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Clarification of anomalous fatigue softening in biomedical Ti-Nb alloys

Research Project

Project/Area Number 26820315
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionOsaka University

Principal Investigator

Todai Mitsuharu  大阪大学, 工学(系)研究科(研究院), 助教 (10610800)

Co-Investigator(Renkei-kenkyūsha) NAKANO TAKAYOSHI  大阪大学, 大学院工学研究科, 教授 (30243182)
Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2015: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2014: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords生体材料 / Ti合金 / ω相変態 / 単結晶 / 疲労試験 / バリアント / 構造・機能材料 / 結晶工学 / 結晶成長 / 格子欠陥 / β型Ti-Nb合金 / 転位運動
Outline of Final Research Achievements

The cyclic deformation behavior and dislocation microstructure in Ti-xNb single crystals were investigated by a fatigue test and the subsequent observation of transmission electron microscopy (TEM), respectively.
An anomalous softening appears in the Ti-34Nb crystal fatigued at a total strain amplitude of Δε = 0.9% and number of cycles, number of cycle over 200 accompanied by the precipitation of ω phase. In contrast, neither fatigue softening nor precipitation of ω phase was found out in the Ti-40Nb crystal. It is concluded that the fatigue softening in the Ti-34Nb crystal is closely related to the stability of β matrix and the precipitation of ω phase induced by dislocations.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (34 results)

All 2016 2015 2014 Other

All Journal Article (5 results) (of which Peer Reviewed: 5 results,  Acknowledgement Compliant: 3 results) Presentation (26 results) (of which Invited: 2 results) Book (1 results) Remarks (2 results)

  • [Journal Article] Microstructure and fracture toughness in boron added NbSi2(C40)/MoSi2(C11b) duplex crystals2016

    • Author(s)
      M. Todai, K. Hagihara, K. Kishida, H. Inui, T. Nakano
    • Journal Title

      Scripta Materiali

      Volume: 113 Pages: 236-240

    • DOI

      10.1016/j.scriptamat.2015.11.004

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Development of Single Crystalline Bone Plate with Low Young’s Modulus Using Beta-type Ti-15Mo-5Zr-3Al Alloy2015

    • Author(s)
      當代光陽,萩原幸司,石本卓也,山本憲吾,中野貴由
    • Journal Title

      Tetsu-to-Hagane

      Volume: 101 Issue: 9 Pages: 501-505

    • DOI

      10.2355/tetsutohagane.TETSU-2015-044

    • NAID

      130005094601

    • ISSN
      0021-1575, 1883-2954
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of phase stability on some physical and mechanical properties in β-Ti single crystal for biomedical applications2014

    • Author(s)
      M. Todai, P. Wang, K. Fukunaga and T. Nakano
    • Journal Title

      Materials Science Forum

      Volume: 783-786 Pages: 1372-1376

    • DOI

      10.4028/www.scientific.net/msf.783-786.1372

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Temperature dependence of diffuse satellites in Ti-(50-x)Pd-xFe (14≦x≦20, at.%) alloys2014

    • Author(s)
      M. Todai, T. Fukuda and T. Kakeshita
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 615 Pages: 1047-1051

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Control of Oriented Extracellular Matrix Similar to Anisotropic Bone Microstructure2014

    • Author(s)
      T. Nakano, A. Matsugaki, T. Ishimoto, M. Todai, A. Serizawa, R. Suetoshi, Y. Noyama and W. Fujitani
    • Journal Title

      Materials Science Forum

      Volume: 783-786 Pages: 72-77

    • DOI

      10.4028/www.scientific.net/msf.783-786.72

    • Related Report
      2014 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Development of Zr based biomedical alloys with low Young’s modulus2016

    • Author(s)
      M. Todai, K. Fukunaga, T. Nakano
    • Organizer
      9th Pacific Rim International Conference on Advanced Materials and Processing (PRICM9)
    • Place of Presentation
      京都国際会議場(京都府京都市)
    • Year and Date
      2016-08-01
    • Related Report
      2015 Annual Research Report
  • [Presentation] Effect of boron addition for microstructure and toughness in NbSi2/MoSi2 duplex crystals2016

    • Author(s)
      M. Todai, K. Hagihara, K. Kishida, H. Inui, T. Nakano
    • Organizer
      9th Pacific Rim International Conference on Advanced Materials and Processing (PRICM9)
    • Place of Presentation
      京都国際会議場(京都府京都市)
    • Year and Date
      2016-08-01
    • Related Report
      2015 Annual Research Report
  • [Presentation] Athermal ω phase transformation and mechanical properties in binary Zr-Nb biomedical alloy2016

    • Author(s)
      M. Todai, K. Fukunaga, T. Nakano
    • Organizer
      International Conference on Processing and Manufacturing of Advanced Materials (Thermec’2016)
    • Place of Presentation
      オーストリア(グラーツ)
    • Year and Date
      2016-05-29
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] レーザー積層造形法と純金属混合粉を用いたTi合金の開発2016

    • Author(s)
      當代光陽, 掘敬雄, 孫世海, 中野貴由
    • Organizer
      粉体粉末冶金協会 平成28年度春季大会
    • Place of Presentation
      京都工芸繊維大学(京都府京都市)
    • Year and Date
      2016-05-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] Development of new single crystalline bone plate using an ISO certified biomedical Ti-15Mo-5Zr-3Al alloy2016

    • Author(s)
      M. Todai, K. Hagihara, M. Tane, T. Ishimoto, T. Nakano
    • Organizer
      10th World Biomaterials Congress (WBC2016)
    • Place of Presentation
      カナダ(モントリオール)
    • Year and Date
      2016-05-17
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子ビーム積層造形法によるTiAl合金の組織制御と力学特性2016

    • Author(s)
      當代光陽, Liu Tianqui、萩原幸司, 安田弘行, 中野貴由, 池田亜矢子, 近藤大介, 長町悠斗, 上田実
    • Organizer
      日本金属学会春期大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-25
    • Related Report
      2015 Annual Research Report
  • [Presentation] 電子ビーム積層造形法で作製したTiAl合金の微細組織と疲労特性2016

    • Author(s)
      趙研, 小林良太, 安田弘行, 當代光陽, 中野貴由, 池田亜矢子, 近藤大介, 長町悠斗, 上田実
    • Organizer
      日本金属学会春期大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-25
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高靭性B添加NbSi2/MoSi2複相シリサイド結晶におけるクリープ特性と変形組織2016

    • Author(s)
      鈴木将裕, 當代光陽, 萩原幸司, 中野貴由
    • Organizer
      日本金属学会春期大会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 微量B添加が複相シリサイド結晶におけるC40/C11b層状組織と力学的諸物性に及ぼす影響2016

    • Author(s)
      鈴木将裕, 當代光陽, 萩原幸司, 中野貴由
    • Organizer
      材料物性工学談話会 平成27年度第2回講演会&ポスター発表会
    • Place of Presentation
      京都大学(京都府左京区)
    • Year and Date
      2016-01-27
    • Related Report
      2015 Annual Research Report
  • [Presentation] 微量のボロン添加がNbSi2/ MoSi2複相シリサイド結晶における層状組織と機械的特性におよぼす影響2015

    • Author(s)
      鈴木将裕, 當代光陽, 萩原幸司, 中野貴由
    • Organizer
      平成27年度 第2回材料開発研究会
    • Place of Presentation
      兵庫県立大学(兵庫県姫路市)
    • Year and Date
      2015-12-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] Relationship between ω-phase transformation and reduction of Young’s modulus in Ti-Nb-Al single crystals2015

    • Author(s)
      M. Todai, P. Wang, T. Nakano
    • Organizer
      International symposium on processing and fabrication of advanced materials (PFAM 24)
    • Place of Presentation
      関西大学(大阪府吹田市)
    • Year and Date
      2015-12-20
    • Related Report
      2015 Annual Research Report
    • Invited
  • [Presentation] Controlling of oriented lamellar microstructure in NbSi2(C40)/MoSi2(C11b) duplex crystals2015

    • Author(s)
      M. Suzuki, M. Todai, Y. Kitani, K. Hagihara, T. Nakano
    • Organizer
      International symposium on processing and fabrication of advanced materials (PFAM 24)
    • Place of Presentation
      関西大学(大阪府吹田市)
    • Year and Date
      2015-12-19
    • Related Report
      2015 Annual Research Report
  • [Presentation] 生体骨程度の低ヤング率を示す単結晶ボーンプレートの創製2015

    • Author(s)
      當代光陽, 萩原幸司, 中野貴由
    • Organizer
      第37回 日本バイオマテリアル学会大会
    • Place of Presentation
      京都テルサ(京都府京都市)
    • Year and Date
      2015-11-10
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高靭性B添加NbSi2/MoSi2複相シリサイドにおけるクリープ特性2015

    • Author(s)
      鈴木将裕, 當代光陽, 萩原幸司, 中野貴由
    • Organizer
      日本金属学会秋季大会
    • Place of Presentation
      九州大学伊都キャンパス(福岡県福岡市)
    • Year and Date
      2015-09-24
    • Related Report
      2015 Annual Research Report
  • [Presentation] β型Ti-15Mo-5Zr-3Al合金を用いた単結晶ボーンプレートの開発2015

    • Author(s)
      當代光陽, 石本卓也,中野貴由
    • Organizer
      日本鉄鋼協会 第170回秋季講演大会
    • Place of Presentation
      九州大学伊都キャンパス(福岡県福岡市)
    • Year and Date
      2015-09-18
    • Related Report
      2015 Annual Research Report
  • [Presentation] 骨異方性構造の解析・制御・形成メカニズムの解明2015

    • Author(s)
      中野貴由, 石本卓也, 松垣あいら, 當代光陽
    • Organizer
      日本バイオマテリアル学会東北ブロック講演会
    • Place of Presentation
      東北大学(宮城県仙台市)
    • Year and Date
      2015-09-07
    • Related Report
      2015 Annual Research Report
  • [Presentation] 生体用β型Ti合金の低ヤング率化に向けた合金設計法2015

    • Author(s)
      當代光陽, P. Wang, 萩原幸司, 中野貴由
    • Organizer
      関西バイオマテリアル学会第10回関西若手研究発表会
    • Place of Presentation
      関西大学(大阪府吹田市)
    • Year and Date
      2015-08-05
    • Related Report
      2015 Annual Research Report
  • [Presentation] Ti-28Nb-7Al合金単結晶における非熱的ω相と低弾性化2015

    • Author(s)
      當代光陽, P. Wang, 中野貴由
    • Organizer
      軽金属学会 第128回春期大会
    • Place of Presentation
      東北大学(宮城県仙台市)
    • Year and Date
      2015-05-17
    • Related Report
      2015 Annual Research Report
  • [Presentation] 生体用Zr-Nb合金へのAl添加による非熱的ω抑制と低弾性化2015

    • Author(s)
      當代光陽,福永圭佑,中野貴由,野村直之,塙隆夫
    • Organizer
      日本金属学会
    • Place of Presentation
      東京大学駒場キャンパス(東京都目黒区)
    • Year and Date
      2015-03-15
    • Related Report
      2014 Research-status Report
  • [Presentation] 異なる弾性率を有する骨プレート埋入による骨配向性への影響2015

    • Author(s)
      田中優衣, 石本卓也, 當代光陽, 中野貴由, 川西洋平, 坂井孝司, 村瀬剛, 吉川秀樹
    • Organizer
      日本金属学
    • Place of Presentation
      東京大学駒場キャンパス(東京都目黒区)
    • Year and Date
      2015-03-15
    • Related Report
      2014 Research-status Report
  • [Presentation] 応力遮蔽抑制のための比低弾性インプラントの開発と骨配向性への影響2015

    • Author(s)
      田中優衣, 石本卓也, 當代光陽, 中野貴由, 川西洋平, 坂井孝司, 村瀬剛,吉川秀樹
    • Organizer
      日本鉄鋼協会関西支部平成26年度第2回材料開発会議
    • Place of Presentation
      関西大学吹田キャンパス(大阪府吹田市)
    • Year and Date
      2015-01-27
    • Related Report
      2014 Research-status Report
  • [Presentation] Effect of B addition on the microstructure and mechanicalproperties of NbSi2/MoSi2 duplex crystal2014

    • Author(s)
      T. Nakano, M. Todai, K. Hagihara
    • Organizer
      MRS 2014 fall meeting
    • Place of Presentation
      Boston, USA
    • Year and Date
      2014-12-01
    • Related Report
      2014 Research-status Report
  • [Presentation] Ti合金単結晶の特異物性とこれを利用した低弾性化2014

    • Author(s)
      當代光陽, 萩原幸司, 中野貴由
    • Organizer
      第二回チタン若手交流会
    • Place of Presentation
      神戸製鋼所 高砂製作所 (兵庫県高砂市)
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] ボロンを微量添加したMoSi2/NbSi2複相シリサイドの層状組織とクリープ特性の評価2014

    • Author(s)
      鈴木将裕, 當代光陽, 萩原幸司,中野貴由
    • Organizer
      日本金属学会
    • Place of Presentation
      名古屋大学東山キャンパス(愛知県名古屋市千種区)
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] Ti-Al-Nb-Mn合金における微細組織と力学特性2014

    • Author(s)
      Liu Tenqui, 當代光陽, 萩原幸司,Y.-W. Kim,中野貴由
    • Organizer
      日本金属学会
    • Place of Presentation
      名古屋大学東山キャンパス(愛知県名古屋市千種区)
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Presentation] MoSi2/NbSi2複相シリサイドにおける層状組織と室温靭性へのボロン添加の影響2014

    • Author(s)
      當代光陽, 木谷友翔,萩原幸司,中野貴由
    • Organizer
      日本金属学会
    • Place of Presentation
      名古屋大学東山キャンパス(愛知県名古屋市千種区)
    • Year and Date
      2014-09-24
    • Related Report
      2014 Research-status Report
  • [Book] バイオマテリアル研究の最前線2014

    • Author(s)
      當代光陽, 中野貴由(分担執筆)
    • Total Pages
      250
    • Publisher
      日本金属学会
    • Related Report
      2014 Research-status Report
  • [Remarks] 大阪大学大学院工学研究科マテリアル生産科学専攻 中野研究室

    • URL

      http://www.mat.eng.osaka-u.ac.jp/msp6/nakano/

    • Related Report
      2015 Annual Research Report
  • [Remarks] 大阪大学 中野研究室

    • URL

      http://www.mat.eng.osaka-u.ac.jp/msp6/nakano/

    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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