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Diamond growth for nanoscale NMR sensing

Research Project

Project/Area Number 26249108
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

watanabe hideyuki  国立研究開発法人産業技術総合研究所, 電子光技術研究部門, 主任研究員 (50392684)

Co-Investigator(Kenkyū-buntansha) 伊藤 公平  慶應義塾大学, 理工学部, 教授 (30276414)
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥39,780,000 (Direct Cost: ¥30,600,000、Indirect Cost: ¥9,180,000)
Fiscal Year 2016: ¥5,720,000 (Direct Cost: ¥4,400,000、Indirect Cost: ¥1,320,000)
Fiscal Year 2015: ¥18,330,000 (Direct Cost: ¥14,100,000、Indirect Cost: ¥4,230,000)
Fiscal Year 2014: ¥15,730,000 (Direct Cost: ¥12,100,000、Indirect Cost: ¥3,630,000)
Keywordsセンサー / 光機能材料 / ダイヤモンド / マイクロ波プラズマ / NMR / ホモエピタキシャル成長 / ソリッドステート / 材料工学 / 機能材料 / 微細構造 / 同位体ダイヤモンド / 量子センサ / 電子スピン / 微細加工
Outline of Final Research Achievements

We have been working on the development of an advanced method for growing diamond thin films, which may enable the implementation of nano NMR sensing. We have explored a method to grow homoepitaxial diamond thin films by focusing on a high purity microwave source (solid state type). The solid state microwave source has almost never been used in the diamond thin film synthesis using the microwave plasma CVD process. The magnetron power source is commonly used one currently.
We have demonstrated, through our systematic experiments on thin film synthesis, that our new method employing a high purity microwave source enables the suppression of crystal defects and the formation of extremely shallow NV centers, which have not been achieved when using the conventional magnetron source. Also we have clarified the features of the CVD process used with the solid state source.

Report

(5 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Annual Research Report
  • 2014 Annual Research Report
  • Products Report
  • Research Products

    (32 results)

All 2022 2017 2016 2015 2014

All Journal Article (7 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 7 results,  Open Access: 3 results,  Acknowledgement Compliant: 2 results) Presentation (23 results) (of which Int'l Joint Research: 4 results,  Invited: 4 results) Patent(Industrial Property Rights) (2 results) (of which Overseas: 1 results)

  • [Journal Article] Formation of Nitrogen-Vacancy Centers in Homoepitaxial Diamond Thin Films Grown via Microwave Plasma-Assisted Chemical Vapor Deposition2016

    • Author(s)
      H. Watanabe, H. Umezawa, T. Ishikawa, K. Kaneko, S. Shikata, J. Ishi-Hayase, and K. M. Itoh
    • Journal Title

      IEEE Transactions on Nanotechnology

      Volume: 15 Issue: 4 Pages: 614-618

    • DOI

      10.1109/tnano.2016.2528678

    • Related Report
      2016 Annual Research Report 2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] High density NV sensing surface created via He^(+) ion implantation of (12)^C diamond2016

    • Author(s)
      Ed E. Kleinsasser, Matthew M. Stanfield, Jannel K.Q. Banks, Zhouyang Zhu, Wen-Di Li, Victor M. Acosta, Hideyuki Watanabe, Kohei M. Itoh, Kai-Mei C. Fu
    • Journal Title

      APPLIED PHYSICS LETTERS

      Volume: 108 Issue: 20

    • DOI

      10.1063/1.4949357

    • Related Report
      2016 Annual Research Report 2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Broadband, large-area microwave antenna for optically detected magnetic resonance of nitrogen-vacancy centers in diamond2016

    • Author(s)
      K. Sasaki, Y. Monnai, S. Saijo, R. Fujita, H. Watanabe, J. Ishi-Hayase, K.M. Itoh and E. Abe
    • Journal Title

      Review of Scientific Instruments

      Volume: 87 Issue: 5

    • DOI

      10.1063/1.4952418

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Broadband, large-area microwave antenna for optically-detected magnetic resonance of nitrogen-vacancy centers in diamond2016

    • Author(s)
      Kento Sasaki, Yasuaki Monnai, Soya Saijo, Ryushiro Fujita, Hideyuki Watanabe, Junko Ishi-Hayase, Kohei Itoh, and Eisuke Abe
    • Journal Title

      Review of Scientific Instruments

      Volume: in press

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Laser-Assisted Field Evaporation and Three-Dimensional Atom-by-Atom Mapping of Diamond Isotopic Homojunctions2016

    • Author(s)
      Samik Mukherjee, Hideyuki Watanabe, Dieter Isheim, David N. Seidman, and Oussama Moutanabbir
    • Journal Title

      Nano Letters

      Volume: 16 Issue: 2 Pages: 1335-1344

    • DOI

      10.1021/acs.nanolett.5b04728

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Friction Modification by Shifting of Phonon Energy Dissipation in Solid Atoms2015

    • Author(s)
      Seiji Kajita, Mamoru Tohyama, Hitoshi Washizu, Toshihide Ohmori, Hideyuki Watanabe, Shinichi Shikata
    • Journal Title

      Tribology Online

      Volume: 10 Issue: 2 Pages: 156-161

    • DOI

      10.2474/trol.10.156

    • NAID

      130005065514

    • ISSN
      1881-218X, 1881-2198
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Isotope engineering of silicon and diamond for quantum computing and sensing applications2014

    • Author(s)
      K.M. Itoh and H. Watanabe
    • Journal Title

      MRS Communications

      Volume: 4 Issue: 4 Pages: 143-157

    • DOI

      10.1557/mrc.2014.32

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed
  • [Presentation] 従来の開発技術の延長線上では越えられない超高感度分析装置の実現へ2017

    • Author(s)
      渡邊幸志, 櫻井竜也, 伊藤公平
    • Organizer
      新技術説明会
    • Place of Presentation
      JST東京本部別館
    • Year and Date
      2017-03-16
    • Related Report
      2016 Annual Research Report
  • [Presentation] ダイヤモンドNV量子センシングによる単一核スピン検出器の設計2016

    • Author(s)
      石川豊史, 渡邊幸志, 柏谷聡,吉澤明男, 馬渡康徳
    • Organizer
      第30回ダイヤモンドシンポジウム
    • Place of Presentation
      東京大学 駒場リサーチキャンパス コンベンションホール
    • Year and Date
      2016-11-17
    • Related Report
      2016 Annual Research Report
  • [Presentation] ソリッドステート方式マイクロ波源を用いたマイクロ波プラズマCVD法によるホモエピタキシャルダイヤモンド薄膜の合成2016

    • Author(s)
      渡邊幸志, 石川豊史, 伊藤公平
    • Organizer
      第30回ダイヤモンドシンポジウム
    • Place of Presentation
      東京大学 駒場リサーチキャンパス コンベンションホール
    • Year and Date
      2016-11-16
    • Related Report
      2016 Annual Research Report
  • [Presentation] 配向制御されたダイヤモンドNV 中心を用いた交流電流センシング2016

    • Author(s)
      西條蒼野, 藤田留士郎, 花野郁也, 北澤清香, 渡邊幸志, 赤羽浩一, 佐々木健人, 松崎雄一郎, 早瀬潤子
    • Organizer
      第77回応用物理学会秋季学術講演会
    • Place of Presentation
      新潟県 朱鷺メッセ
    • Year and Date
      2016-09-13
    • Related Report
      2016 Annual Research Report
  • [Presentation] ダイヤモンド中NV 中心集合体のパルス光検出磁気共鳴イメージング2016

    • Author(s)
      岡崎睦, 渡邊幸志, 赤羽浩一, 門内靖明, 佐々木健人, 伊藤公平, 早瀬潤子
    • Organizer
      第77回応用物理学会秋季学術講演会
    • Place of Presentation
      新潟県 朱鷺メッセ
    • Year and Date
      2016-09-13
    • Related Report
      2016 Annual Research Report
  • [Presentation] 微細加工基板上に生成されたダイヤモンド中窒素空孔中心の物性評価2016

    • Author(s)
      花野郁也, 藤田留士郎, 渡邊幸志, 赤羽浩一, 早瀬潤子
    • Organizer
      第77回応用物理学会秋季学術講演会
    • Place of Presentation
      新潟県 朱鷺メッセ
    • Year and Date
      2016-09-13
    • Related Report
      2016 Annual Research Report
  • [Presentation] Quantum sensing with isotopically purified 12C diamond2016

    • Author(s)
      Kohei M. Itoh, Kento Sasaki, Hideyuki Watanabe, Eisuke Abe
    • Organizer
      ISCSI-VII/ISTDM2016
    • Place of Presentation
      Nagoya, Japan
    • Year and Date
      2016-06-08
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] ダイヤモンド中窒素空孔中心集合体を用いた光検出磁気共鳴イメージング2016

    • Author(s)
      岡崎 睦、藤田 留士郎、渡邊 幸志,赤羽浩一,門内 靖明、伊藤公平,早瀬 潤子
    • Organizer
      第63回応⽤物理学会春季学術講演会
    • Place of Presentation
      東京工業業大学,東京都
    • Year and Date
      2016-03-20
    • Related Report
      2015 Annual Research Report
  • [Presentation] 微細加工基板上化学気相成長により生成した高配向率を有するダイヤモンド中窒素空孔中心のスピン特性2016

    • Author(s)
      藤田 留士郎,西條蒼野,渡邊 幸志,赤羽浩一,伊藤公平,早瀬 潤子
    • Organizer
      第63回応⽤物理学会春季学術講演会
    • Place of Presentation
      東京工業業大学,東京都
    • Year and Date
      2016-03-19
    • Related Report
      2015 Annual Research Report
  • [Presentation] ダイヤモンド超格子の励起子ダイナミクス2016

    • Author(s)
      梅木拓也, 矢田部 翼, 片山郁文, 南康夫, 渡邊幸志, 武田淳
    • Organizer
      第11回ナノテク交流シンポジウム
    • Place of Presentation
      横浜国大教育文化ホール, 横浜
    • Year and Date
      2016-03-02
    • Related Report
      2015 Annual Research Report
  • [Presentation] ダイヤモンド量子センシングデバイス2016

    • Author(s)
      渡邊 幸志,柏谷 聡,吉澤 明男,馬渡 康徳
    • Organizer
      nano tech 2016 第15回 国際ナノテクノロジー総合展・技術会議
    • Place of Presentation
      東京ビッグサイト,東京都
    • Year and Date
      2016-01-27
    • Related Report
      2015 Annual Research Report
  • [Presentation] Engineered nitrogen-vacancy centers in diamond for quantum2015

    • Author(s)
      早瀬 潤子, 渡邊 幸志,伊藤公平
    • Organizer
      EMN meeting on vacuum electronics
    • Place of Presentation
      New York-New York Hotel & Casino, Las Vegas, USA
    • Year and Date
      2015-11-23
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 微細加工(001) 基板上化学気相成長によるダイヤモンド中窒素空孔中心の生成と位置・配向制御2015

    • Author(s)
      藤田 留士郎, 黒木諒, 渡邊 幸志, 赤羽浩一, 伊藤公平,早瀬 潤子
    • Organizer
      第76回応⽤物理学会秋季学術講演会
    • Place of Presentation
      名古屋国際会議場, 名古屋
    • Year and Date
      2015-09-15
    • Related Report
      2015 Annual Research Report
  • [Presentation] 1分子分析を実現する高感度・高空間分解能量子センサー技術2015

    • Author(s)
      渡邊 幸志
    • Organizer
      VACUUM2015 真空展
    • Place of Presentation
      パシフィコ横浜、横浜
    • Year and Date
      2015-09-08
    • Related Report
      2015 Annual Research Report
  • [Presentation] Diamond growth for nanoscale NMR sensing2015

    • Author(s)
      渡邊 幸志、伊藤公平
    • Organizer
      Diamond Quantum Sensing Workshop 2015
    • Place of Presentation
      かがわ国際会議場、高松市
    • Year and Date
      2015-08-05
    • Related Report
      2015 Annual Research Report
  • [Presentation] Isotopically enriched 12C diamond CVD layers for NanoMRI2015

    • Author(s)
      伊藤公平, 渡邊 幸志, 早瀬 潤
    • Organizer
      5th annual NanoMRI Conference
    • Place of Presentation
      University of Waterloo, Waterloo, Canada
    • Year and Date
      2015-07-27
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Control of position and orientation of nitrogen-vacancy centers in CVD-grown diamond thin film2015

    • Author(s)
      早瀬 潤子, 渡邊 幸志,伊藤公平
    • Organizer
      28th International Conference on Defects in Semiconductors
    • Place of Presentation
      Aalto University, Tampere, Finland
    • Year and Date
      2015-07-27
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Isotope composition dependence of the band-gap energy in diamond2015

    • Author(s)
      渡邊 幸志, 是常 隆, 中島 信一, 斎藤 晋, 鹿田真一
    • Organizer
      NDNC2015
    • Place of Presentation
      Shizuoka GRANSHIP、静岡
    • Year and Date
      2015-05-27
    • Related Report
      2015 Annual Research Report
  • [Presentation] 同位体組成制御によるダイヤモンドのバンドギャップチューニング2014

    • Author(s)
      渡邊幸志、是常隆、中島信一、斎藤晋、鹿田真一
    • Organizer
      第28回ダイヤモンドシンポジウム
    • Place of Presentation
      東京電機大学丹波ホール(東京都)
    • Year and Date
      2014-11-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] 新たなデバイス・材料機能として利用可能な同位体ダイヤモンド2014

    • Author(s)
      渡邊幸志
    • Organizer
      VACUUM2014-真空展
    • Place of Presentation
      東京ビッグサイト (東京都)
    • Year and Date
      2014-10-15 – 2014-10-17
    • Related Report
      2014 Annual Research Report
  • [Presentation] ダイヤモンドNVセンターを用いたナノスケール NMR2014

    • Author(s)
      伊藤公平、早瀬潤子、渡邊幸志、鹿田真一
    • Organizer
      第75回応用物理学会秋季学術講演会 シンポジウム
    • Place of Presentation
      北海道大学(北海道)
    • Year and Date
      2014-09-19
    • Related Report
      2014 Annual Research Report
  • [Presentation] Simultaneous Control of Position, Density, Preferential Orientation of Nitrogen-Vacancy Centers in CVD-Grown Diamond Thin Film on Micropatterned Substrate2014

    • Author(s)
      金子和樹、五味朋寛、藤澤康二、渡邊幸志、梅沢仁、鹿田真一、伊藤公平、早瀬潤子
    • Organizer
      international conference on the physics of semiconductors (ICPS) 2014
    • Place of Presentation
      Austin, Texas, USA
    • Year and Date
      2014-08-12
    • Related Report
      2014 Annual Research Report
  • [Presentation] Isotope composition dependence of near-band edge cathodoluminescence in diamond2014

    • Author(s)
      渡邊幸志、是常隆、中島信一、斎藤晋、鹿田真一
    • Organizer
      BIAMS 12
    • Place of Presentation
      物質材料研究機構(つくば)
    • Year and Date
      2014-06-26
    • Related Report
      2014 Annual Research Report
  • [Patent(Industrial Property Rights)] ダイヤモンドを合成する方法及びプラズマ処理装置2022

    • Inventor(s)
      渡邊幸志、佐藤和行、永塚賢治、木山信道、伊藤公平
    • Industrial Property Rights Holder
      国立研究開発法人産業技術総合研究所、日本高周波株式会社
    • Industrial Property Rights Type
      特許
    • Acquisition Date
      2022
    • Related Report
      Products Report
    • Overseas
  • [Patent(Industrial Property Rights)] ダイヤモンドを合成する方法、マイクロ波発生装置及びプラズマ処理装置2016

    • Inventor(s)
      渡邊幸志、佐藤和行、永塚賢治、木山信道、伊藤公平
    • Industrial Property Rights Holder
      渡邊幸志、佐藤和行、永塚賢治、木山信道、伊藤公平
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-221524
    • Filing Date
      2016-11-14
    • Related Report
      2016 Annual Research Report

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Published: 2014-04-04   Modified: 2023-03-30  

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