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A Baic Study of Strengthening of Polycrystalline Magnetic Materials

Research Project

Project/Area Number 61550518
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 金属材料(含表面処理・腐食防食)
Research InstitutionTOHOKU UNIVERSITY

Principal Investigator

WATANABE Tadao  Research Associate, Faculty of Engineering, Tohoku Univ.,, 工学部, 助手 (40005327)

Project Period (FY) 1986 – 1988
Project Status Completed (Fiscal Year 1988)
Budget Amount *help
¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 1988: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1987: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 1986: ¥700,000 (Direct Cost: ¥700,000)
KeywordsGrain Boundary Design / Control of Brittleness and Intergranular Fracture / Grain Boundary Character Distribution (GBCD) / Magnetic Annealing / 磁気焼鈍効果 / SEM-ECP / 急冷凝固 / Fe-6.5mass%Si / 集合組織と粒界 / 低エネルギー粒界 / SEM-ECP法 / 磁気的強化 / Fe-6.5%Si合金 / 強磁性材料 / 磁場中焼鈍
Research Abstract

In order to improve mechanical Properties of polycrystalline megnetic materials which are normally show a significant brittleness associated with intergranular fracture, the possibility of the control of intergranular fracture has been studied according to the concept of grain boundary design recently proposed by the present investigator. The type and frequency of grain boundaries, so called grain boundary character distribution (GBCD) has been investigated in several ferromagnetic iron alloys (iron-cobalt and iron-silicon alloys) produced by different fabrication methods. Firstly, the grain boundary character distribution (GBCD) was determined for iron-10%cobalt alloy polycrystals which were produced by annealing in the magnetic field up to 0.5T. It was found that It was found that the frequency of low-angle boundaries increases linearly with increasing the magnetic field strngth. Almost four times higher frequency (7.8%) of low-angle boundaries was observed for the specimen produce b … More y magnetic annealing at 0.5T than that for the specimen without magnetic annealing. Thus magnetic annealing has been proved to be useful for controlling the GBCD in ferromagnetic polycrystals.
In the present work, the GBCD for rapidly solidified and annealed iron-6.5mass%Si alloy ribbons with {100} or {110} texture, was stueied in order to reveal the origin of high ductility of the ribbone. extremely high frequency ( =45% ) of low-energy boundaries such as low-angle ( 1) boundaries and low coincidence boundaries, was observed. the observed high ductility of the ribbons is attributed to the presence of high frequency of low-energy boundaries which are resistant to intergranular fracture. the inverse cubic root dependence of the frequency of coincidence boundaries was first found. The values of coincidence boundaries which occurred preferentially in {100} or {110} textured riibons, can be predicted from coincidence orientation relationship for <100> or <110> rotation. It has been shown that the grain boundary character distribution (BGCD) can be manupilated in order to endow polycrystalline magnetic materials with desirable properties, particularly to control their brittleness caused by intergranular fracture, according to the concept of grain boundary design recently proposed by the present investigator. Less

Report

(4 results)
  • 1988 Annual Research Report   Final Research Report Summary
  • 1987 Final Research Report Summary
  • 1986 Annual Research Report

Research Products

(19 results)

All Other

All Publications

  • [Publications] Tadao WATANABE.: Scripta Metallurgica. 21. 427-432 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE.: Proceedings of MRS Intern.Symp.on Interfacial Structure,Properties and Design,The Materials Research Society. 122. 443-454 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE.: Materials Forum, Australia Bicentenary Anniversary Volume. II. 284-303 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE,;Hiroyuki FUJII,;Hiroshi OIKAWA,;Ken-Ichi ARAI.: Acta Metallurgica. 37. 941-952 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE,;Ken-Ichi ARAI,;Kyosuke YOSHIMI,;Hiroshi OIKAWA.: Philosophical Magazine Letters. 59. (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE,;L.C.Lim.: Scripta Metallurgica. 23. (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE: "Prediction of Change in Grain Boundary Energy during Grain Growth" Scripta Metallurgica. 21. 427-432 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE: "The Importance of Grain Boundary Character Distribution to Grain Boundary Design (Invited Paper)" Proceedings of MRS Intern.Symposium on Interfacial Structure, Properties and Design, The Materials Rsearch Society (MRS). 122. 443-454 (1988)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE: "The Potential for Grain Boundary Design in Materials Development ( Invited Paper )" Materials Forum, Australia Bicentenary Anniversary Volume. 11. 284-303 (1988)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE; Hiroyuki FUJII; Hiroshi OIKAWA; Ken-Ichi ARAI: "A Grain Boundary Study of Rapidly Solidified and Annealed Fe-6.5mass%Si Polycrystalline Ribbons" Proceedings of the 5th Japan Inst. Metals Intern. Symp. (JIMIS-5) on Non-equlibrium Solid Phases of Metals and Alloys, Trans. Japan Inst. Metals,. 29. 123-126 (1988)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao WATANABE; Hiroyuki FUJII;Hiroshi OIKAWA; Ken-Ichi ARAI: "Grain Boundaries in Rapidly Solidified and Annealed Fe-6.5mass%Si Polycrystalline Ribbons with High Ductility" Acta Metallurgica. 37. 941-952 (1989)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1988 Final Research Report Summary
  • [Publications] Tadao,WATANABE: Proceedings of MRS Intern.Symp.on Interfacial Structure,Properties and Design,The Matkerials Research Society. 122. 443-454 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] Tadao,WATANABE: Materials Forum,Australia Bicentenary Anniversary Volume. 11. 284-303 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] Tadao,WATANABE;Hiroyuki,FUJII;Hiroshi,OIKAWA,Ken-Ichi,ARAI: Proceedings of the 5th Japan Inst.Metals Intern.Symp.(JIMIS-5)on Non-equlibrium Solid Phases of Metals and Alloys. 29. 123-126 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] Tadao,WATANABE;Hiroyuki,FUJII;Hiroshi,OIKAWA,Ken-Ichi,ARAI: Acta Metallurgica. 37. 941-952 (1989)

    • Related Report
      1988 Annual Research Report
  • [Publications] Tadao,WATANABE;Ken-Ichi,Arai;Kyosuke,Yoshimi;Hiroshi,Oikawa;Hiroshi,OIKAWA,: Philosophical Magazine Letters. 59. (1989)

    • Related Report
      1988 Annual Research Report
  • [Publications] Tadao,WATANABE;L.C.Lim: Scripta Metallurgica. 23. (1989)

    • Related Report
      1988 Annual Research Report
  • [Publications] T.Watamake,H.Fujii, H.Oikawa and K.I.Arai: Proceedings of 5th Japan Inst.Metal Symposium( OIMIS-5) an Non-Equilibrium Solid Phases of Metals andatoys.(1988)

    • Related Report
      1987 Final Research Report Summary
  • [Publications] T.A atanake, H.Fujii, H.Oikawa and K.I.Arai: Acta Metallurgica.

    • Related Report
      1987 Final Research Report Summary

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Published: 1987-03-30   Modified: 2016-04-21  

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