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Titanate compound particle fabrication using a liquid phase formed by laser heating

Research Project

Project/Area Number 26870908
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Inorganic industrial materials
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

ISHIKAWA YOSHIE  国立研究開発法人産業技術総合研究所, ナノ材料研究部門, 主任研究員 (20509129)

Co-Investigator(Renkei-kenkyūsha) KOSHIZAKI Naoto  北海道大学, 大学院工学研究院 量子理工学部門, 教授 (40344197)
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2016: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywordsレーザープロセッシング / 液中レーザー溶融法 / サブマイクロメートル球状粒子 / 複合化合物 / サブミクロン球状粒子 / 球状粒子 / サブマイクロメートルサイズ
Outline of Final Research Achievements

Crystalline spheres of composite compound were obtained with a pulsed laser irradiation of a binary particle mixture dispersed in liquid. A chemical composition of formed composite compound by a laser irradiation of a mixture of TiO2 and MgCO3 was only MgTi2O5 even at any mixed composition ratio. Although TiO2 can melt by laser irradiation with 355 nm wavelength, MgCO3 remains as a solid state due to an optical transparency. In contrast, FeB and Fe2B formation occurred with a laser irradiation of mixture a-Fe2O3 and B4C, in which phase transitions to liquid phase of both a-Fe2O3 and B4C was necessary. Thus, a composite compound sphere formation mechanism depends on materials of raw particle mixture in this technique.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (10 results)

All 2017 2016 2015 2014

All Journal Article (2 results) (of which Acknowledgement Compliant: 2 results,  Peer Reviewed: 1 results) Presentation (8 results) (of which Int'l Joint Research: 1 results,  Invited: 1 results)

  • [Journal Article] 液中レーザー溶融法により得られるサブミクロン球状粒子の応用展開2017

    • Author(s)
      石川 善恵,越崎 直人
    • Journal Title

      レーザー研究

      Volume: 印刷中

    • NAID

      130007957293

    • Related Report
      2016 Annual Research Report
    • Acknowledgement Compliant
  • [Journal Article] Nano- and Submicrometer-Sized Spherical Particle Fabrication Using a Submicroscopic Droplet Formed Using Selective Laser Heating2016

    • Author(s)
      Yoshie Ishikawa, Naoto Koshizaki, Alexander Pyatenko, Noriyuki Saitoh, Noriko Yoshizawa, Yoshiki Shimizu
    • Journal Title

      The Journal of Physical Chemistry C

      Volume: 120 Issue: 4 Pages: 2439-2446

    • DOI

      10.1021/acs.jpcc.5b10691

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Internal composite structures of Au-Fe submicrometer spherical particles fabricated by pulsed laser melting in liquid2017

    • Author(s)
      布施北斗,石川 善恵,越崎 直人
    • Organizer
      第34回プラズマプロセシング研究会/第29回プラズマ材料科学シンポジウム(合同会議)
    • Place of Presentation
      北海道大学 学術交流会館
    • Year and Date
      2017-01-17
    • Related Report
      2016 Annual Research Report
  • [Presentation] Size-selective nanoparticle fabrication utilizing particle vaporization conditions for pulsed laser melting in liquid2017

    • Author(s)
      石川 善恵,越崎 直人
    • Organizer
      第34回プラズマプロセシング研究会/第29回プラズマ材料科学シンポジウム(合同会議)
    • Place of Presentation
      北海道大学 学術交流会館
    • Year and Date
      2017-01-17
    • Related Report
      2016 Annual Research Report
  • [Presentation] Nano-sphere formation by pulsed laser melting in liquid2016

    • Author(s)
      石川 善恵,越崎 直人
    • Organizer
      4th Conference on Advanced Nanoparticle Generation and Excitation by Lasers in Liquids (ANGEL)
    • Place of Presentation
      Essen, Germany
    • Year and Date
      2016-05-12
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 液中レーザー溶融法による微小球状粒子の作製とその応用2016

    • Author(s)
      石川善恵, 越崎直人, Pyatenko Timofeevich Alexander
    • Organizer
      レーザー学会学術講演会第36回年次大会
    • Place of Presentation
      名古屋市
    • Year and Date
      2016-01-11
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 液中レーザー溶融法によるサブミクロン結晶性球状粒子の合成の合成2015

    • Author(s)
      石川善恵, 越崎直人
    • Organizer
      公益社団法人日本セラミクス協会 第28回秋季シンポジウム
    • Place of Presentation
      富山市
    • Year and Date
      2015-09-18
    • Related Report
      2015 Research-status Report
  • [Presentation] 液中レーザー溶融法におけるフルーエンスが生成粒子に及ぼす影響2015

    • Author(s)
      石川善恵、越崎直人
    • Organizer
      レーザー学会学術講演愛 第35回年次大会
    • Place of Presentation
      東京 東海大学 高輪校舎
    • Year and Date
      2015-01-10 – 2015-01-11
    • Related Report
      2014 Research-status Report
  • [Presentation] 液中レーザー溶融法により得られた球状粒子の内部観察2014

    • Author(s)
      石川善恵、越崎直人
    • Organizer
      第75回 応用物理学会秋季学術講演会
    • Place of Presentation
      札幌 北海道大学
    • Year and Date
      2014-09-17
    • Related Report
      2014 Research-status Report
  • [Presentation] Reactive fabrication of MgTi2O5 spherical particles by pulsed laser melting in liquid from raw particle mixture2014

    • Author(s)
      石川善恵 越崎直人
    • Organizer
      ANGEL 2014
    • Place of Presentation
      Matsuyama
    • Year and Date
      2014-05-20
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2018-03-22  

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