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Development of scanning three-dimensional x-ray diffraction microscopy using a microbeam and its application to steel

Research Project

Project/Area Number 26870932
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Quantum beam science
Material processing/Microstructural control engineering
Research InstitutionToyota Central R&D Lab., Inc.

Principal Investigator

Hayashi Yujiro  株式会社豊田中央研究所, 分析部 量子ビーム解析研究室, 研究員 (30435953)

Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2016: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2015: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2014: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
KeywordsX線回折 / 3次元 / 3DXRD / 走査型 / マイクロビーム / 非破壊 / 結晶方位 / 鉄鋼材料 / 量子ビーム / 放射光 / 塑性加工・成形 / 機械材料
Outline of Final Research Achievements

Three-dimensional x-ray diffraction microscopy (3DXRD) has enabled non-destructive three-dimensional mapping of orientations in a polycrystalline alloy. From practical interests, we have tried to apply 3DXRD to practical engineering materials such as steel. Such materials tend to be give rise to the massive overlaps of diffraction spots due to a large number of grains or mosaic spreads, which prevent us from reconstructing orientation maps. In addition, the reconstruction of composite microstructures of steel has not been achieved using 3DXRD-based methods. In this study, as a solution of the problems, we propose a scanning type approach termed scanning 3DXRD using an x-ray microbeam. In the scanning 3DXRD method, the microstructures of ferrite-pearlite or ferrite-martensite steel are reconstructed by determing the ferrite microstructure. The validation of the approach has been demonstrated using ferrite-pearlite and ferrite-martensite steel specimens.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (17 results)

All 2017 2016 2015

All Journal Article (4 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 3 results) Presentation (13 results) (of which Int'l Joint Research: 5 results,  Invited: 3 results)

  • [Journal Article] Scanning three-dimensional X-ray diffraction microscopy with a high-energy microbeam at SPring-82017

    • Author(s)
      Yujiro Hayashi, Daigo Setoyama and Yoshiki Seno
    • Journal Title

      Materials Science Forum

      Volume: 印刷中

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] 走査型3DXRD顕微鏡法の開発2017

    • Author(s)
      林雄二郎、広瀬美治、妹尾与志木、吉田友幸
    • Journal Title

      SPring-8/SACLA利用者情報

      Volume: Volume 22, No.1 Pages: 8-13

    • Related Report
      2016 Annual Research Report
    • Acknowledgement Compliant
  • [Journal Article] Scanning Three-dimensional X-Ray Diffraction Microscopy for Non-Destructive Observation of Plastic Deformation in Metallic Materials2016

    • Author(s)
      Y. Hayashi, Y. Seno, D. Setoyama
    • Journal Title

      SPring-8/SACLA Research Frontiers 2015

      Volume: 2015 Pages: 114-115

    • Related Report
      2016 Annual Research Report
  • [Journal Article] Polycrystal orientation mapping using scanning three-dimensional X-ray diffraction microscopy2015

    • Author(s)
      Yujiro Hayashi, Yoshiharu Hirose and Yoshiki Seno
    • Journal Title

      Journal of Applied Crystallography

      Volume: 48 Issue: 4 Pages: 1094-1101

    • DOI

      10.1107/s1600576715009899

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Orientation mapping of steel by scanning three-dimensional x-ray diffraction microscopy2017

    • Author(s)
      Yujiro Hayashi, Yoshiki Seno, Tomoyuki Yoshida
    • Organizer
      The 24th Congress & General Assembly of the International Union of Crystallography 2017
    • Place of Presentation
      Hyderabad International Convention Centre, Hyderabad, India
    • Year and Date
      2017-08-21
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 3D Orientation and Stress Mapping with X-Ray Diffraction2017

    • Author(s)
      Yujiro Hayashi
    • Organizer
      Gordon Research Conference 2017 on Physical Metallurgy
    • Place of Presentation
      University of New England, Biddeford, ME, USA
    • Year and Date
      2017-07-23
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 走査型3DXRD法による実用鋼板中の3次元非破壊結晶方位マッピング2017

    • Author(s)
      林雄二郎、妹尾与志木、吉田友幸
    • Organizer
      第30回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      神戸芸術センター、神戸市
    • Year and Date
      2017-01-07
    • Related Report
      2016 Annual Research Report
  • [Presentation] 走査型3DXRD顕微鏡法とデータ解析2017

    • Author(s)
      林雄二郎
    • Organizer
      第8回SPring-8先端利用技術ワークショップ
    • Place of Presentation
      神戸芸術センター、神戸市
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] 走査型3DXRD顕微鏡法による冷間圧延鋼板内部の結晶方位3次元マッピング2016

    • Author(s)
      林雄二郎、妹尾与志木、吉田友幸、瀬戸山大吾
    • Organizer
      日本金属学会2016年秋季大会
    • Place of Presentation
      大阪大学、豊中市
    • Year and Date
      2016-09-21
    • Related Report
      2016 Annual Research Report
  • [Presentation] 走査3DXRD顕微鏡法の開発2016

    • Author(s)
      妹尾与志木、林雄二郎、吉田友幸
    • Organizer
      第13回SPring-8産業利用報告会
    • Place of Presentation
      兵庫県民会館、神戸市
    • Year and Date
      2016-09-07
    • Related Report
      2016 Annual Research Report
  • [Presentation] 走査型3DXRD顕微鏡法の開発2016

    • Author(s)
      林雄二郎
    • Organizer
      SPring-8シンポジウム 2016
    • Place of Presentation
      関西学院大学、三田市
    • Year and Date
      2016-08-29
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] Scanning 3DXRD Technique using a Microbeam for In-situ Orientation and Stress Mapping2016

    • Author(s)
      Yujiro Hayashi, Yoshiki Seno, Daigo Setoyama
    • Organizer
      The 3rd International Congress on 3D Materials Science (3DMS) 2016
    • Place of Presentation
      St. Charles, Illinois, USA
    • Year and Date
      2016-07-10
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 走査型3DXRD顕微鏡法による冷間圧延鋼板中の第2種残留応力測定2016

    • Author(s)
      林 雄二郎, 妹尾 与志木, 瀬戸山 大吾
    • Organizer
      第29回日本放射光学会年会・放射光科学合同シンポジウム
    • Place of Presentation
      東京大学柏の葉キャンパス駅前サテライト(千葉県・柏市)
    • Year and Date
      2016-01-09
    • Related Report
      2015 Research-status Report
  • [Presentation] 走査型3次元X線回折(3DXRD)顕微鏡法の開発2016

    • Author(s)
      妹尾与志木、林雄二郎、吉田友幸
    • Organizer
      第10回九州シンクロトロン光研究センター研究成果報告会
    • Place of Presentation
      サンメッセ鳥栖、鳥栖市
    • Related Report
      2016 Annual Research Report
  • [Presentation] Scanning three-dimensional x-ray diffraction microscopy with a high-energy microbeam at SPring-82015

    • Author(s)
      Yujiro Hayashi, Daigo Setoyama and Yoshiki Seno
    • Organizer
      8th International Conference on Mechanical Stress Evaluation by Neutrons & Synchrotron Radiation (MECASENS2015)
    • Place of Presentation
      Grenoble, France
    • Year and Date
      2015-09-30
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Scanning three-dimensional x-ray diffraction microscopy using a high-energy microbeam2015

    • Author(s)
      Yujiro Hayashi, Yoshiharu Hirose and Yoshiki Seno
    • Organizer
      12th International Conference on Synchrotron Radiation Instrumentation (SRI 2015)
    • Place of Presentation
      New York City, USA
    • Year and Date
      2015-07-06
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 豊田ビームラインにおける高エネルギーマイクロビームを用いた走査型3DXRD顕微鏡装置の概要2015

    • Author(s)
      林雄二郎、広瀬美治
    • Organizer
      第28回日本放射光学会年会
    • Place of Presentation
      草津、立命館大学
    • Year and Date
      2015-01-10 – 2015-01-12
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2018-03-22  

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