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Construction of novel reaction field for nanoparticle synthesis using both microwave heating and powder handling process

Research Project

Project/Area Number 26420763
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Properties in chemical engineering process/Transfer operation/Unit operation
Research InstitutionHiroshima University

Principal Investigator

Fukui Kunihiro  広島大学, 工学研究院, 教授 (60284163)

Co-Investigator(Kenkyū-buntansha) 吉田 英人  広島大学, 工学研究院, 特任教授 (30116694)
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2016: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2015: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2014: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywordsナノ粒子 / マイクロ波 / 流動層 / 水熱処理 / 電磁界シミュレーション / 粉体ハンドリング / 誘電率 / 熱重量分析 / 電磁界強度分布 / 温度分布 / 粉砕
Outline of Final Research Achievements

As a microwave can heat an object directly and internally, it can induce a selective heating, a heat spot and a superheat. Microwave heating method has been used in various chemical processes. It has been reported that the microwave heating provided the improvement of reaction rate and yield, the appearance of new reaction path, the improvement of selectivity, and so on. However, its precise mechanism has not been sufficiently clarified.
In this study, a new continuous reaction field was constructed by applying the microwave heating for fluidized bed, dry type, wet type pulverization, micro flow channel transportation, respectively. In the newly developed MW-TG device, we clarified the mechanism of thermal and nonthermal effect by microwave heating, and reduced the cost for synthesis of functional nanoparticles, particle complexation and rare metal recovery from waste.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (39 results)

All 2017 2016 2015 2014 Other

All Int'l Joint Research (2 results) Journal Article (14 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 13 results,  Acknowledgement Compliant: 4 results,  Open Access: 1 results) Presentation (23 results) (of which Invited: 2 results)

  • [Int'l Joint Research] Chang Gung University(台湾)

    • Related Report
      2016 Annual Research Report
  • [Int'l Joint Research] Chang-Gung University(台湾)

    • Related Report
      2015 Research-status Report
  • [Journal Article] Synthesis of zeolite from coal fly ash by microwave hydrothermal treatment with pulverization process2017

    • Author(s)
      Fukasawa, T., A.D. Karisma, D. Shibata, A.-N. Huang, K. Fukui
    • Journal Title

      Advanced Powder Technology

      Volume: 28 Issue: 3 Pages: 798-804

    • DOI

      10.1016/j.apt.2016.12.006

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Morphology of woody biomass combustion ash and enrichment of potassium components by particle size classification2017

    • Author(s)
      Maeda, N., T. Katakura, T. Fukasawa, A.-N. Huang, T. Kawano, K. Fukui
    • Journal Title

      Fuel Processing Technology

      Volume: 156 Pages: 1-8

    • DOI

      10.1016/j.fuproc.2016.09.026

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Validation of measured microwave absorption and temperature change for development of a single-mode-type microwave heating thermogravimetry apparatus2017

    • Author(s)
      Karisma, A.D., T. Hamaba, T. Fukasawa, A.-N. Huang, T. Segawa, K. Fukui
    • Journal Title

      Review of Scientific Instruments

      Volume: 88 Issue: 2 Pages: 024101-024101

    • DOI

      10.1063/1.4974813

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Influence of a laminarizer at the inlet on the classification performance of a cyclone separator2017

    • Author(s)
      Huang, A.-N., N. Maeda, D. Shibata, T. Fukasawa, H. Yoshida, H.-P. Kuo, K. Fukui
    • Journal Title

      Separation and Purification Technology

      Volume: 174 Pages: 408-416

    • DOI

      10.1016/j.seppur.2016.09.053

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Influence of the heating method on the particle characteristics of copper oxide powders synthesized from copper nitrate aqueous solutions2016

    • Author(s)
      Segawa, T., T. Fukasawa, A.-N. Huang, Y. Yamada, M. Suzuki, K. Fukui
    • Journal Title

      Chemical Engineering Science

      Volume: 153 Pages: 108-116

    • DOI

      10.1016/j.ces.2016.07.008

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Improvement of particle separation performance by new type hydro cyclone2016

    • Author(s)
      Yamamoto, Tetsuya ; Oshikawa, Takuma ; Yoshida, Hideto ; Fukui, Kunihiro
    • Journal Title

      SEPARATION AND PURIFICATION TECHNOLOGY

      Volume: 158 Pages: 223-229

    • DOI

      10.1016/j.seppur.2015.12.020

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effects of Sintered-Metal Cone Length on Gas-Cyclone Classification Performance2016

    • Author(s)
      Fukasawa, Tomonori ; Sunada, Satoshi ; Shibata, Daiki ; Yoshida, Hideto ; Fukui, Kunihiro
    • Journal Title

      CHEMICAL ENGINEERING & TECHNOLOGY

      Volume: 39 Issue: 3 Pages: 484-490

    • DOI

      10.1002/ceat.201500386

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effect of new blade of centrifugal separator on particle separation performance2016

    • Author(s)
      Yamamoto, Tetsuya ; Kageyama, Takashi ; Yoshida, Hideto ; Fukui, Kunihiro
    • Journal Title

      SEPARATION AND PURIFICATION TECHNOLOGY

      Volume: 162 Pages: 120-126

    • DOI

      10.1016/j.seppur.2016.02.004

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Nickel oxide powder synthesis from aqueous solution of nickel nitrate hexahydrate by a microwave denitration method2015

    • Author(s)
      Segawa, Tomoomi ; Kawaguchi, Koichi ; Ishii, Katsunori ; Suzuki, Masahiro ; Arimitsu, Naoki ; Yoshida, Hideto ; Fukui, Kunihiro
    • Journal Title

      Adavanced Powder Technology

      Volume: 26 Issue: 3 Pages: 983-990

    • DOI

      10.1016/j.apt.2015.04.004

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Development and Evaluation of a Cyclone Type Classifier for Separating Coarse Particles2015

    • Author(s)
      忍足 輝男, 木村 将貴, 山本 一己, 福井 国博, 吉田 英人
    • Journal Title

      Journal of the Society of Powder Technology, Japan

      Volume: 52 Issue: 8 Pages: 435-444

    • DOI

      10.4164/sptj.52.435

    • NAID

      130005098121

    • ISSN
      0386-6157, 1883-7239
    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Improvement of Particle Separation in Louver-type Separator by Use of Numerical Simulation2015

    • Author(s)
      東野 元春, 前田 剛志, 福井 国博, 吉田 英人
    • Journal Title

      Journal of the Society of Powder Technology, Japan

      Volume: 52 Issue: 5 Pages: 252-259

    • DOI

      10.4164/sptj.52.252

    • NAID

      130005072538

    • ISSN
      0386-6157, 1883-7239
    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effect of ring shape attached on upper outlet pipe on fine particle classification of gas-cyclone2015

    • Author(s)
      Wakizono, Yuki, Maeda, Tsuyoshi, Fukui, Kunihiro, Yoshida, Hideto
    • Journal Title

      SEPARATION AND PURIFICATION TECHNOLOGY

      Volume: 141 Pages: 84-93

    • DOI

      10.1016/j.seppur.2014.11.028

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] マイクロ波加熱と粉体プロセスを併用した機能性粒子の合成2015

    • Author(s)
      福井国博
    • Journal Title

      ケミカルエンジニヤリング

      Volume: 60 Pages: 51-57

    • NAID

      40020315372

    • Related Report
      2014 Research-status Report
  • [Journal Article] Effect of Inlet Clean Air and Guide Plate on Fine Particle Classification of Gas-cyclone2014

    • Author(s)
      竹田 尚広, 忍足 輝男, 山本 徹也, 福井 国博, 吉田 英人
    • Journal Title

      Journal of the Society of Powder Technology, Japan

      Volume: 51 Issue: 9 Pages: 614-622

    • DOI

      10.4164/sptj.51.614

    • NAID

      130004691396

    • ISSN
      0386-6157, 1883-7239
    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Presentation] 木質バイオマス発電燃焼灰中のカリウム成分の存在形態とその濃縮法2017

    • Author(s)
      福井 国博・片倉 崇瑛・深澤 智典・Huang An-Ni
    • Organizer
      化学工学会第82年会
    • Place of Presentation
      東京
    • Year and Date
      2017-03-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] The effects of the entrance laminarizer assembly on cyclone performances2017

    • Author(s)
      Huang A.-N.・深澤 智典・吉田 英人・ 福井 国博
    • Organizer
      化学工学会第82年会
    • Place of Presentation
      東京
    • Year and Date
      2017-03-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] The effect of slit secondary flow on the performance of cyclone2016

    • Author(s)
      An-Ni Huang,柴田 大貴,深澤 智典, 吉田 英人,福井 国博
    • Organizer
      第54回粉体に関する討論会
    • Place of Presentation
      北海道
    • Year and Date
      2016-09-12
    • Related Report
      2016 Annual Research Report
  • [Presentation] Development and validity evaluation of a single-mode-type microwave heating thermogravimetry apparatus2016

    • Author(s)
      Achmad Dwitama Karisma,濱場 大周,深澤 智典,An-Ni Huang,福井 国博,瀬川 智臣
    • Organizer
      第54回粉体に関する討論会
    • Place of Presentation
      北海道
    • Year and Date
      2016-09-12
    • Related Report
      2016 Annual Research Report
  • [Presentation] 木質バイオマス発電燃焼灰のカリウム成分の濃縮と循環利用2016

    • Author(s)
      福井 国博,片倉 崇瑛,深澤 智典,An-Ni Huang,吉田 英人
    • Organizer
      第54回粉体に関する討論会
    • Place of Presentation
      北海道
    • Year and Date
      2016-09-12
    • Related Report
      2016 Annual Research Report
  • [Presentation] マイクロ波加熱によるバイオマス発電燃焼灰と石炭灰のK型ゼオライトへの再資源化2016

    • Author(s)
      堀籠 瑛・深澤 智典・ Huang An-Ni・福井 国博
    • Organizer
      化学工学会第48回秋季大会
    • Place of Presentation
      徳島
    • Year and Date
      2016-09-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] 金属硝酸塩混合水溶液のマイクロ波脱硝による金属酸化物粒子の合成2016

    • Author(s)
      福井 国博・中村 陸・深澤 智典・Huang An-Ni・瀬川 智臣・吉田 英人
    • Organizer
      化学工学会第48回秋季大会
    • Place of Presentation
      徳島
    • Year and Date
      2016-09-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] 粒子の凝集特性の差異に着目した振動流動層による成分分離2016

    • Author(s)
      深澤 智典・渡田 寛之・Huang Shih-Yang・平岩 莉歩・ Huang An-Ni・Kuo Hsiu-Po・吉田 英人・福井 国博
    • Organizer
      化学工学会第48回秋季大会
    • Place of Presentation
      徳島
    • Year and Date
      2016-09-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] 電気泳動を利用したサブミクロン粒子の湿式分級2016

    • Author(s)
      深澤 智典・野村 啓介・川幅 康平・福井 国博・吉田 英
    • Organizer
      化学工学会第81年会
    • Place of Presentation
      大阪 関西大学
    • Year and Date
      2016-03-13
    • Related Report
      2015 Research-status Report
  • [Presentation] 金属硝酸塩混合溶液の脱硝反応へのマイクロ波加熱の利用2016

    • Author(s)
      福井 国博・中村 陸・Huang An-Ni・深澤 智典・吉田 英人
    • Organizer
      化学工学会第81年会
    • Place of Presentation
      大阪 関西大学
    • Year and Date
      2016-03-13
    • Related Report
      2015 Research-status Report
  • [Presentation] 振動流動層による凝集粒子の形成に与える粒子物性の影響2016

    • Author(s)
      平岩 莉歩・Huang Shih-Yang・Huang An-Ni・深澤 智典・吉田 英人・福井 国博
    • Organizer
      第18回化学工学会学生発表会(福岡大会)
    • Place of Presentation
      福岡 福岡大学
    • Year and Date
      2016-03-05
    • Related Report
      2015 Research-status Report
  • [Presentation] 金属硝酸塩混合溶液の脱硝反応へのマイクロ波加熱の応用2016

    • Author(s)
      中村 陸・深澤 智典・Huang An-Ni・吉田 英人・福井 国博
    • Organizer
      第18回化学工学会学生発表会(福岡大会)
    • Place of Presentation
      福岡 福岡大学
    • Year and Date
      2016-03-05
    • Related Report
      2015 Research-status Report
  • [Presentation] マイクロ波加熱を利用したバイオマス発電燃焼灰と石炭灰からのK型ゼオライトの合成2016

    • Author(s)
      堀籠 瑛・深澤 智典・Huang An-Ni・吉田 英人・福井 国博
    • Organizer
      第18回化学工学会学生発表会(福岡大会)
    • Place of Presentation
      福岡 福岡大学
    • Year and Date
      2016-03-05
    • Related Report
      2015 Research-status Report
  • [Presentation] 改良型の液体サイクロンによる粒子分離特性2015

    • Author(s)
      吉田 英人・押川 琢磨・福井 国博・深澤 智典
    • Organizer
      化学工学会第47回秋季大会
    • Place of Presentation
      札幌 北海道大学
    • Year and Date
      2015-09-09
    • Related Report
      2015 Research-status Report
  • [Presentation] 木質バイオマス燃焼灰の成分分離に関する研究2015

    • Author(s)
      片倉 崇瑛・深澤 智典・吉田 英人・福井 国博
    • Organizer
      化学工学会第47回秋季大会
    • Place of Presentation
      札幌 北海道大学
    • Year and Date
      2015-09-09
    • Related Report
      2015 Research-status Report
  • [Presentation] 水熱処理による石炭灰とバイオマス燃焼灰のゼオライトへの再資源化2015

    • Author(s)
      福井 国博・津 孝之・深澤 智典・吉田 英人
    • Organizer
      化学工学会第47回秋季大会
    • Place of Presentation
      札幌 北海道大学
    • Year and Date
      2015-09-09
    • Related Report
      2015 Research-status Report
  • [Presentation] 凝集力差を利用した粒子状物質の成分分離法の開発2015

    • Author(s)
      福井 国博・渡田 寛之・吉田 英人
    • Organizer
      化学工学会第80年会
    • Place of Presentation
      東京
    • Year and Date
      2015-03-19 – 2015-03-21
    • Related Report
      2014 Research-status Report
  • [Presentation] 粗大粒子を分離するサイクロン型分級装置の開発と評価2015

    • Author(s)
      忍足 輝男・木村 将貴・山本 一己・福井 国博・吉田 英人
    • Organizer
      化学工学会第80年会
    • Place of Presentation
      東京
    • Year and Date
      2015-03-19 – 2015-03-21
    • Related Report
      2014 Research-status Report
  • [Presentation] CUT SIZE CONTROL OF NOVEL GAS CYCLONE SEPARATOR WITH SINTERED METAL CONE BY CLEAN-AIR INJECTION2015

    • Author(s)
      Kunihiro Fukui, Kenji Jikihara, Satoshi Sunada, Hideto Yoshida
    • Organizer
      FILTECH2015
    • Place of Presentation
      ケルン、 ドイツ
    • Year and Date
      2015-02-24 – 2015-02-26
    • Related Report
      2014 Research-status Report
  • [Presentation] Application of microwave heating to powder synthesis process2014

    • Author(s)
      Kunihiro Fukui
    • Organizer
      Taiwan-Japan Joint Seminar on Particle Technology
    • Place of Presentation
      台北, 台湾
    • Year and Date
      2014-09-22
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] 粉砕を併用したマイクロ波加熱水熱処理によるフライアッシュのゼオライトへの再資源化2014

    • Author(s)
      柴田 大貴・福井 国博・吉田 英人
    • Organizer
      化学工学会第46回秋季大会
    • Place of Presentation
      福岡
    • Year and Date
      2014-09-17 – 2014-09-19
    • Related Report
      2014 Research-status Report
  • [Presentation] 静電場を利用した湿式サブミクロン分級特性2014

    • Author(s)
      吉田 英人・津山 孝行・福井 国博・松沢 光晴
    • Organizer
      化学工学会第46回秋季大会
    • Place of Presentation
      福岡
    • Year and Date
      2014-09-17 – 2014-09-19
    • Related Report
      2014 Research-status Report
  • [Presentation] マイクロ波加熱と粉体プロセスを 併用した機能性粒子の合成2014

    • Author(s)
      福井国博
    • Organizer
      第2回電子デバイス事業化フォーラム
    • Place of Presentation
      福山
    • Year and Date
      2014-08-09
    • Related Report
      2014 Research-status Report
    • Invited

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Published: 2014-04-04   Modified: 2022-02-28  

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