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Mass production of pure nanoparticles using pulse-modulated induction thermal plasma with intermittent feeding of feedstock

Research Project

Project/Area Number 26249034
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Power engineering/Power conversion/Electric machinery
Research InstitutionKanazawa University

Principal Investigator

Tanaka Yasunori  金沢大学, 電子情報学系, 教授 (90303263)

Co-Investigator(Kenkyū-buntansha) 石島 達夫  金沢大学, サステナブルエネルギー研究センター, 准教授 (00324450)
上杉 喜彦  金沢大学, 電子情報学系, 教授 (90213339)
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥40,690,000 (Direct Cost: ¥31,300,000、Indirect Cost: ¥9,390,000)
Fiscal Year 2016: ¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2015: ¥14,300,000 (Direct Cost: ¥11,000,000、Indirect Cost: ¥3,300,000)
Fiscal Year 2014: ¥21,710,000 (Direct Cost: ¥16,700,000、Indirect Cost: ¥5,010,000)
Keywords電気有効利用 / 熱プラズマ / 誘導熱プラズマ / ナノ粒子 / 大量生成 / 量産技術 / 2次元分光 / ドープ / 気相反応 / ナノ材料 / 電気機器工学 / 電気・電子材料 / 酸化物 / 金属イオンドープ
Outline of Final Research Achievements

This study focused on development of an innovative high production synthesis method for pure functional nanoparticles using modulated induction thermal plasmas with intermittent feeding of feedstock. This method was originally developed by our group and modified for high-production of various nanoparticles. As target functional nanoparticles, Al-doped TiO2 nanopowder was tried to be synthesized. Using the developed method, Al-doped TiO2 nanopowder was successfully fabricated with a high production of 400 g/h at 20 kW. In addition, to study the evaporation process of injected feedstock, two-dimensional spectroscopic observation was carried out. Results showed the position and timing of the feedstock evaporation, which would be important to improve the production rate of nanopowder further.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Annual Research Report
  • 2014 Annual Research Report
  • Research Products

    (21 results)

All 2016 2015 2014

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 1 results,  Open Access: 2 results) Presentation (18 results) (of which Int'l Joint Research: 14 results,  Invited: 7 results)

  • [Journal Article] Fundamental study of Ti feedstock evaporation and precursor formation process in inductively coupled thermal plasmas during TiO2 nanopowder synthesis2016

    • Author(s)
      Naoto Kodama, Yasunori Tanaka, K. Kita, Y. Ishisaka, Y.Uesugi, T.Ishijima, S.Sueyasu, K.Nakamura
    • Journal Title

      Journal of Physics D: Applied Physics

      Volume: 49 Issue: 30 Pages: 305501-305501

    • DOI

      10.1088/0022-3727/49/30/305501

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Two-dimensional spectroscopic observation of a pulse-modulated induction thermal plasma torch for nanopowder synthesis2014

    • Author(s)
      N. Kodama, K. Kita, Y. Tanaka, Y. Uesugi, T. Ishijima, S.Watanabe, K. Nakamura
    • Journal Title

      J. Phys.: Conf. Ser.

      Volume: 550 Pages: 012026-012026

    • DOI

      10.1088/1742-6596/550/1/012026

    • NAID

      120005537891

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] A method for large-scale synthesis of Al-doped TiO_2 nanopowder using pulse-modulated induction thermal plasmas with time-controlled feedstock feeding2014

    • Author(s)
      N.Kodama, Y.Tanaka, K.Kita, Y.Uesugi, T.Ishijima, S.Watanabe and K.Nakamura
    • Journal Title

      Phys. D : Appl. Phys

      Volume: Vol.47 Issue: 19 Pages: 195304-195304

    • DOI

      10.1088/0022-3727/47/19/195304

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] Nanopowder synthesis processes using the time-controlled induction thermal plasmas2016

    • Author(s)
      Yasunori Tanaka, N. Kodama, Y.Ishisaka, Y.Uesugi, T.Ishijima, S.Sueyasu, S.Watanabe and T.Nakamura
    • Organizer
      Joint 13th Asia Pacific Physics Conference and 22nd Australian Institute of Physics Congress
    • Place of Presentation
      Brisbane (Australia)
    • Year and Date
      2016-12-04
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Non-Equilibrium Simulation of 'Thermal' Plasmas2016

    • Author(s)
      Yasunori Tanaka
    • Organizer
      Gordon Research Conference
    • Place of Presentation
      Andover (USA)
    • Year and Date
      2016-07-24
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 2-D temperature estimation in Ar-O2 induction thermal plasmas for TiO2 nanopowder synthesis2016

    • Author(s)
      N. Kodama*, K. Kita, Y. Ishisaka, Y. Tanaka, Y. Uesugi, T. Ishijima, K. Nakamura, S. Sueyasu
    • Organizer
      14th High-Tech Plasma Processes
    • Place of Presentation
      Munich (Germany)
    • Year and Date
      2016-07-03
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] High rate synthesis of Si/SiOx nanoparticles/nanowires using modulated induction thermal plasmas with controlled feedstock feeding2016

    • Author(s)
      Y. Tanaka*, Y.Ishisaka, N.Kodama, K.Kita, Y. Uesugi, T. Ishijima, S. Sueyasu, K. Nakamura
    • Organizer
      14th High-Tech Plasma Processes
    • Place of Presentation
      Munich (Germany)
    • Year and Date
      2016-07-03
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Estimation on two-dimensional distribution of Ti excitation temperature during Ti feedstock injection into Ar induction thermal plasma torch2016

    • Author(s)
      N.Kodama*, K. Kita, Y. Ishisaka, Y. Tanaka, Y. Uesugi, T. Ishijima, S. Sueyasu, K. Nakamura
    • Organizer
      18th Int.Congress on Plasmas Physics (ICPP2016)
    • Place of Presentation
      Kaoshung(Taiwan)
    • Year and Date
      2016-06-26
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Development of various types of induction thermal plasma source and their applications to materials processings2016

    • Author(s)
      Y.Tanaka
    • Organizer
      18th Int.Congress on Plasmas Physics (ICPP2016)
    • Place of Presentation
      Kaoshung (Taiwan)
    • Year and Date
      2016-06-26
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Modulated Induction Thermal Plasmas for Large-Scale Nanopowder Synthesis2016

    • Author(s)
      Y.Tanaka
    • Organizer
      13th Asia-Pacific Conference on Plasma Science and Technology (APCPST2016)
    • Place of Presentation
      Shanghai (China)
    • Year and Date
      2016-05-19
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Comparison of intermittent synchronized feeding and continuous feeding of feedstock during Si nanoparticle synthesis using pulse modulated induction thermal plasmas2016

    • Author(s)
      Yousuke Ishisaka*, Kentaro Kita, Naoto Kodama, Yasunori Tanaka, Yoshihiko Uesugi, Tatsuo Ishijima, Shiori Sueyasu, Keitaro Nakamura
    • Organizer
      13th Asia-Pacific Conference on Plasma Science and Technology (APCPST2016)
    • Place of Presentation
      Shanghai (China)
    • Year and Date
      2016-05-19
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Silicon nanoparticles synthesized by pulse-modulated induction thermal plasmas with intermittent feedstock feeding2016

    • Author(s)
      Y.Ishisaka*, K.Kita, N.Kodama,Y.Tanaka, Y. Uesugi, T.Ishijima, S.Sueyasu,K.Nakamura
    • Organizer
      ISPlasma2016/ICPLANTS2016
    • Place of Presentation
      Nagoya
    • Year and Date
      2016-03-07
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Two-Dimensional Spectroscopic Observation from Ar/H2 Modulated Induction Thermal Plasma for Si Nanopowder Synthesis2015

    • Author(s)
      Kentaro Kita*, Yousuke Ishisaka, Naoto Kodama, Yasunori Tanaka, Yoshihiko Uesugi, Tatsuo Ishijima, Shiori Sueyasu, Keitaro Nakamura
    • Organizer
      APSPT-9/SPSM-28
    • Place of Presentation
      Nagasaki
    • Year and Date
      2015-12-11
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Silicon Nanoparticle Synthesis using Pulse-Modulated Induction Thermal Plasmas with Intermittent Feedstock Feeding2015

    • Author(s)
      Yasunori Tanaka*, Yousuke Ishisaka, Kentaro Kita, Naoto Kodama, Tatsuo Ishijima, Yoshihiko Uesugi, Shiori Sueyasu, Keitaro Nakamura
    • Organizer
      APSPT-9/SPSM-28
    • Place of Presentation
      Nagasaki
    • Year and Date
      2015-12-11
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Investigation on evaporation of Ti feedstock and formation of precursor TiO molecules during TiO2 nanopowder synthesis in induction thermal plasma with time-controlled feedstock injection2015

    • Author(s)
      Naoto Kodama*, Kentaro Kita, Yosuke Ishisaka, Yasunori Tanaka, Yoshihiko Uesugi, Tatsuo Ishijima, Shiori Sueyasu, Keitaro Nakamura
    • Organizer
      GEC-68/ICRP-9/SPP-33
    • Place of Presentation
      Honolulu
    • Year and Date
      2015-10-12
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Influence of quenching gas injection on the temperature field in pulse-modulated induction thermal plasma for large scale nanopowder synthesis2015

    • Author(s)
      Yasunori Tanaka*, Weixuan Guo, Naoto Kodama, Kentaro Kita, Yoshihiko Uesugi, Tatsuo Ishijima, Shu Watanabe, Keitaro Nakamura
    • Organizer
      GEC-68/ICRP-9/SPP-33
    • Place of Presentation
      Honolulu
    • Year and Date
      2015-10-12
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Spectroscopic study on evaporation of Ti feedstock intermittently supplied and formation of precursor TiO in TiO2 nanopowder synthesis in the induction thermal plasma torch2015

    • Author(s)
      N.Kodama*, K.Kita, Y.Tanaka, Y.Uesugi, T.Ishijima, S.Watanabe, K.Nakamura
    • Organizer
      22nd Int. Sym. Plasma Chem. (ISPC-22)
    • Place of Presentation
      Antwerp
    • Year and Date
      2015-07-05
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Two-Dimensional Spectroscopic Observation in the Plasma Torch for Pulse-Modulated Induction Thermal Plasmas for Nanopowder Synthesis2014

    • Author(s)
      N. Kodama*, K.Kita, Y.Tanaka, Y.Uesugi, T.Ishijima, S.Watanabe, K.Nakamura
    • Organizer
      High-Tech Plasma Processes HTTP-2014
    • Place of Presentation
      Toulouse,France
    • Year and Date
      2014-06-23 – 2014-06-27
    • Related Report
      2014 Annual Research Report
  • [Presentation] Adoption of Pulse-Modulated Induction Thermal Plasmas with Time-Controlled Feedstock Feeding to High Production Rate Synthesis of Metallic Ion Doped TiO2 Nanopowder2014

    • Author(s)
      Y. Tanaka*, N.Kodama, K.Kita, Y.Uesugi, T.Ishijima, S.Watanabe, K.Nakamura
    • Organizer
      High-Tech Plasma Processes HTTP-2014
    • Place of Presentation
      Toulouse,France
    • Year and Date
      2014-06-23 – 2014-06-27
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Application of modulated RF thermal plasmas to synthesis of large amounts of nanoparticles2014

    • Author(s)
      Y.Tanaka
    • Organizer
      International Microwave Power Institude Symposium IMPI-48
    • Place of Presentation
      New Orleans, USA
    • Year and Date
      2014-06-19 – 2014-06-21
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Development of modulated induction thermal plasmas and their application to large scale synthesis of nanopowder2014

    • Author(s)
      Y.Tanaka
    • Organizer
      International Conference on Microelectronics and Plasma Technology, ICMAP2014
    • Place of Presentation
      Gunsan, S.Korea
    • Year and Date
      2014-06-08 – 2014-06-11
    • Related Report
      2014 Annual Research Report
    • Invited

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Published: 2014-04-04   Modified: 2018-03-22  

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