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Toughening mechanism of laminar brittle phases sandwiched by ductile phases

Research Project

Project/Area Number 25709066
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypePartial Multi-year Fund
Research Field Structural/Functional materials
Research InstitutionKyoto University

Principal Investigator

OKAMOTO Norihiko  京都大学, 工学(系)研究科(研究院), 助教 (60505692)

Project Period (FY) 2013-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥23,010,000 (Direct Cost: ¥17,700,000、Indirect Cost: ¥5,310,000)
Fiscal Year 2014: ¥10,010,000 (Direct Cost: ¥7,700,000、Indirect Cost: ¥2,310,000)
Fiscal Year 2013: ¥13,000,000 (Direct Cost: ¥10,000,000、Indirect Cost: ¥3,000,000)
Keywords微小寸法試料 / 単結晶 / 結晶構造 / 集束イオンビーム(FIB)法 / 走査透過電子顕微鏡 / 異相界面 / 塑性変形 / 正20面体クラスター / 脆性延性転移 / その場観察変形試験 / 透過電子顕微鏡 / サイズ効果
Outline of Final Research Achievements

Galvannealed (GA) steels have been widely used in the automobile industry because of their high corrosion resistance, weldability, and paintability. When GA steels are deformed under severe conditions such as press-forming operations, the coating layer occasionally fails by decohesion at the coating-substrate interface. However, the mechanism of the coating decohesion has not been clarified yet. In the present research, we have performed systematic compression deformation experiments of single-phase polycrystalline and single-crystalline micropillars and two-phase micorpillars with one hetero-interface of the five different intermetallic compounds in the iron-zinc system constituting the coating layer of GA steels. We have clarified the fundamental mechanisms of the deformation of the coating layer and proposed a guideline for improving the decohesion-resistance of the coating layer of GA steels.

Report

(3 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • Research Products

    (26 results)

All 2015 2014 2013 Other

All Journal Article (15 results) (of which Peer Reviewed: 15 results,  Acknowledgement Compliant: 6 results) Presentation (8 results) (of which Invited: 2 results) Remarks (3 results)

  • [Journal Article] Arrangements of Fe-Centered Zn12 Icosahedra in Fe-Zn Intermetallic Compounds Determined by Ultra-High Resolution Scanning Transmission Electron Microscopy2015

    • Author(s)
      Norihiko L. Okamoto, Akira Yasuhara, Katsushi Tanaka and Haruyuki Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1760 Pages: 1-6

    • DOI

      10.1557/opl.2015.10

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Order-disorder structure of the phase in the Fe-Zn system determined by scanning transmission electron microscopy2014

    • Author(s)
      Norihiko L. Okamoto, Akira Yasuhara, Haruyuki Inui
    • Journal Title

      Acta Materialia

      Volume: 81 Pages: 345-357

    • DOI

      10.1016/j.actamat.2014.08.025

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Compression of Single-Crystal Micropillars of the Γ Intermetallic Phase in the Fe-Zn System2014

    • Author(s)
      Masahiro Inomoto, Norihiko L. Okamoto and Haruyuki Inui
    • Journal Title

      Advanced Materials Research

      Volume: 922 Pages: 264-269

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Micropillar Compression Deformation of Single Crystals of the Intermetallic Compound ζ-FeZn132014

    • Author(s)
      Norihiko L. Okamoto, Masahiro Inomoto, Hiroki Adachi, Hiroshi Takebayashi, and Haruyuki Inui
    • Journal Title

      Acta Materialia

      Volume: 65 Pages: 229-239

    • DOI

      10.1016/j.actamat.2013.10.065

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Specimen- and Grain-Size Dependence of Compression Deformation Behavior in Nanocrystalline Copper2014

    • Author(s)
      Norihiko L. Okamoto, Daisuke Kashioka, Tetsuji Hiratoh, and Haruyuki Inui
    • Journal Title

      International Journal of Plasticity

      Volume: 56 Pages: 173-183

    • DOI

      10.1016/j.ijplas.2013.12.003

    • NAID

      120005434967

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Crystal Structure Refinement of the δ1p Phase in the Fe-Zn System by Single-Crystal X-ray Diffraction Combined with Scanning Transmission Electron Microscopy2014

    • Author(s)
      N.L. Okamoto, K. Tanaka, A. Yasuhara and H. Inui
    • Journal Title

      Acta Crystallographica B

      Volume: 70 Issue: 2 Pages: 275-282

    • DOI

      10.1107/s2052520613034410

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Plastic Deformation of Single Crystals of Pt3Al with the L12 Structure Having a Far Al-Rich Off-Stoichiometric Composition of Pt-29at.%Al2014

    • Author(s)
      Norihiko L. Okamoto, Yoshihiko Hasegawa, and Haruyuki Inui
    • Journal Title

      Philosophical Magazine

      Volume: 94-12 Issue: 12 Pages: 1327-1344

    • DOI

      10.1080/14786435.2014.885142

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Compression Deformability of Γ and ζ Fe-Zn Intermetallics to Mitigate Detachment of Brittle Intermetallic Coating of Galvannealed Steels2013

    • Author(s)
      N.L. Okamoto, D. Kashioka, M. Inomoto, H. Inui, and S. Yamaguchi
    • Journal Title

      Scripta Materialia

      Volume: Vol.669, No.4 Issue: 4 Pages: 307-310

    • DOI

      10.1016/j.scriptamat.2013.05.003

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Quantitative Z-Contrast Imaging of Supported Metal Complexes and Clusters―A Gateway to Understanding Catalysis on the Atomic Scale2013

    • Author(s)
      Nigel D. Browning , Ceren Aydin, Jing Lu, Apoorva Kulkarni, Norihiko L. Okamoto, Volkan Ortalan, Bryan W. Reed, Alper Uzun, and Bruce C. Gates
    • Journal Title

      ChemCatChem

      Volume: 5 Issue: 9 Pages: 2673-2683

    • DOI

      10.1002/cctc.201200872

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Plastic Deformation of Single Crystals of Pt3Al with the L12 Structure2013

    • Author(s)
      N.L. Okamoto, Y. Hasegawa, W. Hashimoto and H. Inui
    • Journal Title

      Philosophical Magazine

      Volume: Vol. 93 Issue: 1-3 Pages: 60-81

    • DOI

      10.1080/14786435.2012.705037

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Micropillar Compression Deformation of Fe-Zn Intermetallic Compounds in the Coating Layer of Galvanized Steel2013

    • Author(s)
      N.L. Okamoto, D. Kashioka and H. Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1516 Pages: 283-288

    • DOI

      10.1557/opl.2012.1752

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Investigation of Specimen- and Grain-Size Dependence of Yield Stress in Electrodeposited Nanocrystalline Copper through Micropillar Compression2013

    • Author(s)
      Norihiko L. Okamoto, Daisuke Kashioka and Haruyuki Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1513 Pages: 1-6

    • DOI

      10.1557/opl.2013.559

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Difference in Elastic Properties of CrB2 Determined by Microscopic and Macroscopic Measurements2013

    • Author(s)
      Katsushi Tanaka, Satoshi Tsutsui, Norihiko L. Okamoto, Haruyuki Inui and Alfred Q.R. Baron
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1528 Pages: 1-6

    • DOI

      10.1557/opl.2013.362

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Compression Deformation of Single-Crystal Pt3Al with the L12 Structure2013

    • Author(s)
      Yoshihiko Hasegawa, Norihiko L. Okamoto and Haruyuki Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1516 Pages: 177-182

    • DOI

      10.1557/opl.2013.359

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Compression of Single-Crystal Micropillars of the ζ Intermetallic Phase in the Fe-Zn System2013

    • Author(s)
      N. Inomoto, N.L. Okamotoa and H. Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1516 Pages: 157-162

    • DOI

      10.1557/opl.2012.1667

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Presentation] Arrangements of Fe-Centered Zn12 Icosahedra in Fe-Zn Intermetallic Compounds Determined by Ultra-High Resolution Scanning Transmission Electron Microscopy2014

    • Author(s)
      Norihiko L. Okamoto, Akira Yasuhara, Katsushi Tanaka and Haruyuki Inui
    • Organizer
      Materials Research Society Fall Meeting,
    • Place of Presentation
      Boston, MA
    • Year and Date
      2014-11-30 – 2014-12-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] Micropillar Compression Deformation of Single Crystals of Fe-Zn Intermetallic Compounds Constituting the Coating Layer of Galvannealed Steels2014

    • Author(s)
      Norihiko L. Okamoto, Masahiro Inomoto and Haruyuki Inui
    • Organizer
      Materials Research Society Fall Meeting
    • Place of Presentation
      Boston, MA
    • Year and Date
      2014-11-30 – 2014-12-05
    • Related Report
      2014 Annual Research Report
  • [Presentation] GA鋼板のめっき被膜を構成するFe-Zn系金属間化合物の結晶構造と力学特性2014

    • Author(s)
      岡本範彦
    • Organizer
      日本金属学会第155回大会
    • Place of Presentation
      名古屋大学
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Fe-Zn系金属間化合物ζ相のマイクロピラー圧縮変形 Zn12二十面体の挙動2014

    • Author(s)
      岡本範彦, 井元雅弘, 乾晴行
    • Organizer
      日本金属学会第154回大会
    • Place of Presentation
      東京工業大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] Compression Deformation of the Fe-Zn Intermetallic Compounds Constituting the Coating Layer of Galvannealed Steels2013

    • Author(s)
      Norihiko L. Okamoto, Daisuke Kashioka, Masahiro Inomoto, Haruyuki Inui
    • Organizer
      THERMEC 2013
    • Place of Presentation
      Las Vegas, NV
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Compression of Single-Crystal Micropillars of the Γ Intermetallic Phase in the Fe-Zn System2013

    • Author(s)
      Masahiro Inomoto, Norihiko L. Okamoto, Haruyuki Inui
    • Organizer
      THERMEC 2013
    • Place of Presentation
      Las Vegas, NV
    • Related Report
      2013 Annual Research Report
  • [Presentation] 合金化溶融亜鉛めっき鋼板の被膜を構成するFe-Zn系金属間化合物相のマイクロピラー圧縮試験2013

    • Author(s)
      岡本範彦, 井元雅弘, 乾晴行
    • Organizer
      日本鉄鋼協会第166回秋季講演大会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fe-Zn系金属間化合物δ1p相の単結晶X線構造解析 ζ相構造との類似性2013

    • Author(s)
      岡本範彦, 田中克志, 乾晴行
    • Organizer
      日本金属学会第153回大会
    • Place of Presentation
      金沢大学
    • Related Report
      2013 Annual Research Report
  • [Remarks] 研究代表者のホームページ

    • URL

      http://nlokamoto.web.fc2.com/

    • Related Report
      2014 Annual Research Report
  • [Remarks] 研究者個人のホームページ

    • URL

      http://nlokamoto.web.fc2.com/

    • Related Report
      2013 Annual Research Report
  • [Remarks] 研究者が所属する研究室のホームページ

    • URL

      http://imc.mtl.kyoto-u.ac.jp/

    • Related Report
      2013 Annual Research Report

URL: 

Published: 2013-05-21   Modified: 2019-07-29  

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