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Specimen size dependence of strength and fracture toughness of extrinsically brittle metals

Research Project

Project/Area Number 26630347
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionKyoto University

Principal Investigator

Okamoto Norihiko  京都大学, 工学(系)研究科(研究院), 助教 (60505692)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2014: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Keywords微小寸法試料 / サイズ依存性 / 集束イオンビーム(FIB)法 / ナノ結晶 / 超微細粒多結晶 / 銅 / パルス電析法 / 脆性材料 / 集束イオンビーム / 破壊靭性 / スケールファクター
Outline of Final Research Achievements

Although most pure metals such as aluminum, copper and so on are intrinsically ductile, they are known to become brittle when the crystal grain size is considerably reduced. It had remained an open question if these extrinsically brittle metals exhibit any specimen size dependence of strength and fracture toughness. In the present research, we have performed compression tests and bending tests for micrometer-sized specimens of nanocrystalline copper fabricated by pulsed electrodeposition. We have revealed that when the crystal grain size is reduced down to 34 nm, where the dislocation motion is difficult, the specimen size dependence of strength disappears in contrast to the coarse grained polycrystalline copper, and that the brittle fracture behavior, which is observed when the bulk nanocrystalline copper is bent, disappears and turns to be ductile when the specimen size is reduced to the micrometer size.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (10 results)

All 2015 2014 Other

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Acknowledgement Compliant: 1 results) Presentation (6 results) (of which Int'l Joint Research: 1 results,  Invited: 1 results) Remarks (1 results)

  • [Journal Article] Effects of Alloying Elements on the Temperature Dependence of Yield Stress in L12-Co3(Al,W)2015

    • Author(s)
      Zhenghao M. T. Chin, Norihiko L. Okamoto and Haruyuki Inui
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1760 Pages: 1-6

    • DOI

      10.1557/opl.2015.161

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Factors Controlling the Temperature Dependence of Yield Stress in L12-Ordered Intermetallic Compounds2015

    • Author(s)
      Haruyuki Inui and Norihiko L. Okamoto
    • Journal Title

      Materials Research Society Symposium Proceedings

      Volume: 1760 Pages: 1-11

    • DOI

      10.1557/opl.2015.27

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Specimen- and Grain-Size Dependence of Compression Deformation Behavior in Nanocrystalline Copper2014

    • Author(s)
      Norihiko L. Okamoto, Daisuke Kashioka, Tetsuji Hiratoh, and Haruyuki Inui
    • Journal Title

      International Journal of Plasticity

      Volume: 56 Pages: 173-183

    • DOI

      10.1016/j.ijplas.2013.12.003

    • NAID

      120005434967

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Micropillar Compression of Single Crystals of L12-Co3(Al,W)2015

    • Author(s)
      Zhenghao M. T. Chin, Norihiko L. Okamoto and Haruyuki Inui
    • Organizer
      Intermetallics Conference 2015
    • Place of Presentation
      Kloster Banz, Germary
    • Year and Date
      2015-09-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Fe-Zn系金属間化合物中のZn12二十面体クラスターの配列と塑性変形時の役割2015

    • Author(s)
      岡本範彦, 井元雅弘, 乾晴行
    • Organizer
      日本金属学会第157回大会
    • Place of Presentation
      九州大学
    • Year and Date
      2015-09-17
    • Related Report
      2015 Annual Research Report
  • [Presentation] Temperature Dependence of Yield Stress in L12-Co3(Al,W) Alloyed with Quaternary Elements2014

    • Author(s)
      Zhenghao M. T. Chin, Norihiko L. Okamoto and Haruyuki Inui
    • Organizer
      Materials Research Society Fall Meeting
    • Place of Presentation
      Boston, MA
    • Year and Date
      2014-11-30 – 2014-12-05
    • Related Report
      2014 Research-status Report
  • [Presentation] Factors Controlling the Temperature Dependence of Yield Stress in L12-Ordered Intermetallic Compounds2014

    • Author(s)
      Haruyuki Inui and Norihiko L. Okamoto
    • Organizer
      Materials Research Society Fall Meeting
    • Place of Presentation
      Boston, MA5
    • Year and Date
      2014-11-30 – 2014-12-05
    • Related Report
      2014 Research-status Report
  • [Presentation] Anisotropy in Elastic Properties and Thermal Expansion of Single Crystals of Transition-Metal Diborides with the AlB2-Type Structure2014

    • Author(s)
      Norihiko L. Okamoto, Katsushi Tanaka, Haruyuki Inui, and Shigeki Otani
    • Organizer
      International Symposium on Boron, Borides and Related Materials
    • Place of Presentation
      Hawai’i, USA
    • Year and Date
      2014-08-31 – 2014-09-05
    • Related Report
      2014 Research-status Report
  • [Presentation] Mechanical Properties of Co-Based Alloys with L12 Cuboidal Precipitates2014

    • Author(s)
      Norihiko L. Okamoto, and Haruyuki Inui
    • Organizer
      EUROSUPERALLOYS2014
    • Place of Presentation
      Giens, France
    • Year and Date
      2014-05-12 – 2014-05-16
    • Related Report
      2014 Research-status Report
    • Invited
  • [Remarks] 研究代表者のホームページ

    • URL

      http://nlokamoto.web.fc2.com/

    • Related Report
      2015 Annual Research Report 2014 Research-status Report

URL: 

Published: 2014-04-04   Modified: 2017-05-10  

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