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Differential Scanning Calorimetry of Retrogradation and Freezing Process in Starch

Research Project

Project/Area Number 61580072
Research Category

Grant-in-Aid for General Scientific Research (C)

Allocation TypeSingle-year Grants
Research Field 家政学
Research InstitutionKyoritsu Women's University, Faculty of Home Economics

Principal Investigator

NAKAZAWA Fumiko  Kyoritsu Women's University, Faculty of Home Economics, 家政学部, 教授 (60086725)

Co-Investigator(Kenkyū-buntansha) TAKAHASHI Junko  Kyoritsu Women's University, Faculty of Home Economics, 家政学部, 助手 (90146530)
Project Period (FY) 1986 – 1987
Project Status Completed (Fiscal Year 1987)
Budget Amount *help
¥1,900,000 (Direct Cost: ¥1,900,000)
Fiscal Year 1987: ¥600,000 (Direct Cost: ¥600,000)
Fiscal Year 1986: ¥1,300,000 (Direct Cost: ¥1,300,000)
KeywordsGelatinization of Starch / Retrogradation of Starch / Starch mixed with Sugar / Differential Scanning Calorimetry of Starch / 澱粉糊化のDSC / 老化澱粉のDSC / 砂糖添加澱粉の熱的性質
Research Abstract

1. Thermal properties of starch with sugar: Gelatinization and re-gelatinization after retrogradation of 10-50% starch with 0-200% sugar were studied by differential scanning calorimetry (DSC). Thermal spectra of re-gelatinization after retrogradation of starch with sugar were far different from those of gelatinization of the natural starch granule with sugar. The surface state of the natural granule may protect the starch from penetration of water molecules in the suger solution
The gelatinization temperature shifted to higher temperature as increase of the sugar concentration. Start temperature of the transition Ts, peak Tp, conclusion Tc were linearly increased with x, the fraction of sugar to water. It was expressed as Ts (Tp and Tc) =22x + 52 (60 and 71) C in the case of 20% starch. 2. Freezing of starch: Another endothermic peak appeared at -5 C lower side of the free water peak soon after freezing of gelatinization starch. It grew to about 10% of the melting energy of the free water during several days even at -18 C. DSC gives a sensitive method to detect the mobility of water at freezing temperature.

Report

(2 results)
  • 1987 Final Research Report Summary
  • 1986 Annual Research Report
  • Research Products

    (10 results)

All Other

All Publications (10 results)

  • [Publications] 中沢文子: New Food Industry. 28. 83-87 (1986)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 中沢文子: New Food Industry. 29. 75-82 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 野口駿: 日本家政学会誌. 38. 261-265 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 中沢文子,松本幸雄: "食品の物性第13集" 食品資材研究会, 10(210) (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] Fumiko Nakazawa: "Retrogradation Process of Gelatinized Starch Studied by Differential Scanning Calorimetry" New Food Industry. 28. 83-87 (1986)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] Fumiko Nakazawa: "Thermal Equilibrium State and Retrogradation Process of Starch-Water Mixture Studied by DSC" New Food Industry. 29. 75-82 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] Shun Noguchi: "Development of a method for Measuring the Unfrozen Water at -20C and its Aalication to some Sugar Solution" Journal of Home Economics of Japan. 38. 261-265 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] Fumiko Nakazawa (ed. by Sachio Matsumoto): Food Science (Part 13). Shokuhin Shizai Kenkyukai, 169-178 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 中沢文子: New Food Industry. 29. 75-81 (1987)

    • Related Report
      1986 Annual Research Report
  • [Publications] 山野善正 編: "食品の物性第13集" 食品資材研究会, (1987)

    • Related Report
      1986 Annual Research Report

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Published: 1987-03-31   Modified: 2016-04-21  

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