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Control of phase decomposition by nano plastic forming and its application for ultrahigh aspect ratio nano-machinning

Research Project

Project/Area Number 25630317
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Research InstitutionTohoku University

Principal Investigator

KOIZUMI Yuichiro  東北大学, 金属材料研究所, 准教授 (10322174)

Co-Investigator(Kenkyū-buntansha) YAMANAKA Akinori  東京農工大学, 大学院工学府, 准教授 (50542198)
NISHIYAMA Hiroaki  山形大学, 大学院工学研究科, 准教授 (80403153)
Co-Investigator(Renkei-kenkyūsha) YOSHINO Masahiko  東京工業大学, 理工学研究科, 教授 (40201032)
Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2014: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2013: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywordsトップダウンーボトムアップ融合プロセス / 相分離 / 析出 / 転位 / 相変態 / 鍛造 / 多孔体 / 選択溶解 / トップダウン-ボトムアップ融合プロセス / 精密・特殊加工プロセス / ナノ塑性加工 / 微細加工
Outline of Final Research Achievements

We successfully controlled gamma lamellae precipitation in Ti-39 at.% Al single crystals by nanogrooving process (NGP) intending to introduce periodic dislocation bands as preferential nucleation sites of gamma-TiAl lamellae precipitates. In NGP, grooves were formed along the trace of (0001) basal plane on the surfaces of single crystal of alpha 2-phase supersaturated with Al-atoms by nano-scale plastic deformation. Beneath the grooves, dislocation bands consisting of both basal dislocations and non-basal dislocations were formed. After aging at a dual phase temperature, pairs of gamma lamellae were found to form only beneath the grooves to depths greater than 30 μm, meaning that the location of gamma lamellae could be controlled by NGP. Also, selective dissolution of TiAl phase from hot deformed Ti-Al polycrystal was also performed. These findings opens new avenue for the manufacturing of near- or sub-wavelength grating structures with ultra-high aspect ratio.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (22 results)

All 2016 2015 2014 2013 Other

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (15 results) (of which Invited: 2 results) Remarks (2 results)

  • [Journal Article] Submicron lamellar porous structure formed by selective dissolution of Ti-Al alloy2016

    • Author(s)
      Dai-Xiu Wei, Yuichiro Koizumi, Yunping Li, Kenta Yamanaka, Akihiko Chiba
    • Journal Title

      Materials & Design

      Volume: 98 Pages: 1-11

    • DOI

      10.1016/j.matdes.2016.02.096

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Nano-lamellar/nano-tubular hierarchical porous structure produced by selective dissolution and anodization of lamellar Ti-40 at.% Al alloy2015

    • Author(s)
      D.X. Wei, Y. Koizumi, H. Bian, Y. Li, A. Chiba
    • Journal Title

      Materials Letters

      Volume: 145 Pages: 15-18

    • DOI

      10.1016/j.matlet.2014.11.059

    • Related Report
      2015 Annual Research Report 2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Nanoplastic deformation on Ti-39 at.% Al single crystals for manipulation of every single lamella2014

    • Author(s)
      D.X. Wei, Y. Koizumi, H. Nishiyama, A. Yamanaka, M. Yoshino, S. Miyamoto, K. Yoshimi, A. Chiba
    • Journal Title

      Acta Materialia

      Volume: 76 Pages: 331-341

    • DOI

      10.1016/j.actamat.2014.05.031

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Selective pore growth on lamellar Ti-41at.Al alloy2013

    • Author(s)
      Hiroaki Tsuciya
    • Journal Title

      Electrochemistry Communicaitons

      Volume: 26 Pages: 117-120

    • DOI

      10.1016/j.elecom.2012.08.025

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Journal Article] Microstructures developed by super-rapid induction heating-and-quenching (SRIHQ) of Fe-1.4%Cr-1%C pearlitic steel2013

    • Author(s)
      Y. Koizumi, T. Otsuka, Y. Minamino, T. Takayama, M. Ueyama, T. Daio, S. Hata
    • Journal Title

      Mater. Sci. Eng. A

      Volume: 577 Pages: 29-35

    • DOI

      10.1016/j.msea.2013.04.024

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] Anisotropic nano plastic deformation introduced by nanogrooving process in Ti-40 at.% Al single crystals2015

    • Author(s)
      Daixiu Wei, Yuichiro Koizumi, Akihiko Chiba, Takeshi Wada, Takayuki Ueno, Masahiko Yoshino
    • Organizer
      日本機械学会 M&M2015 材料力学カンファレンス
    • Place of Presentation
      東京工業大学
    • Year and Date
      2015-11-21
    • Related Report
      2015 Annual Research Report
  • [Presentation] Anisotropic nano plastic deformation introduced by nanogrooving process in Ti-40 at.% Al single crystals2015

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦, 和田 武, 加藤 秀実, 上野 貴之, 吉野 雅彦
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] Anistropic nano plastic deformation introduced by nanogrooving process in Ti-40 at.% Al single crystals2015

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦, 吉野 雅彦
    • Organizer
      第129回金属材料研究所講演会
    • Place of Presentation
      東北大学金属材料研究所
    • Year and Date
      2015-05-29
    • Related Report
      2015 Annual Research Report
  • [Presentation] Nano-plastic deformation on Ti-39 at.%Al single crystals for manipulating the precipitation of γ lamellae2015

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦, 西山 宏昭, 山中 晃徳, 吉野 雅彦
    • Organizer
      日本金属学会秋期(第156回)講演大会
    • Place of Presentation
      東京大学
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] Control of phase decomposition by nanogrooving process in Ti-39 at.% Al single crystals2015

    • Author(s)
      Dai-Xiu Wei, Yuichiro Koizumi, Hiroaki Nishiyama, Akinori Yamanaka, Masahiko Yoshino, Akihiko Chiba
    • Organizer
      Japan-Russia Joint Seminar "Advanced Materials Synthesis Process and Nanostructure"
    • Place of Presentation
      Sendai, Miyagi, Japan
    • Year and Date
      2015-03-09 – 2015-03-10
    • Related Report
      2014 Research-status Report
  • [Presentation] Refinement of lamellar structure by dislocations in Ti-40at.% Al alloy2014

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦
    • Organizer
      第128回東北大学金属材料研究所講演会
    • Place of Presentation
      東北大学金属材料研究所
    • Year and Date
      2014-11-27
    • Related Report
      2014 Research-status Report
  • [Presentation] Laminated Porous Structure Produced by Selective Dissolution and Anodization of Lamellar TiAl Alloy2014

    • Author(s)
      Daixu Wei, Yuichiro Koizumi, Akihiko Chiba
    • Organizer
      The 2nd International Symposium on Anodizing Science and Technology AST2014
    • Place of Presentation
      Sapporo, Hokkaido, Japan
    • Year and Date
      2014-06-04 – 2014-06-06
    • Related Report
      2014 Research-status Report
  • [Presentation] Control of phase decomposition by nano-plastic deformation in Ti-39 at.%Al single crystal2014

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦, 西山 宏昭, 山中 晃徳, 吉野 雅彦
    • Organizer
      第127回東北大学金属材料研究所講演会
    • Place of Presentation
      東北大学金属材料研究所
    • Year and Date
      2014-05-28
    • Related Report
      2014 Research-status Report
  • [Presentation] Control of phase decomposition by nano-plastic deformation in Ti-39 at.%Al single crystal2014

    • Author(s)
      Daixiu Wei, Yuichiro Koizumi, Akihiko Chiba
    • Organizer
      2014 Annu. Meeting of Excellent Graduate Schools for "Mat Integration Center" and "Mate Science Center" in conjunction with Intern. Workshop on Advanced Materials Synthesis Process and Nanostructure
    • Place of Presentation
      Akiu, Sendai
    • Related Report
      2013 Research-status Report
  • [Presentation] Nano-laminated Ti3Al Porous Structure Produced by Hot Forging and Selective Dissolution2014

    • Author(s)
      Daixiu Wei, Yuichiro Koizumi, Akihiko Chiba
    • Organizer
      2014 Functional Nanomaterials: Synthesis, Properties and Applications ― Nanomanufacturing I, TMS 2014 143rd Annual Meeting & Exhibition
    • Place of Presentation
      San Diego, TX, USA
    • Related Report
      2013 Research-status Report
  • [Presentation] Ultrahigh Aspect-ratio Nano-gratings of Ti-Al Alloy Fabricated by a Combined Top-down Bottom-up Approach2014

    • Author(s)
      Yuichiro Koizumi, Daixiu Wei, Akihiko Chiba, Akinori Yamanaka, Masahiko Yoshino, Hiroaki Nishiyama
    • Organizer
      2014 Functional Nanomaterials: Synthesis, Properties and Applications ― Nanomanufacturing II & Fabrication and Fundamentals I, TMS 2014 143rd Annual Meeting & Exhibition, San Diego, USA
    • Place of Presentation
      San Diego, TX, USA
    • Related Report
      2013 Research-status Report
  • [Presentation] Laminated Porous Structure Produced by Selective Dissolution and Anodization2014

    • Author(s)
      魏 代修, 小泉 雄一郎, 千葉 晶彦
    • Organizer
      第12 回日本金属学会東北支部研究発表大会
    • Place of Presentation
      名取
    • Related Report
      2013 Research-status Report
  • [Presentation] Control of phase decomposition by nano-plastic deformation in Ti-39 at.%Al single crysta2014

    • Author(s)
      Daixiu Wei, Yuichiro Koizumi, Akihiko Chiba, Hiroaki Nishiyama, Akinori Yamanaka, Masahiko Yoshino
    • Organizer
      日本金属学会春期 (第154回) 講演大会
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Research-status Report
  • [Presentation] ナノ塑性加工による金属ナノラメラ多孔体製造の試みと電子ビーム積層造形の可能性2014

    • Author(s)
      小泉 雄一郎
    • Organizer
      2013年度第5回ナノインプリント技術研究会
    • Place of Presentation
      東京
    • Related Report
      2013 Research-status Report
    • Invited
  • [Presentation] Ti-Al合金の加工・熱処理による組織制御とナノラメラ多孔体創製2014

    • Author(s)
      小泉 雄一郎
    • Organizer
      日本金属学会春期 (第154回) 講演大会[功績賞受賞講演].
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Research-status Report
    • Invited
  • [Remarks] 東北大学金属材料研究所 加工プロセス工学研究部門 千葉研究室

    • URL

      http://www.chibalab.imr.tohoku.ac.jp

    • Related Report
      2015 Annual Research Report
  • [Remarks] 東北大学金属材料研究所 加工プロセス工学研究部門 千葉研究室 WEBページ

    • URL

      http://www.chibalab.imr.tohoku.ac.jp/

    • Related Report
      2014 Research-status Report

URL: 

Published: 2014-07-25   Modified: 2019-07-29  

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