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Multi-modal multi-scale X-ray imaging complementary using synchrotron X-rays and free electron lasers

Research Project

Project/Area Number 25709057
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypePartial Multi-year Fund
Research Field Physical properties of metals/Metal-base materials
Research InstitutionOsaka University

Principal Investigator

Takahashi Yukio  大阪大学, 工学(系)研究科(研究院), 准教授 (00415217)

Project Period (FY) 2013-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥24,440,000 (Direct Cost: ¥18,800,000、Indirect Cost: ¥5,640,000)
Fiscal Year 2016: ¥5,330,000 (Direct Cost: ¥4,100,000、Indirect Cost: ¥1,230,000)
Fiscal Year 2015: ¥6,110,000 (Direct Cost: ¥4,700,000、Indirect Cost: ¥1,410,000)
Fiscal Year 2014: ¥6,110,000 (Direct Cost: ¥4,700,000、Indirect Cost: ¥1,410,000)
Fiscal Year 2013: ¥6,890,000 (Direct Cost: ¥5,300,000、Indirect Cost: ¥1,590,000)
KeywordsX線イメージング / ナノ材料 / X線自由電子レーザー / 放射光 / 金属物性 / X線
Outline of Final Research Achievements

We developed high-resolution coherent X-ray diffraction imaging techniques using focused hard X-ray free-electron laser pulses at SACLA. We performed the coherent X-ray diffraction imaging analysis of nanoparticles, allowing us to analyze the size distribution of particles as well as the electron density projection of individual particles. We measured 1000 single-shot coherent X-ray diffraction patterns of shape-controlled Ag nanocubes and Au/Ag nanoboxes, and estimated the edge length from the speckle size of the coherent diffraction patterns. We then reconstructed the two-dimensional electron density projection with sub-10-nm resolution from selected coherent diffraction patterns. We established a scheme for the complementary use of XFEL at SACLA and synchrotron X-rays at SPring-8

Report

(5 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Annual Research Report
  • 2014 Annual Research Report
  • 2013 Annual Research Report
  • Research Products

    (24 results)

All 2016 2015 2014 2013 Other

All Journal Article (4 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 4 results,  Open Access: 2 results,  Acknowledgement Compliant: 1 results) Presentation (17 results) (of which Invited: 10 results) Remarks (3 results)

  • [Journal Article] Multiple defocused coherent diffraction imaging: Method for simultaneously reconstructing objects and probe using X-ray free-electron lasers2016

    • Author(s)
      Makoto Hirose, Kei Shimomura, Akihiro Suzuki, Nicolas Burdet, Yukio Takahashi
    • Journal Title

      Optics Express

      Volume: 24 Issue: 11 Pages: 11917-11925

    • DOI

      10.1364/oe.24.011917

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Efficient use of coherent X-rays in ptychography: Towards high-resolution and high-throughput observation of weak-phase objects2016

    • Author(s)
      Nicolas Burdet, Kei Shimomura, Makoto Hirose, Akihiro Suzuki, Yukio Takahashi
    • Journal Title

      Applied Physics Letters

      Volume: 108 Issue: 7 Pages: 07113-07113

    • DOI

      10.1063/1.4942105

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] KOTOBUKI-1 apparatus for cryogenic coherent X-ray diffraction imaging2013

    • Author(s)
      M. Nakasako, Y. Takayama, T. Oroguchi, Y. Sekiguchi, A. Kobayashi, K. Shirahama, M. Yamamoto*, T. Hikima, K. Yonekura, S. Maki-Yonekura, Y. Kohmura, Y. Inubushi, Y. Takahashi*, A. Suzuki, S. Matsunaga, Y. Inui, K. Tono, T. Kameshima, Y. Joti, and T. Hoshi
    • Journal Title

      Review of Scientific Instruments

      Volume: 84 Issue: 12 Pages: 93705-16

    • DOI

      10.1021/nl403247x

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Anomalous Dressing of Dirac Fermions in the Topological Surface State of Bi2Se3, Bi2Te3, and Cu-Doped Bi2Se32013

    • Author(s)
      T. Kondo
    • Journal Title

      Phys. Rev. Lett

      Volume: 110 Issue: 6 Pages: 32002-32002

    • DOI

      10.1103/physrevlett.112.068103

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Presentation] 部分コヒーレントX線を用いたタイコグラフィ2016

    • Author(s)
      下村啓、Nicolas Burdet、鈴木明大、広瀬真、高橋幸生
    • Organizer
      第29回日本放射光学会年会放射光科学合同シンポジウム
    • Place of Presentation
      東京大学フューチャーセンター推進機構、千葉県柏市
    • Year and Date
      2016-01-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] プリセッション測定による高分解能X線タイコグラフィ2015

    • Author(s)
      下村啓、鈴木明大、広瀬真、香村芳樹、石川哲也、高橋幸生
    • Organizer
      第28回日本放射光学会年会
    • Place of Presentation
      立命館大学
    • Year and Date
      2015-01-11
    • Related Report
      2014 Annual Research Report
  • [Presentation] 暗視野X線タイコグラフィーの提案2015

    • Author(s)
      鈴木明大、下村啓、広瀬真、高橋幸生
    • Organizer
      第28回日本放射光学会年会
    • Place of Presentation
      立命館大学
    • Year and Date
      2015-01-11
    • Related Report
      2014 Annual Research Report
  • [Presentation] コヒーレントX線が拓く新しい3次元イメージング2014

    • Author(s)
      高橋幸生
    • Organizer
      日本結晶学会
    • Place of Presentation
      東京大学農学部
    • Year and Date
      2014-11-03
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] High-resolution hard x-ray ptychography of extended thick objects using multislice approach2014

    • Author(s)
      鈴木明大、下村啓、古宅伸、山内和人、香村芳樹、石川哲也、高橋幸生
    • Organizer
      International Conference on X-ray Microscopy(XRM2014)
    • Place of Presentation
      Melbourne Convention and Exibition Center, Melbourne, Australia
    • Year and Date
      2014-10-30
    • Related Report
      2014 Annual Research Report
  • [Presentation] High-resolution coherent X-ray diffraction imaging at SPring-8 and SACLA2014

    • Author(s)
      高橋幸生
    • Organizer
      AOFSRR2014
    • Place of Presentation
      Hsinchu, Taiwan
    • Year and Date
      2014-09-11
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] A method for ptychographic X-ray imaging of weak-phase objects2014

    • Author(s)
      鈴木明大、高橋幸生
    • Organizer
      The International Workshop on Phase Retrieval and Coherent Scattering (Coherence 2014)
    • Place of Presentation
      Northwestern University, Evanston, Illinois, USA
    • Year and Date
      2014-09-04
    • Related Report
      2014 Annual Research Report
  • [Presentation] Recent Progress of Hard X-ray Ptychography at SPring-82014

    • Author(s)
      高橋幸生
    • Organizer
      The International Workshop on Phase Retrieval and Coherent Scattering (Coherence 2014)
    • Place of Presentation
      Northwestern University, Evanston, Illinois, USA
    • Year and Date
      2014-09-03
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Coherent Diffraction Imaging with Focused Hard X-ray Beams2014

    • Author(s)
      高橋幸生
    • Organizer
      NSS-8(International Workshop on Nanoscale Spectroscopy and Nanotechnology)
    • Place of Presentation
      Chicago, USA
    • Year and Date
      2014-07-30
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] コヒーレントX線回折イメージングが拓く構造可視化の新しい世界2014

    • Author(s)
      高橋幸生
    • Organizer
      医学・生物学電子顕微鏡技術学会第30回学術講演
    • Place of Presentation
      大阪大学銀杏会館
    • Year and Date
      2014-05-24
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] XFEL コヒーレント回折イメージングによる金属ナノ粒子の組織と粒度分布の複合解析2014

    • Author(s)
      高橋幸生、鈴木明大、是津信行、苙口友隆、高山裕貴、関口優希、小林 周、山本雅貴、中迫雅由
    • Organizer
      第27回日本放射光学会年会
    • Place of Presentation
      広島国際会議場
    • Related Report
      2013 Annual Research Report
  • [Presentation] マルチスライスアプローチを用いた高分解能 X 線タイコグラフィー2014

    • Author(s)
      鈴木明大、古宅伸、下村啓、山内和人、香村芳樹、石川哲也、高橋幸生
    • Organizer
      第27回日本放射光学会年会
    • Place of Presentation
      広島国際会議場
    • Related Report
      2013 Annual Research Report
  • [Presentation] コヒーレントX線が拓く新しい結晶学2014

    • Author(s)
      高橋幸生
    • Organizer
      第27回日本放射光学会年会
    • Place of Presentation
      広島国際会議場
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] コヒーレントX線回折イメージングの現状と将来展望2013

    • Author(s)
      高橋幸生
    • Organizer
      第69回日本顕微鏡学会・学術講演会
    • Place of Presentation
      ホテル阪急エキスポパーク
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] コヒーレントX線回折を利用したマルチスケールイメージング2013

    • Author(s)
      高橋幸生
    • Organizer
      第62回高分子討論会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] High-resolution and High-sensitivity X-ray Ptychography Using Focused Hard X-ray Beam2013

    • Author(s)
      Yukio Takahashi
    • Organizer
      Ptycho2013
    • Place of Presentation
      Hohenkammer, Germany
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] High-resolution ptychographic imaging2013

    • Author(s)
      Yukio Takahashi
    • Organizer
      ICXOM22
    • Place of Presentation
      Hamburg, Germany
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Remarks]

    • URL

      http://www-up.prec.eng.osaka-u.ac.jp/takahashi

    • Related Report
      2015 Annual Research Report
  • [Remarks]

    • URL

      http://www-up.prec.eng.osaka-u.ac.jp/takahashi

    • Related Report
      2014 Annual Research Report
  • [Remarks] http://www-up.prec.eng.osaka-u.ac.jp/takahashi

    • Related Report
      2013 Annual Research Report

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Published: 2013-05-21   Modified: 2019-07-29  

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