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Synergistic creep strengthening mechanism by dislocations and precipitates in ferritic heat-resistant steels

Research Project

Project/Area Number 26820317
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionKyushu University

Principal Investigator

Mitsuhara Masatoshi  九州大学, 総合理工学研究科(研究院), 准教授 (10514218)

Project Period (FY) 2014-04-01 – 2016-03-31
Project Status Completed (Fiscal Year 2015)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2015: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2014: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywordsフェライト系耐熱鋼 / クリープ / 強化機構 / 炭化物 / SEM / 結晶方位分布 / 粒界性格 / 高Crフェライト系耐熱鋼 / クリープ変形 / ラスマルテンサイト / M23C6炭化物 / 結晶粒界 / 電子顕微鏡 / 結晶方位解析
Outline of Final Research Achievements

In conventional ferritic heat-resistant steels with 9% Cr, the creep strength at an elevated temperature is improved by a combination of dislocation strengthening and M23C6 carbide strengthening. The M23C6 carbides are almost located on the grain boundaries in the lath martensite. In this study, we quantified some carbide parameters on each boundary using SEM techniques and discussed the effect of boundary character on the M23C6 carbides distribution. The M23C6 carbides size and coverage as function of creep time on each boundary in crept Gr. 91 steels were estimated using SEM-BSE images and SEM-EBSD analyses. Those parameters obviously had a dependency on the boundary character. On the prior γ grain boundary, the coverage was the highest before creep but it was drastically decreases with increasing creep time because the carbides were quickly coarsened.

Report

(3 results)
  • 2015 Annual Research Report   Final Research Report ( PDF )
  • 2014 Research-status Report
  • Research Products

    (15 results)

All 2016 2015 2014

All Journal Article (3 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 1 results) Presentation (10 results) (of which Int'l Joint Research: 4 results,  Invited: 3 results) Book (2 results)

  • [Journal Article] Creep strengthening by lath boundaries in 9Cr ferritic heat-resistant steel2016

    • Author(s)
      M. Mitsuhara, S. Yamasaki, M. Miake, H. Nakashima, M. Nishida, J. Kusumoto, A. Kanaya
    • Journal Title

      Philosophical Magazine Letters

      Volume: 96 Issue: 2 Pages: 76-83

    • DOI

      10.1080/09500839.2016.1154200

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effect of grain boundary character on M23C6 carbide distribution in high Cr ferritic heat-resistant steel2016

    • Author(s)
      T. Okano, T. Ito, M. Mitsuhara, M. Nishida
    • Journal Title

      Proceedings of Advanced High-Temperature Materials Technology for Sustainable and Reliable Power Engineering, 123HiMAT-2015

      Volume: in press

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 4種類の異なるラスマルテンサイト界面におけるM23C6炭化物の生成・成長挙動2015

    • Author(s)
      岡野倫明、伊藤孝矩、光原昌寿、西田稔
    • Journal Title

      日本学術振興会耐熱金属材料第123委員会研究報告

      Volume: 56 Pages: 165-172

    • Related Report
      2015 Annual Research Report
  • [Presentation] 9Crフェライト系耐熱鋼におけるマルテンサイト界面とM23C6粗大化挙動の関係2016

    • Author(s)
      岡野倫明、伊藤孝矩、光原昌寿、西田稔
    • Organizer
      日本鉄鋼協会 第171回春季講演大会
    • Place of Presentation
      東京理科大学
    • Year and Date
      2016-03-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] 高Crフェライト鋼におけるM23C6炭化物の分散状態と強度への寄与に関する一考察2015

    • Author(s)
      光原昌寿、岡野倫明、伊藤孝矩、西田稔
    • Organizer
      「高Cr鋼溶接部組織の基礎的理解とその応用」自主フォーラム第7回会合
    • Place of Presentation
      東北大学
    • Year and Date
      2015-11-13
    • Related Report
      2015 Annual Research Report
  • [Presentation] Microstructural evolution of welded joint during creep in high Cr ferritic heat-resistant steel2015

    • Author(s)
      M. Mitsuhara, S. Akada, S. Yamasaki, H. Nakashima, M. Nishida, Y. Hasegawa
    • Organizer
      Advanced High-Temperature Materials Technology for Sustainable and Reliable Power Engineering, 123HiMAT-2015
    • Place of Presentation
      北海道大学
    • Year and Date
      2015-06-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of grain boundary character on M23C6 carbide distribution in high Cr herritic heat-resistant steel2015

    • Author(s)
      T. Okano, T. Ito, M. Mitsuhara, M. Nishida
    • Organizer
      Advanced High-Temperature Materials Technology for Sustainable and Reliable Power Engineering, 123HiMAT-2015
    • Place of Presentation
      北海道大学
    • Year and Date
      2015-06-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Change in major creep reinforcer of ferritic heat-resistant steel depending on applied stress2015

    • Author(s)
      S. Yamasaki, M. Mitsuhara, S. Hata, H. Nakashima
    • Organizer
      Advanced High-Temperature Materials Technology for Sustainable and Reliable Power Engineering, 123HiMAT-2015
    • Place of Presentation
      北海道大学
    • Year and Date
      2015-06-29
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Lath boundary strengthening mechanism in high Cr ferritic heat-resistant steel2015

    • Author(s)
      M. Mitsuhara, M. Miake, S. Yamasaki, M. Nishida, J. Kusumoto, A. Kanaya
    • Organizer
      13th International Conference on Creep and Fracture of Engineering Materials and Structures, CREEP2015
    • Place of Presentation
      Espace Vanel, Toulouse, France
    • Year and Date
      2015-05-31
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] フェライト系耐熱鋼の強化・弱化機構解明に向けた金相学的アプローチ2014

    • Author(s)
      光原昌寿、岡野倫明、伊藤孝矩、山崎重人、中島英治、西田稔
    • Organizer
      日本鉄鋼協会 材料の組織と特性部会 若手フォーラム 平成26年度研究会
    • Place of Presentation
      種子島大和温泉ホテル
    • Year and Date
      2014-12-16 – 2014-12-17
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] High temperature deformation dynamics in crystalline materials2014

    • Author(s)
      H. Nakashima, M. Mitsuhara
    • Organizer
      The 4th International Symposium on Steel Science (ISSS 2014)
    • Place of Presentation
      Kansai Seminar House, Kyoto
    • Year and Date
      2014-11-03 – 2014-11-06
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] トモグラフィーによる耐熱用合金の3次元構造解析2014

    • Author(s)
      光原昌寿、波田慎太郎、伊藤孝矩、山崎重人、西田稔
    • Organizer
      日本金属学会 2014年秋期講演(第155回)大会
    • Place of Presentation
      名古屋大学 東山キャンパス
    • Year and Date
      2014-09-24 – 2014-09-26
    • Related Report
      2014 Research-status Report
    • Invited
  • [Presentation] 高Crフェライト系耐熱鋼のクリープ強度とサブグレイン組織2014

    • Author(s)
      光原昌寿、三明正樹、山崎重人、西田稔
    • Organizer
      日本金属学会 高温強度と組織形成の材料科学研究会「平成 26 年度夏の学校」および超塑性研究会第 155 回研究会
    • Place of Presentation
      北見工業大学 屈斜路湖研究所
    • Year and Date
      2014-08-21 – 2014-08-23
    • Related Report
      2014 Research-status Report
  • [Book] 第5版鉄鋼便覧 第3巻 21章1-2節2014

    • Author(s)
      光原昌寿、中島英治
    • Total Pages
      8
    • Publisher
      日本鉄鋼協会
    • Related Report
      2014 Research-status Report
  • [Book] 第5版鉄鋼便覧 第3巻 35章5節2014

    • Author(s)
      光原昌寿
    • Total Pages
      2
    • Publisher
      日本鉄鋼協会
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2017-05-10  

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