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Fabrication of partially stabilized austenitic steel with high strength and performance against hydrogen embrittlement

Research Project

Project/Area Number 26630352
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionKyushu University

Principal Investigator

Takaki Setsuo  九州大学, 工学(系)研究科(研究院), 教授 (90150490)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2014: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords鉄鋼材料 / 耐水素脆化特性 / 加工誘起マルテンサイト変態 / 固相窒素吸収処理
Outline of Final Research Achievements

In this study, the stabilization of surface austenite layer was attempted by applying the solid nitrogen absorption treatment in order to realize the high strength and performance against hydrogen embrittlement in a conventional austenitic stainless steel (SUS 304). As a result, it was found that 1) the austenite phase containing 0.4% or more is stable even after 60% cold working, 2) the stable austenite layer plays a role to retard the hydrogen absorption from the surface, 3) the center potion of material has been strengthened to a high level by the deformation induced martensitic transformation. As expected in the initial research plan, a high strength stainless steel with high performance against hydrogen embrittlement could be fabricated by applying the solid nitrogen absorption treatment to SUS 304.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (17 results)

All 2016 2015 2014

All Journal Article (6 results) (of which Int'l Joint Research: 4 results,  Peer Reviewed: 6 results,  Open Access: 3 results,  Acknowledgement Compliant: 1 results) Presentation (11 results) (of which Int'l Joint Research: 5 results)

  • [Journal Article] Critical grain size to limit the hydrogen-induced ductility drop in a metastable austenitic steel2015

    • Author(s)
      Macadre, A., Nakada, N., Tsuchiyama, T. and Takaki, S.
    • Journal Title

      International Journal of Hydrogen Energy

      Volume: 40 Issue: 33 Pages: 10697-10703

    • DOI

      10.1016/j.ijhydene.2015.06.111

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Difference in martensitic transformation behavior between carbon- and nitrogen-added metastable asutenitic stainless steels2015

    • Author(s)
      Masumura, T., Nakada, N., Tsuchiyama, T., Takaki, S., Koyano, T., Adachi, K.
    • Journal Title

      Proceeding of PTM2015

      Volume: 1 Pages: 591-592

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effects of carbon and nitrogen additions on mechanical stability of metastable austenitic stainless steel2015

    • Author(s)
      Masumura, T.,Fujino, K., Nakada, N., Tsuchiyama, T., Takaki, S., Adachi, K.
    • Journal Title

      Proceeding of Asia Steel International Conference 2015

      Volume: 1 Pages: 96-97

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effect of grain size and solute hydrogen on the tensile properties and fracture behaviour of an austenitic steel2015

    • Author(s)
      Macadre, A., Nakada, N., Tsuchiyama, T. and Takaki, S.
    • Journal Title

      Proceeding of Asia Steel International Conference 2015

      Volume: 1 Pages: 542-543

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Suppression of Hydrogen Embrittlement by Formation of Stable Austenite-Layer in Metastable Austenitic Stainless Steel2014

    • Author(s)
      Tsuchiyama, T., Tsuboi, K., Iwanaga, S., Masumura, T., Macadre, A., Nakada, N. and Takaki, S.
    • Journal Title

      Scripta Materialia

      Volume: 90-91 Pages: 14-16

    • DOI

      10.1016/j.scriptamat.2014.07.005

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Thermodynamics and Kinetics of Solution Nitriding2014

    • Author(s)
      N. Nakada, K.Tsuboi, T.Onomoto, T.Tsuchiyama, S.Takaki, G.Inden
    • Journal Title

      CALPHAD: Computer Coupling of Phase Diagrams and Thermochemistry

      Volume: 47 Pages: 168-173

    • DOI

      10.1016/j.calphad.2014.09.006

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] 炭素・窒素を含有した準安定オーステナイト鋼における機械的安定度と変形温度の関係2016

    • Author(s)
      増村拓朗、藤野昂平、土山聡宏、高木節雄、安達和彦
    • Organizer
      日本鉄鋼協会 第171回春季講演大会
    • Place of Presentation
      東京理科大
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] Effects of carbon and nitrogen additions on mechanical stability of metastable austenitic stainless steel2015

    • Author(s)
      Takuro Masumura, Kohei Fujino, Nobuo Nakada, Toshihiro Tsuchiyama, Setsuo Takaki and Kazuhiko Adachi
    • Organizer
      Asia Steel 2015
    • Place of Presentation
      パシフィコ横浜
    • Year and Date
      2015-10-05
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of grain size and solute hydrogen on the tensile properties and fracture behavior of an austenitic steel2015

    • Author(s)
      A. Macadre, N. Nakada, T. Tsuchiyama, S. Takaki
    • Organizer
      Asia Steel 2015
    • Place of Presentation
      パシフィコ横浜
    • Year and Date
      2015-10-05
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Improvement of resistance to hydrogen by ultra-grain refinement in a metastable austenitic steel2015

    • Author(s)
      A. Macadre, N. Nakada, T. Tsuchiyama, S. Takaki
    • Organizer
      European Congress and Exhibition on advanced materials and processes (EUROMAT 2015)
    • Place of Presentation
      Warsaw University
    • Year and Date
      2015-09-20
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 安定オーステナイト系ステンレス鋼の水素侵入挙動に及ぼす転位の影響2015

    • Author(s)
      坂巻嘉明、赤間大地、土山聡宏、高木節雄
    • Organizer
      日本鉄鋼協会 第170回秋季講演大会
    • Place of Presentation
      九州大学
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 準安定オーステナイト系ステンレス鋼のMd30に及ぼす炭素および窒素の影響2015

    • Author(s)
      藤野昂平、増村拓朗、土山聡宏、高木節雄、中田伸生、安達和彦
    • Organizer
      日本鉄鋼協会 第170回秋季講演大会
    • Place of Presentation
      九州大学
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] 準安定オーステナイト系ステンレス鋼の加工硬化挙動に及ぼす炭素および窒素の影響2015

    • Author(s)
      増村拓朗、藤野昂平、土山聡宏、高木節雄、中田伸生、安達和彦
    • Organizer
      日本鉄鋼協会 第170回秋季講演大会
    • Place of Presentation
      九州大学
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
  • [Presentation] Evolution of fracture mode for varying grain sizes in a hydrogen-charged metastable austenitic steel2015

    • Author(s)
      A. Macadre, N. Nakada, T. Tsuchiyama, S. Takaki
    • Organizer
      Crack Paths 2015
    • Place of Presentation
      Palazzo Tassoni
    • Year and Date
      2015-09-16
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Difference in martensitic transformation behavior between carbon- and nitrogen-added metastable austenitic stainless steels2015

    • Author(s)
      Takuro Masumura, Nobuo Nakada, Toshihiro Tsuchiyama, Setsuo Takaki, Tamotsu Koyano and Kazuhiko Adachi
    • Organizer
      International Conference on Solid-Solid Phase Transformations in Inorganic Materials (PTM 2015)
    • Place of Presentation
      Westin Whistler Resort & Spa
    • Year and Date
      2015-06-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 安定オーステナイト系ステンレス鋼の水素侵入挙動に及ぼす予歪の影響2015

    • Author(s)
      坂巻嘉明、赤間大地、土山聡宏、高木節雄
    • Organizer
      第79回日本熱処理技術協会講演大会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2015-06-04
    • Related Report
      2015 Annual Research Report
  • [Presentation] 安定オーステナイト系ステンレス鋼の水素侵入挙動に及ぼす低歪速度変形の影響2014

    • Author(s)
      坂巻嘉明・岩永修一・中田伸生・土山聡宏・高木節雄
    • Organizer
      平成26年度合同学術講演会 日本金属学会九州支部 日本鉄鋼協会九州支部 軽金属学会九州支部
    • Place of Presentation
      九州大学
    • Year and Date
      2014-06-07
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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