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Development of a non-evaporable getter pump using a three-dimensional mesh zirconium porous body

Research Project

Project/Area Number 26390070
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Thin film/Surface and interfacial physical properties
Research InstitutionHigh Energy Accelerator Research Organization

Principal Investigator

kikuchi takashi  大学共同利用機関法人高エネルギー加速器研究機構, 物質構造科学研究所, 技師 (30592927)

Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2016: ¥390,000 (Direct Cost: ¥300,000、Indirect Cost: ¥90,000)
Fiscal Year 2015: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2014: ¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Keywords真空 / 真空排気 / 非蒸発ゲッターポンプ / 排気速度測定
Outline of Final Research Achievements

Non-evaporable getter (NEG) pumps are widely used in ultrahigh vacuum because they have a high pumping speed for active residual gases. We constructed a new NEG pump which uses commercial 60 NEG pills (St707, 70 wt% Zr, 24.6 wt% V, and 5.4 wt% Fe). The NEG pills are vertically and radially aligned around a heater to maximize the effective area for pumping. After activation at 400°C for 30 min, the pumping speeds of the NEG pump were measured with the orifice method. Pumping speeds of 140-130, 200-140, 190-130, and 35-17 L/s were estimated for H2, CO, CO2, and N2 gasses, respectively. The performance is comparable with commercial NEG pumps. Next we developed a new NEG coating method using titanium (Ti) vacuum sublimation followed by palladium (Pd) vacuum sublimation. The Pd/Ti thinfilm work as a NEG pump after 6-hours baking with a maximum temperature of 185 °C. Since the Pd/Ti thinfilm is durable against repeated vent-activation cycles, it can be used for various vacuum systems.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (15 results)

All 2016 2015 2014

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Open Access: 2 results,  Acknowledgement Compliant: 1 results) Presentation (11 results) (of which Int'l Joint Research: 3 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Low-cost, high-performance nonevaporable getter pumps using nonevaporable getter pills2016

    • Author(s)
      Hiraku Kodama, Shinya Ohno, Masatoshi Tanaka, Masato Tanaka, Koji K. Okudaira, Kazuhiko Mase, and Takashi Kikuchi
    • Journal Title

      J. Vac. Sci. Technol.A

      Volume: 34 Issue: 5

    • DOI

      10.1116/1.4961050

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Development of Low-Cost, High-Performance Non-Evaporable Getter (NEG) Pumps2016

    • Author(s)
      K. Mase, M. Tanaka, N. Ida, H. Kodama, and T. Kikuchi
    • Journal Title

      AIP Conf. Proc.

      Volume: 1741 Pages: 030015-030015

    • DOI

      10.1063/1.4952838

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 非蒸発ゲッタポンプ用合金膜のスパッタ製膜2016

    • Author(s)
      三嶋東、桑島理樹、中野武雄、大家渓、間瀬一彦、菊地貴司
    • Organizer
      2016年真空・表面科学合同講演会
    • Place of Presentation
      名古屋国際会議場(愛知県名古屋市)
    • Year and Date
      2016-11-29
    • Related Report
      2016 Annual Research Report
  • [Presentation] 新しい非蒸発ゲッター(NEG)コーティングの開発2016

    • Author(s)
      宮澤徹也、間瀬一彦、飛嶋健佑、菊地貴司
    • Organizer
      2016年真空・表面科学合同講演会
    • Place of Presentation
      名古屋国際会議場(愛知県名古屋市)
    • Year and Date
      2016-11-29
    • Related Report
      2016 Annual Research Report
  • [Presentation] Low-Cost, High-Performance Non-Evaporable Getter (NEG) Pumps Using NEG Pills2016

    • Author(s)
      K. Mase, T. Kikuchi, H. Kodama, S. Ohno, M. Tanaka, K. K. Okudaira, M. Tanaka
    • Organizer
      the 9th edition of the Mechanical Engineering Design of Synchrotron Radiation Equipment and Instrumentation (MEDSI) conference
    • Place of Presentation
      Cosmocaixa, Barcelona(Spain)
    • Year and Date
      2016-09-14
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Development of Low-Cost, High-Performance Non-Evaporable Getter (NEG) Pumps for Synchrotron Light Facilities2016

    • Author(s)
      H. Kodama, S. Ohno, M. Tanaka, M. Tanaka, K. K. Okudaira, K. Mase, T. Kikuchi
    • Organizer
      80th IUVSTA Workshop on the Ultra Low Emittance Light Source Vacuum Systems
    • Place of Presentation
      NSRRC, Hsinchu, Taiwan
    • Year and Date
      2016-08-27
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Sputter deposition of Zr-V-Fe (St707) alloy films for NEG applications2016

    • Author(s)
      Azuma Mishima, Naoyuki Hayasaka, Kei Oya, Takeo Nakano, Kazuhiko Mase, Takashi Kikuchi
    • Organizer
      20th International Vacuum Congress (IVC-20)
    • Place of Presentation
      Busan Exhibition & Convention Center (BEXCO), Busan(Koria)
    • Year and Date
      2016-08-24
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 非蒸発ゲッタポンプ用合金膜のスパッタ製膜2016

    • Author(s)
      三嶋東
    • Organizer
      表面技術協会第133回講演大会
    • Place of Presentation
      早稲田大学 西早稲田キャンパス(東京都新宿区大久保3-4-1)
    • Year and Date
      2016-03-22
    • Related Report
      2015 Research-status Report
  • [Presentation] 高性能ピル積層型NEGポンプの開発と排気速度測定2016

    • Author(s)
      菊地貴司
    • Organizer
      第29回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      三井ガーデンホテル柏の葉(千葉県柏市 若柴178-4 柏の葉キャンパス148街区2)
    • Year and Date
      2016-01-10
    • Related Report
      2015 Research-status Report
  • [Presentation] NEG ピルを用いた低コスト高性能NEG ポンプの開発2015

    • Author(s)
      菊地貴司
    • Organizer
      2015年真空・表面科学合同講演会
    • Place of Presentation
      つくば国際会議場(茨城県つくば市竹園2-20-3)
    • Year and Date
      2015-12-03
    • Related Report
      2015 Research-status Report
  • [Presentation] ビームライン、エンドステーションのための低コスト高性能非蒸発ゲッター(NEG)ポンプの開発と排気速度測定2015

    • Author(s)
      菊地貴司
    • Organizer
      第3回物構研サイエンスフェスタ
    • Place of Presentation
      つくば国際会議場(エポカルつくば)
    • Year and Date
      2015-03-17
    • Related Report
      2014 Research-status Report
  • [Presentation] 加速器,ビームライン,エンドステーションのための低コスト高性能非蒸発ゲッター(NEG)ポンプの開発と排気速度測定2015

    • Author(s)
      田中正人,伊田直也,小玉開,菊地貴司,間瀬一彦
    • Organizer
      第28回日本放射光学会年会放射光科学合同シンポジウム
    • Place of Presentation
      立命館大学びわこ・くさつキャンパス
    • Year and Date
      2015-01-12
    • Related Report
      2014 Research-status Report
  • [Presentation] 'In situ removal of carbon contamination from optics, suppression of higher harmonics in the carbon K-edge region, and development of low-cost and high-performance non-evaporable getter (NEG) pumps2014

    • Author(s)
      Kazuhiko Mase, Akio Toyoshima, Takashi Kikuchi, Hirokazu Tanaka, and Kenta Amemiya
    • Organizer
      Mechanical Engineering Design of Synchrotron Radiation Equipment and Instrumentation 2014, 20th - 24th October 2014
    • Place of Presentation
      Hilton on the Park(メルボルン、オーストラリア)
    • Year and Date
      2014-10-21
    • Related Report
      2014 Research-status Report
  • [Patent(Industrial Property Rights)] 非蒸発型ゲッタコーティング部品、容器、製法、装置2016

    • Inventor(s)
      間瀬一彦、菊地貴司
    • Industrial Property Rights Holder
      間瀬一彦、菊地貴司
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-230510
    • Filing Date
      2016-11-28
    • Related Report
      2016 Annual Research Report
  • [Patent(Industrial Property Rights)] 非蒸発型ゲッターポンプ2015

    • Inventor(s)
      間瀬一彦、菊地貴司
    • Industrial Property Rights Holder
      間瀬一彦、菊地貴司
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-233674
    • Filing Date
      2015-11-30
    • Related Report
      2015 Research-status Report

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Published: 2014-04-04   Modified: 2018-03-22  

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