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Development of Low-Temperature Solid-State Bonding Process for SiC-Fiber-Reinforced SiC-Matrix Composites

Research Project

Project/Area Number 26820306
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Composite materials/Surface and interface engineering
Research InstitutionOsaka University

Principal Investigator

Kohama Kazuyuki  大阪大学, 接合科学研究所, 助教 (00710287)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2014: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords接合 / 炭化ケイ素 / 粉体 / ペースト / 焼結 / 放電プラズマ焼結装置 / Siペースト / 微粒子 / 融点降下 / 再溶融温度 / SiC
Outline of Final Research Achievements

This study aims at the development of low-temperature bonding process to obtain joint structure of SiC-fiber-reinforced SiC-matrix composites (SiC-CMCs), and paste-like Si powder is selected as the insert material to reduce bonding temperature to less than 1400°C and to maintain high-temperature reliability of the joints. SiC sintered materials were used for fundamental investigation, and the paste-like Si powder was inserted at the bonding interface. The SiC sintered materials were successfully bonded at 1300°C due to formation of the insert layer consisting of sintered Si powder. The joint strength increased as the densified sintered Si powder was obtained. The densification behavior in the sintered Si powder correlated with the median diameter and volume fraction of particles in the paste-like Si powder was systematically investigated. Based on these results, this process was considered to be applicable to SiC-CMCs.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (10 results)

All 2016 2015 2014

All Presentation (10 results) (of which Int'l Joint Research: 1 results,  Invited: 1 results)

  • [Presentation] Siペーストの粒子体積分率制御によるSiC低温接合と接合強度向上2016

    • Author(s)
      小濱和之、寺田俊一、伊藤和博、桐原聡秀
    • Organizer
      (公社)日本金属学会2016年春期大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京)
    • Year and Date
      2016-03-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] 接合部微細組織制御による低温接合2016

    • Author(s)
      小濱和之
    • Organizer
      (一社)溶接学会若手会員の会 溶接・接合若手研究会
    • Place of Presentation
      琵琶湖畔おごと温泉木もれび(滋賀県・大津市)
    • Year and Date
      2016-03-09
    • Related Report
      2015 Annual Research Report
  • [Presentation] 接合部の微細組織制御による固相拡散接合温度の低温化2015

    • Author(s)
      小濱和之
    • Organizer
      (一社)溶接学会四国支部・(一社)溶接学会若手会員の会共催研究会
    • Place of Presentation
      川田工業(株)四国工場(香川県・多度津町)
    • Year and Date
      2015-11-12
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] Siペースト中間材の初期粒子径分布制御によるSiCの低温・高強度接合2015

    • Author(s)
      寺田俊一、小濱和之、伊藤和博、桐原聡秀
    • Organizer
      (一社)溶接学会平成27年度秋季全国大会
    • Place of Presentation
      北海道科学大学(北海道・札幌市)
    • Year and Date
      2015-09-04
    • Related Report
      2015 Annual Research Report
  • [Presentation] Formation of ZrC-ZrC Joints Using Spark Plasma Sintering System2015

    • Author(s)
      Kazuyuki Kohama, Kazuhiro Ito
    • Organizer
      68th Annual Assembly of International Institute of Welding
    • Place of Presentation
      Helsinki (Finland)
    • Year and Date
      2015-07-01
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Siペースト塗布による炭化ケイ素の低温接合2015

    • Author(s)
      小濱和之、伊藤和博、寺田俊一、桐原聡秀
    • Organizer
      (一社)溶接学会平成27年度春季全国大会
    • Place of Presentation
      学術総合センター2階一橋大学一橋講堂(東京)
    • Year and Date
      2015-04-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] 放電プラズマ焼結装置を用いた炭化ジルコニウムの直接固相接合2015

    • Author(s)
      小濱和之、伊藤和博
    • Organizer
      溶接学会
    • Place of Presentation
      東京ビッグサイト(東京都)
    • Year and Date
      2015-04-24
    • Related Report
      2014 Research-status Report
  • [Presentation] Siペースト塗布による炭化ケイ素の低温接合2015

    • Author(s)
      小濱和之、伊藤和博、寺田俊一、桐原聡秀
    • Organizer
      溶接学会
    • Place of Presentation
      学術総合センター(東京都)
    • Year and Date
      2015-04-24
    • Related Report
      2014 Research-status Report
  • [Presentation] Siペースト中間材を用いたSiC接合温度の低温化2015

    • Author(s)
      小濱和之、伊藤和博、寺田俊一、桐原聡秀
    • Organizer
      日本金属学会
    • Place of Presentation
      東京大学駒場IIキャンパス(東京大学)
    • Year and Date
      2015-03-18
    • Related Report
      2014 Research-status Report
  • [Presentation] ZrC-ZrC Bonding Using Spark Plasma Sintering System2014

    • Author(s)
      Kazuyuki KOHAMA, Kazuhiro ITO
    • Organizer
      The International Symposium on Visualization in Joining & Welding Science through Advanced Measurements and Simulation (Visual-JW 2014)
    • Place of Presentation
      ホテル阪急エキスポパーク(大阪府)
    • Year and Date
      2014-11-28
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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