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Development of Transmission Electron Microscopic Three Dimensional Analysis Systems

Research Project

Project/Area Number 59850117
Research Category

Grant-in-Aid for Developmental Scientific Research

Allocation TypeSingle-year Grants
Research Field 金属材料(含表面処理・腐食防食)
Research InstitutionInstitute of Industrial Science, University of Tokyo

Principal Investigator

YOICHI ISHIDA  Institute of Industrial Science, University of Tokyo, 生産技術研究所, 教授 (60013108)

Co-Investigator(Kenkyū-buntansha) 小久保 靖  日本電子株式会社, 技術部, 主任研究員
HIDEKI ICHINOSE  Institute of Industrial Science, University of Tokyo, 生産技術研究所, 助手 (30159842)
MINORU MORI  Institute of Industrial Science, University of Tokyo, 生産技術研究所, 助教授 (30134646)
SUSUMU NANAO  Institute of Industrial Science, University of Tokyo, 生産技術研究所, 助教授 (60013231)
MORIO ONOE  Institute of Industrial Science, University of Tokyo, 生産技術研究所, 名誉教授 (70013076)
YASUSHI KOKUBO  Japan Electron Optics Laboratory LTD
Project Period (FY) 1984 – 1986
Project Status Completed (Fiscal Year 1986)
Budget Amount *help
¥14,000,000 (Direct Cost: ¥14,000,000)
Fiscal Year 1986: ¥500,000 (Direct Cost: ¥500,000)
Fiscal Year 1985: ¥2,900,000 (Direct Cost: ¥2,900,000)
Fiscal Year 1984: ¥10,600,000 (Direct Cost: ¥10,600,000)
Keywordstransmission electron microscopy / three-dimensional analysis / computer tomography / image analysis / 弱ビーム像 / 透過電子顕微鏡 / 画像処理システム / 3次元組織 / 立体観察 / 粒界並進成分
Research Abstract

Application of computer tomography to three dimensional analysis of internal structures in a thin foil specimen by combining an image analyser to a transmission electron microscope is the objective of this research. A high voltage electron microscope of the University was used and special computer programs were produced to do the analysis. As for the specimens (1) a splat-cooled Al-Sn alloy with small spherical <bata> -Sn particles dispersed in Al matrix, (2) doped GaP single crystal with a characteristic dislocation network, (3) stainless steels with defect introduced by either helium ion irradiation or hydrogen charging and (4) tritium transmission electron microscopic autoradiography specimen. The last two subjects are basic researches related to the development of fusion reactor first wall material. In all cases a set of photographs were taken for a same area tilting the specimen foil by a side-entry type goniometer by <-!+> 60 degrees and marking representative points by a digitizer. On-line analysis was delayed because of the problems in using the high voltage electron microscope of the University. As the bases of the present project, several analysis techniques (1) crystalline orientation relationship representation, (2) weak-beam common diffraction method and (3) image analysis of weak-beam, lattice image and channeling pattern were developed. Weak-beam imaging is particularly useful for the present analysis because localized and high contrast images are obtained for a set of micrographs at a single diffraction if the tilting axis was made approximately parallel to that of the side entry goniometer. Analysis of fine interface structures by a common diffraction ( <alpha> -fringe) is a favorable subject of the method and number of works were published in this area, the copies of which are included in the report.
Lattice Imaging Analysis of <SIGMA> 3 Coincidence-site-lattice Boundaries

Report

(2 results)
  • 1986 Final Research Report Summary
  • 1985 Annual Research Report
  • Research Products

    (19 results)

All Other

All Publications (19 results)

  • [Publications] H.Ichinose;Y.Ishida: Scripta Metallurgica. 19. 5-9 (1985)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] H.Ichinose;Y.Ishida;N.Baba;K.Konaga: Philosophical Magazine. A52. 51-59 (1985)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida;M.Mori: Journal de Physique. 46 C4. 465-474 (1985)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] H.Ichinose;Y.Ishida: Journal de Physique. 46 C4. 39-49 (1985)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida;K.Miyazawa;M.Mori: Philosophical Magazine. A53. 131-140 (1986)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] K.Miyazawa;Y.Ishida: Journal of Microscopy. 142. 163-169 (1986)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida Editor in Chief: "Grain Boundary Structure and Related Phenomena(Proceedings of 4th Japan Institute of Metals International Symposium)" The Japan Institute of Metals, 1,105 (1986)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida Editor: "Fundamentals of Joining" North Holland Publications, (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] H.Ichinose and Y.Ishida: "High Resolution Electron Microscopy of Rapidly Quenched Al-Sn Alloy" Scripta Mettallurgica. 19. 5-9 (1985)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] H.Ichinose, Y.Ishida, N.Baba and K.Konaga: "in Gold" Philosophical Magazine. A52. 51-59 (1985)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida and M.Mori: "Theoretical Studies of Segregated Internal Interfaces" Journal de Physique. 46/C4. 465-474 (1985)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] H.Ichinose and Y.Ishida: "High Resolution Electron Microscopy of Grain Boundaries in fcc and bcc Metals" Journal de Physique. 46/C4. 39-49 (1985)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida, K.Miyazawa and M.Mori: "Determination of the Burgers Vector of an Isolated Boundary Dislocation by Weak-beam High Voltage Electron Microscopy" Philosophical Magazine. A53. 131-140 (1986)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Y.Ishida,ed.: Grain Boundary Structure and Related Phenomena ( Proceedings of 4th Japan Institute of Metals International Symposium ), 1,105 (1986)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1986 Final Research Report Summary
  • [Publications] Dislocation in Solids. 667-670. (1985)

    • Related Report
      1985 Annual Research Report
  • [Publications] Journal de Physique. 46C4. (1985)

    • Related Report
      1985 Annual Research Report
  • [Publications] Phlosophycal Magazine. 52-1. (1985)

    • Related Report
      1985 Annual Research Report
  • [Publications] Progress in Image Processing(International Conference). (1985)

    • Related Report
      1985 Annual Research Report
  • [Publications] Progress in Image Processing(International Conference). (1985)Proceeding of JIMIS4(Minakami Conference).

    • Related Report
      1985 Annual Research Report

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Published: 1987-03-31   Modified: 2016-04-21  

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