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Proposal of metallic-compound creating process

Research Project

Project/Area Number 26630013
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Research InstitutionKeio University

Principal Investigator

KOMOTORI Jun  慶應義塾大学, 理工学部, 教授 (30225586)

Co-Investigator(Kenkyū-buntansha) MURAI Kazue  慶應義塾大学, 理工学部, 助教 (70645944)
Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2014: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords微粒子ピーニング / 高周波誘導加熱 / 表面改質 / 金属間化合物
Outline of Final Research Achievements

To form a Ni-Al intermetallic compound layer on a carbon steel surface, AIH-FPP was carried out at 900℃ in argon atmosphere with a Ni and Al particle milled by means of planetary ball mills. The treated surface was analyzed using SEM, EDX and an XRD. Oxidation test was carried out at 900℃ for 100 hours. Results showed that the Ni-Al intermetallic compound layer with a thickness of 200 μm was formed in the case of the specimen treated by the aluminum rich shot particles; the ratio of Ni to Al was 1 to 4 at.%. This was because (i) melted Al particles reduced the melting point of Ni particles and Fe substrate, and (ii) partially melted area promoted a combustion synthesis reaction between Ni and Al, resulting in forming the Ni-Al intermetallic compound layer. The AIH-FPP treated surface showed a higher oxidation resistance than that of the un-treated specimen. This was because Al2O3 continually created from the Ni-Al intermetallic compound layer protected the steel substrate.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (8 results)

All 2016 2015 2014

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (6 results) (of which Int'l Joint Research: 1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] 雰囲気制御IH-FPP(AIH-FPP)を用いたFe-Al金属間化合物の形成とその応用2015

    • Author(s)
      亀山雄高,竹嶋隼人,小茂鳥潤,村澤功基
    • Journal Title

      日本金属学会誌

      Volume: Vol.79, No.9 Pages: 452-460

    • NAID

      130005095941

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] AIH-FPP処理による炭素鋼表面のTi-Al金属間化合物化とその性能評価2016

    • Author(s)
      齋藤周也,小茂鳥潤,深沢剣吾,三阪佳孝,川嵜一博
    • Organizer
      第158回日本金属学会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都・葛飾区)
    • Year and Date
      2016-03-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] Evaluation of Carbon Steel Surface Treated by AIH-FPP using Ti and Al Particles2015

    • Author(s)
      Shuya Saito, Kouya Suzuki, Jun Komotori, Kengo Fukazawa, Yoshitaka Misaka, Kazuhiro Kawasaki,
    • Organizer
      42nd International Conference on Metallurgical Coatings and Thin Films
    • Place of Presentation
      San Diego(USA)
    • Year and Date
      2015-04-20
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] AIH-FPP による炭素鋼表面の金属間化合物とそれによる耐酸化性向上2015

    • Author(s)
      鈴木広野,齋藤周也,小茂鳥 潤,深沢剣吾,三阪佳孝,川嵜一博
    • Organizer
      日本金属学会第156回春期講演大会
    • Place of Presentation
      東京大学駒場 I キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] 雰囲気制御IH-FPP 処理によるTi-Al 金属間化合物被膜創製プロセスの検討2015

    • Author(s)
      齋藤 周也,鈴木 広野,小茂鳥 潤,深沢 剣吾,三阪 佳孝,川崎 一博
    • Organizer
      日本金属学会第156回春期講演大会
    • Place of Presentation
      東京大学駒場 I キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] Cr/高速度工具鋼混合粒子を用いた真空置換AIH-FPP 処理による炭素鋼の表面改質2015

    • Author(s)
      太田 俊平,村井一恵,小茂鳥潤,深沢剣吾,三阪佳孝,川嵜一博
    • Organizer
      日本金属学会第156回春期講演大会
    • Place of Presentation
      東京大学駒場 I キャンパス
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Research-status Report
  • [Presentation] AIH-FPPを利用した炭素鋼表面へのNi-Al金属間化合物創製プロセスの検討2014

    • Author(s)
      鈴木広野,亀山雄高,小茂鳥潤
    • Organizer
      日本金属学会第155回秋期講演大会
    • Place of Presentation
      名古屋大学東山キャンパス
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Research-status Report
  • [Patent(Industrial Property Rights)] 表面処理方法及び金属間化合物被膜付き金属製部材2015

    • Inventor(s)
      鈴木広野、齋藤周也、小茂鳥潤、深沢剣吾、三阪佳孝、川嵜一博
    • Industrial Property Rights Holder
      学校法人慶應義塾、高周波熱錬株行会社
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-037046
    • Filing Date
      2015-02-26
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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