo, K. Yamamura
    • Journal Title

      Key Eng. Mater.

      Volume: 625 Pages: 570-575

    • DOI

      10.4028/www.scientific.net/kem.625.570

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Electro-chemical mechanical polishing of single-crystal SiC using CeO2 slurry2015

    • Author(s)
      Hui Deng, Kenji Hosoya, Yusuke Imanishi, Katsuyoshi Endo, Kazuya Yamamura
    • Journal Title

      Electrochemistry Communications

      Volume: 52 Pages: 5-8

    • DOI

      10.1016/j.elecom.2015.01.002

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Preliminary study on highly efficient polishing of 4H-SiC by utilization of anodic oxidation2014

    • Author(s)
      K. Yamamura, K. Hosoya, Y. Imanishi, H. Deng, K. Endo
    • Journal Title

      Adv. Mater. Res.

      Volume: 1017 Pages: 509-514

    • DOI

      10.4028/www.scientific.net/amr.1017.509

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] 電気化学機械研磨による金型用SiC材の高能率・ダメージフリー研磨(第 1 報) -研磨中における電気化学測定の結果と得られた表面性状の相関-2015

    • Author(s)
      今西勇介, 遠藤勝義, 山村和也
    • Organizer
      2015年度精密工学会春季大会学術講演会
    • Place of Presentation
      東洋大学・白山キャンパス
    • Year and Date
      2015-03-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] 陽極酸化援用研磨による4H-SiCの平滑化に関する研究 ‐膜形成速度および膜除去速度の最適化-2014

    • Author(s)
      細谷憲治, 今西勇介, 遠藤勝義, 山村和也
    • Organizer
      電気加工学会全国大会
    • Place of Presentation
      新潟大学
    • Year and Date
      2014-12-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] 反応焼結SiC材の陽極酸化援用研磨法における加工状態の電気化学的モニタリングに関する検討2014

    • Author(s)
      今西勇介, 下園直樹, 遠藤勝義, 山村和也
    • Organizer
      電気加工学会全国大会
    • Place of Presentation
      新潟大学
    • Year and Date
      2014-12-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] Preliminary study on highly efficient polishing of 4H-SiC utilizing anodic oxidation2014

    • Author(s)
      K. Yamamura, K. Hosoya, Y. Imanishi, H. Deng, K. Endo
    • Organizer
      The 17th International Symposium on Advances in Abrasive Technology (ISAAT2014)
    • Place of Presentation
      Hawaii, USA
    • Year and Date
      2014-09-22 – 2014-09-25
    • Related Report
      2014 Annual Research Report
  • [Presentation] 陽極酸化援用研磨による4H-SiCの平滑化に関する研究 -セリアスラリーを電解液とした場合の研磨特性-2014

    • Author(s)
      細谷憲治, 今西勇介, 遠藤勝義, 山村和也
    • Organizer
      2014年度砥粒加工学会学術講演会
    • Place of Presentation
      岩手大学
    • Year and Date
      2014-09-14
    • Related Report
      2014 Annual Research Report
  • [Presentation] Investigation of the anodic oxide layer/SiC interface morphology during anodic oxidation assisted polishing2014

    • Author(s)
      K. Hosoya, Y. Imanishi, K. Endo, K. Yamamura
    • Organizer
      The 15th International Conference on Precision Engineering (ICPE2014)
    • Place of Presentation
      Kanazawa, Japan
    • Year and Date
      2014-07-23 – 2014-07-25
    • Related Report
      2014 Annual Research Report
  • [Presentation] 反応焼結SiC材の陽極酸化援用研磨における電極/研磨パッド複合ヘッドの開発2014

    • Author(s)
      今西勇介, 下園直樹, 遠藤勝義, 山村和也
    • Organizer
      精密工学会2014年度関西地方定期学術講演会
    • Place of Presentation
      近畿大学・東大阪キャンパス
    • Year and Date
      2014-07-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] 陽極酸化援用研磨法の単結晶4H-SiC基板への適用に関する検討

    • Author(s)
      細谷憲治
    • Organizer
      精密工学会2013年度関西地方定期学術講演会
    • Place of Presentation
      大阪工業大学大宮キャンパス
    • Related Report
      2013 Research-status Report
  • [Presentation] 陽極酸化援用加工における反応焼結SiC材の基礎的加工特性の評価

    • Author(s)
      下園直樹
    • Organizer
      精密工学会2013年度関西地方定期学術講演会
    • Place of Presentation
      大阪工業大学大宮キャンパス
    • Related Report
      2013 Research-status Report
  • [Presentation] 陽極酸化援用加工を用いた反応焼結 SiC 材の高精度ダメージフリー加工に関する研究 -陽極酸化における SiCと Si の酸化レートの評価-

    • Author(s)
      下園直樹
    • Organizer
      2013年度精密工学会秋季大会学術講演会
    • Place of Presentation
      関西大学千里山キャンパス
    • Related Report
      2013 Research-status Report
  • [Presentation] 陽極酸化援用研磨法の開発(第1報) -4H-SiCの基礎加工特性-

    • Author(s)
      細谷憲治
    • Organizer
      2013年度精密工学会秋季大会学術講演会
    • Place of Presentation
      関西大学千里山キャンパス
    • Related Report
      2013 Research-status Report
  • [Presentation] Figuring and finishing of reaction-sintered SiC by anodic oxidation assisted process

    • Author(s)
      下園直樹
    • Organizer
      5th International Conference of Asian Society for Precision Engineering and Nanotechnology (ASPEN2013)
    • Place of Presentation
      Taipei, Taiwan
    • Related Report
      2013 Research-status Report
  • [Presentation] 陽極酸化援用加工による反応焼結SiC材の加工特性の評価

    • Author(s)
      下園直樹
    • Organizer
      電気加工学会全国大会
    • Place of Presentation
      愛知県産業労働センター(ウインクあいち)
    • Related Report
      2013 Research-status Report
  • [Presentation] 4H-SiCの陽極酸化援用研磨による酸化膜形成メカニズムの考察

    • Author(s)
      細谷憲治
    • Organizer
      電気加工学会全国大会
    • Place of Presentation
      愛知県産業労働センター(ウインクあいち)
    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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