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In-situ observation of the graphene through the thermal decomposition of silicon carbide by shcrotron surface x-ray difraction

Research Project

Project/Area Number 26790045
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Crystal engineering
Research InstitutionKwansei Gakuin University

Principal Investigator

YOSHIDA MASAHIRO  関西学院大学, 理工学研究科, 博士研究員 (80634500)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Keywords表面X線回折 / グラフェン / シリコンカーバイド / その場観察 / 放射光X線 / 結晶成長
Outline of Final Research Achievements

I have established the in-situ observation method by synchrotron surface x-ray diffraction in order to investigate surface/interface structures during the grphene growth through the thermal decomposition of silicon carbide(SiC). Firstly, I identified that Bragg peaks caused by SiC and/or graphene and a superstructure reflection caused by buffer layer lie at geometric positions. Subsequently, I performed the in-situ observation of the superstrucure reflection combining the custom-designed furnace, multi-axes diffractometer and two-dimensional detector PILATUS. I considered that obtained temperature changes of the peak profile were explained based on the growth model widely supported. As a result, I have successfully proved the practicality of the established in-situ method.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (4 results)

All 2016 2015 2014

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (3 results) (of which Int'l Joint Research: 1 results)

  • [Journal Article] Development of the compact furnace for the in-situ observation under ultra-high temperature by synchrotron x-ray surface diffraction2016

    • Author(s)
      M. Yoshida, Y. Kutsuma, D. Dohjima, K. Ohwadad,T.Inami, N. Ohtani, T. Kaneko and J. Mizuki
    • Journal Title

      Materials Science Forum

      Volume: 858 Pages: 505-508

    • DOI

      10.4028/www.scientific.net/msf.858.505

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Presentation] In-situ observation of the SiC surface during thermal decomposition by synchrotron x-ray surface diffraction2015

    • Author(s)
      Masahiro Yoshida, Yasunori Kutsuma, Daichi Dohjima, Kenji Ohwada, Toshiya Inami, Noboru Ohtani, Tadaaki Kaneko and Jun’ichiro Mizuki
    • Organizer
      16th Internaitonal Conference of Silicon Carbide and Related Materials
    • Place of Presentation
      Giardini Naxos, Italy
    • Year and Date
      2015-10-04
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放射光X線回折によるSiC熱分解表面のその場観察法の開発2015

    • Author(s)
      吉田雅洋, 河邉文哉, 久津間保徳, 堂島大地, 重政英史, 大和田謙二, 稲見俊哉, 玉井尚登, 大谷昇, 金子忠昭, 水木純一郎
    • Organizer
      第62回応用物理学会春季学術講演会
    • Place of Presentation
      東海大学 (神奈川県)
    • Year and Date
      2015-03-11 – 2015-03-14
    • Related Report
      2014 Research-status Report
  • [Presentation] Development of in-situ observation method of the graphene growth by sychrotron x-ray surface diffraction2014

    • Author(s)
      M.Yoshida, F. Kawabe, Y. Kutsuma, D. Dohjima, H. Shigemasa, K. Ohwada, N. Tamai, N. Ohtani, T. Kaneko and J. Mizuki
    • Organizer
      European Conference on Silicon Carbide and Related Materials 2014
    • Place of Presentation
      グルノーブル(フランス)
    • Year and Date
      2014-09-21 – 2014-09-25
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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