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Construction of scientific principle on novel directly applied current sintering and its development toward functional and structural materials design

Research Project

Project/Area Number 26289272
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Material processing/Microstructural control engineering
Research InstitutionOsaka University

Principal Investigator

Mikio Ito  大阪大学, 工学(系)研究科(研究院), 准教授 (00294033)

Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥16,120,000 (Direct Cost: ¥12,400,000、Indirect Cost: ¥3,720,000)
Fiscal Year 2016: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2015: ¥7,410,000 (Direct Cost: ¥5,700,000、Indirect Cost: ¥1,710,000)
Fiscal Year 2014: ¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Keywords通電焼結 / 固化成型 / 反応焼結 / 熱電材料 / 微細組織 / 熱電特性 / 微細組織化 / 低温迅速焼結 / 焼結プロセス / 微細組織制御 / 直接通電焼結 / 緻密化挙動 / 高効率焼結 / 熱電半導体
Outline of Final Research Achievements

In order to investigate the effects of directly applied current sintering on promotion of densification and reaction, synthesis of the thermoelectric Mg2Si sintered body was tried. The densification behaviour, Mg2Si phase formation and the power consumption during sintering and the relative density of the sample were compared to those of a sample sintered by the conventional PCS. When the powders were heated by directly applied current sintering, the densification became larger during heating and the density of a sintered body was also significantly higher as compared to the conventional PCS. Furthermore, directly applied current sintering is found to accelerate the reaction between Mg and Si to form Mg2Si phase. In the case of the thermoelectric β-FeSi2, the similar densification behavior and fine microstructure were obtained by this modified PCS process, indicating that this process is expected to be significantly beneficial for synthesis of thermoelectric materials.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Annual Research Report
  • 2014 Annual Research Report
  • Research Products

    (18 results)

All 2017 2016 2015 2014

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 2 results) Presentation (15 results) (of which Int'l Joint Research: 4 results,  Invited: 9 results)

  • [Journal Article] 直接通電焼結法による熱電材料の作製2016

    • Author(s)
      井藤幹夫
    • Journal Title

      材料の科学と工学

      Volume: 53 Pages: 10-13

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 直接通電焼結法を用いた反応焼結によるMg2Si系熱電材料の合成2015

    • Author(s)
      井藤幹夫,川原賢太
    • Journal Title

      粉体および粉末冶金

      Volume: 62 Pages: 221-227

    • NAID

      130005074107

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Synthesis of Thermoelectric Mg<sub>2</sub>Si by Reactive Sintering Utilizing Directly Applied Current Sintering2015

    • Author(s)
      Mikio Ito and Kenta Kawahara
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 56 Issue: 12 Pages: 2023-2028

    • DOI

      10.2320/matertrans.Y-M2015829

    • NAID

      130005110131

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Densification behavior and thermoelectric properties of β-FeSi2 synthesized by directly applied current sintering2017

    • Author(s)
      Mikio Ito
    • Organizer
      International Conference on Frontiers in Materials Processing Applications, Research and Technology, FiMPART’2017
    • Place of Presentation
      ボルドー,フランス
    • Year and Date
      2017-07-09
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 直接通電による高効率焼結プロセスの開発と熱電変換材料合成への応用2017

    • Author(s)
      井藤幹夫
    • Organizer
      同志社大学先端複合材料研究センターコロキウム講演
    • Place of Presentation
      同志社大学,京田辺市
    • Year and Date
      2017-01-13
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] SPS を用いた直接通電による導電性粉末焼結体の合成2016

    • Author(s)
      井藤幹夫
    • Organizer
      フォーラム「MACKIY」2016
    • Place of Presentation
      長岡技術科学大学,長岡市
    • Year and Date
      2016-12-22
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] β-FeSi2熱電材料合成における直接通電の効果2016

    • Author(s)
      井藤幹夫
    • Organizer
      第21回通電焼結研究会
    • Place of Presentation
      東北大学,仙台市
    • Year and Date
      2016-12-02
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] SPS法における導電性粉末の緻密化挙動に及ぼす直接通電の影響2016

    • Author(s)
      鉄谷尚史,井藤幹夫
    • Organizer
      粉体粉末冶金協会平成28年度秋季大会
    • Place of Presentation
      東北大学,仙台市
    • Year and Date
      2016-11-09
    • Related Report
      2016 Annual Research Report
  • [Presentation] 直接通電焼結法における導電性粉末の緻密化挙動2016

    • Author(s)
      鉄谷尚史,井藤幹夫
    • Organizer
      日本金属学会2016年秋期講演大会
    • Place of Presentation
      大阪大学,豊中市
    • Year and Date
      2016-09-21
    • Related Report
      2016 Annual Research Report
  • [Presentation] Synthesis of β-FeSi2 by directly applied current sintering and its thermoelectric properties2016

    • Author(s)
      Mikio Ito
    • Organizer
      The 8th International Conference on PROCESSIMG & MANUFACTURING OF ADVANCED MATERIALS (THERMEC 2016)
    • Place of Presentation
      グラ-ツ,オーストリア
    • Year and Date
      2016-06-02
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Synthesis of β-FeSi2 by directly applied current sintering and its thermoelectric properties2016

    • Author(s)
      Mikio Ito, Kenta Kawahara
    • Organizer
      International Conference on Processing & Manufacturing of Advanced Materials, THERMEC'2016
    • Place of Presentation
      Graz, Austria
    • Year and Date
      2016-05-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 直接通電焼結法によるβ-FeSi2熱電材料の合成2016

    • Author(s)
      井藤幹夫,荒木敬太
    • Organizer
      粉体粉末冶金協会平成28年度春季大会
    • Place of Presentation
      京都工芸繊維大学,京都市
    • Year and Date
      2016-05-25
    • Related Report
      2016 Annual Research Report
  • [Presentation] 直接通電焼結によるβ-FeSi2熱電材料の合成2016

    • Author(s)
      井藤幹夫
    • Organizer
      粉体粉末冶金協会春季講演大会
    • Place of Presentation
      京都工芸繊維大学,京都市
    • Year and Date
      2016-05-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] SPSを用いた直接通電焼結による導電性粉末の固化成型2016

    • Author(s)
      井藤幹夫
    • Organizer
      日本セラミックス協会年会サテライト講演
    • Place of Presentation
      早稲田大学,東京都
    • Year and Date
      2016-03-14
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] Densification Behaviors of Electrically Conductive Powders Sintered by Directly Applied Current Heating Process2015

    • Author(s)
      Mikio Ito
    • Organizer
      The 11th Pacific Rim Conference of Ceramic Societies, PACRIM 11
    • Place of Presentation
      ICC Jeju, Korea
    • Year and Date
      2015-08-30
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Synthesis of thermoelectric Mg2Si polycrystals by directrly applied current heating2014

    • Author(s)
      Mikio Ito
    • Organizer
      Japan-Russia Workshop on Advanced Materials Synthesis Process and Nanostructure
    • Place of Presentation
      東北大学金属材料研究所(仙台市)
    • Year and Date
      2014-12-05
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] 接通電焼結法を用いた反応焼結によるMg2Si系熱電変換材料の合成2014

    • Author(s)
      川原賢太,井藤幹夫
    • Organizer
      粉体粉末冶金協会秋季講演大会
    • Place of Presentation
      大阪大学(吹田市)
    • Year and Date
      2014-10-30
    • Related Report
      2014 Annual Research Report
  • [Presentation] 直接通電焼結によるMg2Si系熱電変換材料の合成2014

    • Author(s)
      川原賢太,井藤幹夫
    • Organizer
      日本熱電学会学術講演会
    • Place of Presentation
      物質・材料研究機構(つくば市)
    • Year and Date
      2014-09-30
    • Related Report
      2014 Annual Research Report

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Published: 2014-04-04   Modified: 2018-03-22  

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