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Development of nuclear resonant scattering diffractometer using synchrotron radiation

Research Project

Project/Area Number 26400338
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Condensed matter physics II
Research InstitutionTeikyo University

Principal Investigator

NAKAMURA Shinichi  帝京大学, 理工学部, 准教授 (80217851)

Co-Investigator(Kenkyū-buntansha) 池田 直  岡山大学, 自然科学研究科, 教授 (00222894)
三井 隆也  国立研究開発法人量子科学技術研究開発機構, 関西光科学研究所 放射光科学研究センター, 上席研究員(定常) (20354988)
Research Collaborator SHIMOMURA Susumu  京都産業大学, 理学部, 教授
KOBAYASHI Yasuhiro  京都大学, 原子炉実験所, 助教
KUROKUZU Masayuki  京都大学, 原子炉実験所, 研究員
FUJIWARA Kosuke  岡山大学, 自然科学研究科
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2016: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2014: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Keywords放射光メスバウアー回折 / 核共鳴散乱 / 結晶サイト選択性 / 複鉄サイト酸化物 / 45度法 / 偏光アナライザー法 / 純核ブラッグ散乱法 / 放射光 / 回折装置 / 鉄酸化物
Outline of Final Research Achievements

At SPring-8 BL11XU, we have developed a nuclear resonant scattering diffractometer (synchrotron Mossbauer diffractometer) by installing θ-2θ goniometer between the nuclear monochromater and a detecting counter. A specific spectrum arising only from a selected γ ray reflection can be measured, which will represent crystal-site-selective Mossbauer spectrum. In order to extract only nuclear resonant scattering, we have established 45 degree-method, polarization analyzer method, and pure nuclear Bragg reflection method. With the use of these three methods, we have succeeded in obtaining crystal-site-selective Mossbauer spectra of typical multi-Fe-site compounds, Fe3O4 and Fe3BO6.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (16 results)

All 2017 2016 2015 Other

All Journal Article (4 results) (of which Peer Reviewed: 4 results,  Acknowledgement Compliant: 2 results) Presentation (11 results) (of which Int'l Joint Research: 2 results,  Invited: 1 results) Remarks (1 results)

  • [Journal Article] Crystal-site-selective spectrum of Fe<sub>3</sub>O<sub>4</sub> obtained by Mössbauer diffraction2017

    • Author(s)
      Shin Nakamura, Takaya Mitsui, Kosuke Fujiwara, Naoshi Ikeda, Masayuki Kurokuzu, Susumu Shimomura
    • Journal Title

      Journal of the Physical Society of Japan

      Volume: 86 Issue: 2 Pages: 0237061-4

    • DOI

      10.7566/jpsj.86.023706

    • NAID

      210000134244

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Crystal-Site-Selective Spectrum of Fe3BO6 by Synchrotron Mossbauer Diffraction with Pure Nuclear Bragg Scattering2017

    • Author(s)
      Shin Nakamura, Takaya Mitsui, Kosuke Fujiwara, Naoshi Ikeda, Masayuki Kurokuzu, Susumu Shimomura
    • Journal Title

      J. Phys. Soc. Jpn.

      Volume: 印刷中

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Development of Mössbauer diffractometer by using nuclear resonant scattering at SPring-8 BL11XU2016

    • Author(s)
      S. Nakamura, T. Mitsui, K. Fujiwara, N. Ikeda, Y. Kobayashi and S. Shimomura
    • Journal Title

      Hyperfine Interactions

      Volume: 237 Issue: 1 Pages: 1571-9

    • DOI

      10.1007/s10751-016-1370-x

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Observation of flux-grown α-Fe<sub>2</sub>O<sub>3</sub> single crystal at the morin transition by <sup>57</sup>Fe synchrotron radiation mössbauer diffraction2016

    • Author(s)
      Takaya Mitsui, Shin Nakamura, Naoshi Ikeda, Kohsuke Hujiwara, Ryo Masuda, Yasuhiro Kobayashi, and Makoto Seto
    • Journal Title

      J. Phys. Soc. Jpn.

      Volume: 85 Issue: 5 Pages: 0547051-5

    • DOI

      10.7566/jpsj.85.054705

    • NAID

      210000133942

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] 純核ブラッグ散乱によるFe3BO6の磁気構造の検証2017

    • Author(s)
      中村真一, 三井隆也,藤原孝将,池田直,下村晋,黒葛真行
    • Organizer
      日本物理学会
    • Place of Presentation
      大阪大学(大阪府豊中市)
    • Year and Date
      2017-03-17
    • Related Report
      2016 Annual Research Report
  • [Presentation] 放射光を用いたFe3O4のメスバウアー回折実験2016

    • Author(s)
      中村真一, 三井隆也,藤原孝将,池田直,下村晋,黒葛真行
    • Organizer
      日本物理学会
    • Place of Presentation
      金沢大学(石川県金沢市)
    • Year and Date
      2016-09-13
    • Related Report
      2016 Annual Research Report
  • [Presentation] Development of Mossbauer diffractometer by using nuclear resonant scattering at SPring-8 BL11XU2016

    • Author(s)
      Shin Nakamura, Takaya Mitsui, Kosuke Fujiwara, Naoshi Ikeda, Yasuhiro Kobayashi and Susumu Shimomura
    • Organizer
      International Conference on Hyperfine Interaction and Their Applications 2016
    • Place of Presentation
      Leuven (Belgium)
    • Year and Date
      2016-07-03
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 鉄欠損を制御したYbFe2O4の電荷秩序と磁気・誘電特性2016

    • Author(s)
      藤原孝将,烏谷友之,古林宏之,福永守,狩野旬,加倉井和久,三井隆也,中村真一,池田直
    • Organizer
      日本物理学会
    • Place of Presentation
      東北学院大学(宮城県仙台市)
    • Year and Date
      2016-03-19
    • Related Report
      2015 Research-status Report
  • [Presentation] 核共鳴散乱回折装置による結晶サイト選択的メスバウアースペクトルの測定II2016

    • Author(s)
      中村真一,三井隆也,藤原孝将,池田直,下村晋
    • Organizer
      日本物理学会
    • Place of Presentation
      東北学院大学(宮城県仙台市)
    • Year and Date
      2016-03-19
    • Related Report
      2015 Research-status Report
  • [Presentation] 放射光を用いたメスバウアー回折スペクトルの測定2016

    • Author(s)
      中村真一
    • Organizer
      第4回先進的放射光メスバウアー分光研究会
    • Place of Presentation
      名古屋工業大学(愛知県名古屋市)
    • Year and Date
      2016-03-03
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] モーリン温度近傍における酸化鉄単結晶の放射光メスバウアー回折2016

    • Author(s)
      三井隆也,中村真一,池田直,藤原孝将
    • Organizer
      JAEA放射光科学シンポジウム2016
    • Place of Presentation
      SPring-8(兵庫県佐用郡)
    • Year and Date
      2016-02-25
    • Related Report
      2015 Research-status Report
  • [Presentation] Trial of the Combined Observation for Mossbauer Spectroscopy and Diffraction in YbFe2O4 with Synchrotron Light Source2015

    • Author(s)
      Kosuke Fujiwara, Shin Nakamura, Takaya Mitsui, Mizuki Miyajima, Tomoyuki Karasudani, Mamoru Fukunaga, Hiroyuki Kobayashi, Tomoko Nagata, Jun Kano, and Naoshi Ikeda
    • Organizer
      第25回日本MRS年次大会国際シンポジウム
    • Place of Presentation
      横浜市開港記念会館(神奈川県横浜市)
    • Year and Date
      2015-12-08
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 核共鳴散乱回折装置による結晶サイト選択的メスバウアースペクトルの測定2015

    • Author(s)
      中村真一,三井隆也,池田直,藤原孝将,小林康浩
    • Organizer
      日本物理学会
    • Place of Presentation
      関西大学(大阪府吹田市)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
  • [Presentation] 核ブラッグモノクロメーターによる放射光メスバウアーγ線回折の研究2015

    • Author(s)
      三井隆也,中村真一,池田直,藤原孝将,小林康浩
    • Organizer
      日本物理学会
    • Place of Presentation
      関西大学(大阪府吹田市)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
  • [Presentation] 酸化鉄化合物のメスバウアー回折実験の試行2015

    • Author(s)
      三井隆也, 池田直,中村真一,藤原孝将
    • Organizer
      PF研究会
    • Place of Presentation
      KEK(茨城県つくば市)
    • Year and Date
      2015-07-27
    • Related Report
      2015 Research-status Report
  • [Remarks] 中村研究室ホームページ

    • URL

      http://www.ase.teikyo-u.ac.jp/faculty/nakamura/

    • Related Report
      2016 Annual Research Report 2015 Research-status Report

URL: 

Published: 2014-04-04   Modified: 2020-05-15  

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