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Development of frontier for growth of large single crystal diamond wafers to realize energy saving power electronic devices

Research Project

Project/Area Number 25820129
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Electronic materials/Electric materials
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

Hideaki Yamada  国立研究開発法人産業技術総合研究所, 先進パワーエレクトロニクス研究センター, 主任研究員 (90443233)

Project Period (FY) 2013-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,420,000 (Direct Cost: ¥3,400,000、Indirect Cost: ¥1,020,000)
Fiscal Year 2015: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Fiscal Year 2014: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2013: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Keywordsダイヤモンド / プラズマ / バルク単結晶 / ダイヤモンドウェハ / マイクロ波プラズマ / シミュレーション
Outline of Final Research Achievements

Aiming at realization of diamond wafers with a size larger than 1-inch size, I conducted numerical simulation of the plasma for the actual apparatus under the adopted growth conditions, which could give information about plasmas to grow such large size diamond with good uniformity as well as high growth rate. I found insufficiency in a conventional model to predict distribution of the growth rate. I modified the model and succeed in explaining the uniformity/non-uniformity of the growth rates. As a result of studying effects of small amount of nitrogen in the gas phase and preparation of the substrates, a 2-inch size mosaic diamond wafer was realized. For realization of further higher growth rate over larger area, effect of the rare gas was studied. I found that the introduction of the rare gas could realize improved growth rates with maintaining of uniformity.

Report

(4 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • 2013 Research-status Report
  • Research Products

    (34 results)

All 2016 2015 2014 2013

All Journal Article (9 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 9 results,  Acknowledgement Compliant: 7 results) Presentation (21 results) (of which Int'l Joint Research: 4 results,  Invited: 4 results) Patent(Industrial Property Rights) (4 results)

  • [Journal Article] Factors to control uniformity of single crystal diamond growth by using microwave plasma CVD2016

    • Author(s)
      山田英明、茶谷原 昭義、大曲 新矢、杢野 由明
    • Journal Title

      DIAMOND AND RELATED MATERIALS

      Volume: 63 Pages: 17-20

    • DOI

      10.1016/j.diamond.2015.09.016

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effects of intentionally introduced nitrogen and substrate temperature on growth of diamond bulk single-crystals2015

    • Author(s)
      山田英明、茶谷原 昭義、杢野 由明
    • Journal Title

      JAPANESE JOURNAL OF APPLIED PHYSICS

      Volume: 55 Issue: 1S Pages: 01AC07-01AC07

    • DOI

      10.7567/jjap.55.01ac07

    • NAID

      210000145955

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Dielectric properties of single crystalline diamond wafers with large area at microwave wavelengths2015

    • Author(s)
      山田英明、Andreas Meier、Francesco Mazzocchi、Sabine Schreck、Theo A. Scherer
    • Journal Title

      DIAMOND AND RELATED MATERIALS

      Volume: 58 Pages: 1-4

    • DOI

      10.1016/j.diamond.2015.05.004

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Numerical microwave plasma discharge study for the growth of large single-crystal diamond2015

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明、鹿田 真一
    • Journal Title

      DIAMOND AND RELATED MATERIALS

      Volume: 54 Pages: 9-14

    • DOI

      10.1016/j.diamond.2014.11.005

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effects of crystallographic orientation on the homoepitaxial overgrowth on tiled single crystal diamond clones2015

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明、加藤 有香子、鹿田 真一
    • Journal Title

      DIAMOND AND RELATED MATERIALS

      Volume: 印刷中 Pages: 17-21

    • DOI

      10.1016/j.diamond.2015.01.007

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Unintentional tungsten incorporation in diamond during hot-filament chemical vapor deposition2015

    • Author(s)
      大曲 新矢、Srimongkon Kridsanapan、Vittaya Amornkitbamrung、山田 英明、茶谷原 昭義、鹿田 真一
    • Journal Title

      Transactions of the Materials Research Society of Japan

      Volume: 40 Issue: 1 Pages: 47-50

    • DOI

      10.14723/tmrsj.40.47

    • NAID

      130005068870

    • ISSN
      1382-3469, 2188-1650
    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Characterization of free-standing single-crystal diamond prepared by hot-filament chemical vapor deposition2014

    • Author(s)
      S.Ohmagari, H.Yamada, H.Umezawa,A.Chayahara,T.Teraji and S.Shikata
    • Journal Title

      Diamond and Related Materials

      Volume: 48 Pages: 19-23

    • DOI

      10.1016/j.diamond.2014.06.001

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] デバイス用ダイヤモンドウェハのUVアシスト研磨に関する研究2014

    • Author(s)
      田川 智彦, 峠 睦, 坂本 武司, 鹿田真一, 山田 英明, 加藤 有香子
    • Journal Title

      精密工学会誌

      Volume: 80 Pages: 587-591

    • NAID

      130004745482

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] A 2-in. mosaic wafer made of a single-crystal diamond2014

    • Author(s)
      H. Yamada, A. Chayahara, Y. Mokuno, Y. Kato and S. Shikata
    • Journal Title

      Applied Physics Letters

      Volume: 104 Issue: 10 Pages: 102110-102110

    • DOI

      10.1063/1.4868720

    • Related Report
      2013 Research-status Report
    • Peer Reviewed
  • [Presentation] 大面積ダイヤモンド基板上への合成におけるAr導入効果2016

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明
    • Organizer
      第63回応用物理学会春季学術講演会
    • Place of Presentation
      東京工業大学(東京)
    • Year and Date
      2016-03-19
    • Related Report
      2015 Annual Research Report
  • [Presentation] ダイヤモンド合成用のマイクロ波のパルス化による効果2015

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明
    • Organizer
      第32回プラズマ・核融合学会年会
    • Place of Presentation
      名古屋大学(愛知)
    • Year and Date
      2015-11-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] 単結晶ダイヤモンドウェハ作製技術開発2015

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明
    • Organizer
      先進パワー半導体分科会 第2回講演会
    • Place of Presentation
      大阪国際交流センター(大阪)
    • Year and Date
      2015-11-09
    • Related Report
      2015 Annual Research Report
  • [Presentation] Single-crystal diamond growth with sub-millisecond-pulsed discharge of microwave plasma2015

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明
    • Organizer
      CRP-9/GEC-68/SPP-3
    • Place of Presentation
      Honolulu, USA
    • Year and Date
      2015-10-12
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] ダイヤモンドウェハ・バルクの作製技術開発2015

    • Author(s)
      山田 英明
    • Organizer
      第3回放電・プラズマ気相シミュレーション技法調査専門委員会
    • Place of Presentation
      金沢大学(石川)
    • Year and Date
      2015-09-18
    • Related Report
      2015 Annual Research Report
  • [Presentation] Planarization and Smoothing of CVD Grown Diamond Wafer by Atmospheric Pressure Plasma Based Process2015

    • Author(s)
      道上久也、田畑雄壮、遠藤勝義、山田 英明、茶谷原 昭義、杢野 由明、山村和也
    • Organizer
      ASPEN2015
    • Place of Presentation
      ハルピン,中国
    • Year and Date
      2015-08-15
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Progress and current status of single crystal diamond wafers for high power electronics2015

    • Author(s)
      山田英明
    • Organizer
      The 3rd French Japanese workshop on diamond power devices
    • Place of Presentation
      Nimes, FRANCE
    • Year and Date
      2015-07-07
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Study of growth mechanism for uniform CVD of single-crystal diamond2015

    • Author(s)
      山田 英明、茶谷原 昭義、大曲 新矢、杢野 由明
    • Organizer
      NDNC2015
    • Place of Presentation
      静岡グランシップ(静岡)
    • Year and Date
      2015-05-25
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effects of inpurity and substrate temperature on diamond growth2015

    • Author(s)
      山田 英明
    • Organizer
      ISPlasma2015/IC-PLANTS2015
    • Place of Presentation
      Nagoya Univ.
    • Year and Date
      2015-03-26
    • Related Report
      2014 Research-status Report
  • [Presentation] 次世代型の省エネパワーデバイスを指向した単結晶ダイヤモンドウェハ作製技術【キーノート講演】2015

    • Author(s)
      山田 英明
    • Organizer
      精密加工学会
    • Place of Presentation
      東洋大学
    • Year and Date
      2015-03-19
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] プラズマCVDを用いたダイヤモンド単結晶成長における基板温度変化と窒素添加効果2015

    • Author(s)
      山田 英明
    • Organizer
      応用物理学会春季学術講演会
    • Place of Presentation
      東海大学
    • Year and Date
      2015-03-11
    • Related Report
      2014 Research-status Report
  • [Presentation] ダイヤモンド単結晶基板の作製とパワーデバイス応用2015

    • Author(s)
      山田 英明
    • Organizer
      平成26年度 第3回ナノ理工学情報交流会
    • Place of Presentation
      大阪大学
    • Year and Date
      2015-01-14
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] Processing to fabricate mosaic wafers of single-crystal diamond with 2 inch size2014

    • Author(s)
      山田 英明
    • Organizer
      International Conference on Diamond and Carbon Materials
    • Place of Presentation
      Madrid, Spain
    • Year and Date
      2014-09-17
    • Related Report
      2014 Research-status Report
  • [Presentation] マイクロ波プラズマCVDを用いたダイヤモンド単結晶成長速度およびその分布解析2014

    • Author(s)
      山田 英明
    • Organizer
      Plasma Conference 2014
    • Place of Presentation
      朱鷺メッセ
    • Year and Date
      2014-09-14
    • Related Report
      2014 Research-status Report
  • [Presentation] Current status of techniques to fabricate single-crystal diamond wafers2014

    • Author(s)
      山田 英明
    • Organizer
      15th IUMRS-ICA
    • Place of Presentation
      Fukuoka Univ
    • Year and Date
      2014-08-24
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] 結晶ダイヤモンドウェハ作製技術開発の現状-合成・加工及び関連技術-2014

    • Author(s)
      山田 英明
    • Organizer
      第2回「表面創成工学の新展開」研究会
    • Place of Presentation
      田沢湖芸術村(秋田県)
    • Related Report
      2013 Research-status Report
  • [Presentation] 2インチ大の接合型単結晶ダイヤモンドウェハの試作2014

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明、加藤 有香子、鹿田 真一
    • Organizer
      第61回応用物理学会春季学術講演会
    • Place of Presentation
      青山学院大学(神奈川)
    • Related Report
      2013 Research-status Report
  • [Presentation] 熱フィラメントCVD法で成長した単結晶ダイヤモンド膜の構造評価2014

    • Author(s)
      大曲 新矢、山田 英明、茶谷原 昭義、鹿田 真一
    • Organizer
      第61回応用物理学会春季学術講演会
    • Place of Presentation
      青山学院大学(神奈川)
    • Related Report
      2013 Research-status Report
  • [Presentation] マイクロ波プラズマCVDによるダイヤモンドの合成速度の制御2013

    • Author(s)
      山田 英明、茶谷原 昭義、杢野 由明
    • Organizer
      第27回ダイヤモンドシンポジウム
    • Place of Presentation
      日本工業大学(埼玉)
    • Related Report
      2013 Research-status Report
  • [Presentation] パワーデバイス応用を目指したウェハ・デバイスの開発課題2013

    • Author(s)
      鹿田 真一、梅澤 仁、加藤 有香子、大曲 新矢、山田 英明、坪内 信輝、杢野 由明、茶谷原 昭義
    • Organizer
      第27回ダイヤモンドシンポジウム
    • Place of Presentation
      日本工業大学(埼玉)
    • Related Report
      2013 Research-status Report
  • [Presentation] 熱フィラメントCVD法によるホモエピタキシャルダイヤモンド膜合成2013

    • Author(s)
      大曲 新矢、山田 英明、茶谷原 昭義、鹿田 真一
    • Organizer
      第27回ダイヤモンドシンポジウム
    • Place of Presentation
      日本工業大学(埼玉)
    • Related Report
      2013 Research-status Report
  • [Patent(Industrial Property Rights)] モザイク状ダイヤモンドの製造方法2014

    • Inventor(s)
      山田英明、茶谷原昭義、杢野由明、鹿田真一
    • Industrial Property Rights Holder
      山田英明、茶谷原昭義、杢野由明、鹿田真一
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-096700
    • Filing Date
      2014-05-08
    • Related Report
      2014 Research-status Report
  • [Patent(Industrial Property Rights)] ダイヤモンドのエッチング方法、ダイヤモンドの結晶欠陥の検出方法、およびダイヤモンド結晶の結晶成長方法2014

    • Inventor(s)
      姚永昭、石川由加里、山田英明、茶谷原昭義
    • Industrial Property Rights Holder
      姚永昭、石川由加里、山田英明、茶谷原昭義
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-259658
    • Filing Date
      2014-12-24
    • Related Report
      2014 Research-status Report
  • [Patent(Industrial Property Rights)] 単結晶ダイヤモンドの製造方法2013

    • Inventor(s)
      山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Holder
      山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2013-205146
    • Filing Date
      2013-09-30
    • Related Report
      2013 Research-status Report
  • [Patent(Industrial Property Rights)] 単結晶ダイヤモンドの製造方法2013

    • Inventor(s)
      山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Holder
      山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2013-205154
    • Filing Date
      2013-09-30
    • Related Report
      2013 Research-status Report

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Published: 2014-07-25   Modified: 2019-07-29  

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