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The development of the dislocation evaluation method by high-intensity, high-resolution pulsed neutron

Research Project

Project/Area Number 26600146
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Quantum beam science
Research InstitutionJapan Atomic Energy Agency

Principal Investigator

HARJO Stefanus  国立研究開発法人日本原子力研究開発機構, 原子力科学研究部門 J-PARCセンター, 研究主幹 (40391263)

Co-Investigator(Renkei-kenkyūsha) KAWASAKI Takuro  国立研究開発法人日本原子力研究開発機構, 原子力科学研究部門 J-PARCセンター, 研究員 (20626361)
Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Fiscal Year 2015: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2014: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Keywords中性子回折 / 飛行時間法 / 転位密度 / 転位配列 / 強度 / その場測定 / 転位 / 金属 / 中性子 / 回折 / 鉄鋼 / 変形
Outline of Final Research Achievements

We challenged to establish a dislocation evaluation technique for the time-of-flight neutron diffraction with high-intensity-resolution, which was needed to elucidate the microstructure effects on deformation mechanisms of metallic materials. In this study, we focused on a lath martensitic steel because it showed large changes in width and shape of diffraction profiles during deformation, and carried out dislocation evaluations using two kinds of methods. The evaluation using the profile separation method based on the peak width gave possibly un-correct results because of ignoring the profile tails. The evaluation using the convolution method of whole profile gave reliable dislocation density results and also information of dislocation arrangement which was related to the large work hardening at the beginning of deformation. The establishment of dislocation evaluation technique led also to the elucidation of microstructure changes associated with deformation of other materials.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (18 results)

All 2016 2015 2014

All Journal Article (2 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 2 results,  Open Access: 2 results,  Acknowledgement Compliant: 2 results) Presentation (15 results) (of which Int'l Joint Research: 5 results,  Invited: 2 results) Book (1 results)

  • [Journal Article] Effect of Prior Martensite on Bainite Transformation in Nanobainite Steel2015

    • Author(s)
      W. Gong, Y. Tomota, Y.H. Su and S.Harjo
    • Journal Title

      Acta Mater.

      Volume: 85 Pages: 243-249

    • DOI

      10.1016/j.actamat.2014.11.029

    • Related Report
      2015 Annual Research Report 2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Dislocation Characteristics of Martensitic Steel Studied by In-Situ Neutron Diffraction Experiment2015

    • Author(s)
      T. Kawasaki, S. Harjo, W. Gong, K. Aizawa, T. Iwahashi, Z. Shi, J. Li, Y. Tomota, T. Ungár
    • Journal Title

      JPS Conference Proceeding

      Volume: 8 Pages: 031009-031009

    • DOI

      10.7566/jpscp.8.031009

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research / Acknowledgement Compliant
  • [Presentation] 二相ステンレス鋼の475℃脆化のミクロ組織特徴解明に向けた中性子ラインプロファイル解析2016

    • Author(s)
      佐藤こずえ、佐藤成男、加藤倫彬、友田陽、Stefanus Harjo、轟秀和、齋藤洋一、我妻和明、鈴木茂
    • Organizer
      日本鉄鋼協会第171回春季講演大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] Dislocation Monitoring during Deformation and New Sample Environment Device for Engineering Studies2016

    • Author(s)
      S. Harjo, T. Kawasaki, Y. Tomota, A. Shibata, N. Tsuji, K. Aizawa
    • Organizer
      The 15th Japan-Korea Meeting on Neutron Science
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2016-01-06
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Unusual Plastic Deformation Behavior in Lath Martensitic Steel Containing High Dislocation Density2015

    • Author(s)
      S. Harjo, T. Kawasaki, Y. Tomota, W. Gong, K. Aizawa
    • Organizer
      8th International Conference on Mechanical Stress Evaluation by Neutron and Synchrotron Radiation
    • Place of Presentation
      Grenoble, France
    • Year and Date
      2015-09-30
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Long Range Internal Stresses in Lath Martensite Steels2015

    • Author(s)
      T. Ungar, P.J. Szabo, S. Harjo
    • Organizer
      8th International Conference on Mechanical Stress Evaluation by Neutron and Synchrotron Radiation
    • Place of Presentation
      Grenoble, France
    • Year and Date
      2015-09-30
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 中性子を用いた工学材料の内部応力及び金属組織の研究2015

    • Author(s)
      ハルヨ ステファヌス、相澤一也、川崎卓郎
    • Organizer
      日本分析化学会 第 64 年会
    • Place of Presentation
      九州大学伊都キャンパス(福岡県福岡市)
    • Year and Date
      2015-09-09
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] Dislocation characteristics in lath martensitic steel by neutron diffraction2015

    • Author(s)
      S. Harjo, T. Kawasaki, W. Gong, Y. Tomota, K. Aizawa
    • Organizer
      6th European Conference on Neutron Scattering
    • Place of Presentation
      Zaragoza, Spain
    • Year and Date
      2015-08-30
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Neutron Diffractometer for Research on Strength of Materials at J-PARC2015

    • Author(s)
      S. Harjo, K. Aizawa, T. Kawasaki
    • Organizer
      17th International Conference on the Strength of Materials
    • Place of Presentation
      Brno, Czech Rep.
    • Year and Date
      2015-08-09
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 中性子回折によるマルテンサイト鋼の変形中の転位組織の変化2015

    • Author(s)
      ハルヨ ステファヌス、川崎卓郎、ゴンウー、友田陽、Z.M. Shi、相澤一也
    • Organizer
      第169回春季講演大会
    • Place of Presentation
      東京大学駒場 I キャンパス(東京都目黒区)
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] その場中性子回折による動的フェライト変態挙動の解析2015

    • Author(s)
      柴田曉伸、朴魯謹、山崎慎太郎、林杉、JAEA ステファヌスハルヨ、辻伸泰
    • Organizer
      第169回春季講演大会
    • Place of Presentation
      東京大学駒場 I キャンパス(東京都目黒区)
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] 焼入れマルテンサイト鋼の塑性変形に伴う転位密度・組織の変化2015

    • Author(s)
      ハルヨ ステファヌス、川崎卓郎、友田陽、ゴン ウー、相澤一也
    • Organizer
      物構研サイエンスフェスタ2014(第6回MLFシンポジウム/第32回PFシンポジウム)
    • Place of Presentation
      つくば国際会議場(茨城県つくば市)
    • Year and Date
      2015-03-17 – 2015-03-19
    • Related Report
      2014 Research-status Report
  • [Presentation] Trials of in-situ materials processing at TAKUMI2014

    • Author(s)
      S. Harjo
    • Organizer
      ESS Science Symposium 2014 “Future Engineering Diffraction Research in Materials Processing and Testing”
    • Place of Presentation
      Vila Lanna (Prague, Czech Republic)
    • Year and Date
      2014-11-17 – 2014-11-18
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] Cryogenic Loading Devices for Materials Science & Engineering Studies at J-PARC2014

    • Author(s)
      S. Harjo , K. Aizawa, T. Kawasaki, T. Nakamoto, T. Hemmi and T. Iwahashi
    • Organizer
      ICANS XXI (International Collaboration on Advanced Neutron Sources)
    • Place of Presentation
      茨城県文化センター(茨城県水戸市)
    • Year and Date
      2014-09-29 – 2014-10-03
    • Related Report
      2014 Research-status Report
  • [Presentation] Dislocation characteristics of martensitic steel studied by in-situ neutron diffraction experiment2014

    • Author(s)
      T. Kawasaki, S. Harjo, W. Gong, K. Aizawa, T. Iwahashi, Y. Tomota and T. Ungar
    • Organizer
      The 2nd International Symposium on Science at J-PARC
    • Place of Presentation
      つくば国際会議場(茨城県つくば市)
    • Year and Date
      2014-07-12 – 2014-07-15
    • Related Report
      2014 Research-status Report
  • [Presentation] Metastable Austenitic Steel Deformation at Low Temperature2014

    • Author(s)
      S. Harjo, T. Kawasaki, W. Gong, K. Aizawa and T. Iwahashi
    • Organizer
      The 2nd International Symposium on Science at J-PARC
    • Place of Presentation
      つくば国際会議場(茨城県つくば市)
    • Year and Date
      2014-07-12 – 2014-07-15
    • Related Report
      2014 Research-status Report
  • [Presentation] Cyclic Tension-Compression Loading of Ductile Cast Irons2014

    • Author(s)
      S. Harjo, S. Kubota, Y. Tomota and K. Aizawa
    • Organizer
      9th European Conference on Residual Stresses
    • Place of Presentation
      University of Technology of Troyes, Troyes, France
    • Year and Date
      2014-07-07 – 2014-07-10
    • Related Report
      2014 Research-status Report
  • [Book] In-situ Studies with Photons, Neutrons and Electrons II2014

    • Author(s)
      YH. Su, Y. Tomota, S. Harjo, J. Suzuki and Y.Adachi
    • Total Pages
      259
    • Publisher
      Springer
    • Related Report
      2014 Research-status Report

URL: 

Published: 2014-04-04   Modified: 2017-05-10  

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