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Developemtn of Low temperture Surface Electron Mictoscpy and its Application to Gas Adsotption on Surfaces.

Research Project

Project/Area Number 61880011
Research Category

Grant-in-Aid for Developmental Scientific Research

Allocation TypeSingle-year Grants
Research Field 結晶学
Research InstitutionTokyo Institute of Technology

Principal Investigator

YAGI Katsumichi  Professor, Faculty of Science, 理学部, 教授 (90016072)

Co-Investigator(Kenkyū-buntansha) 高柳 邦夫  東京工業大学, 理学部, 助教授 (80016162)
TANISHIRO Yasumasa  Reserach Associate, Faculty of Science, 理学部, 助手 (40143648)
Project Period (FY) 1986 – 1987
Project Status Completed (Fiscal Year 1987)
Budget Amount *help
¥12,200,000 (Direct Cost: ¥12,200,000)
Fiscal Year 1987: ¥3,800,000 (Direct Cost: ¥3,800,000)
Fiscal Year 1986: ¥8,400,000 (Direct Cost: ¥8,400,000)
KeywordsSurface Electron Mictoscpy / Reflection Electron Mictoscpy / Si Surfaces / Oxygen on Si / Hydrogen on Si / 表面電子顕微鏡 / 反射電子顕微法 / シリコン表面
Research Abstract

Surface electron mictosopy has been developed for these several years as a method which shows surface structures and their dynamic processes with high spactial resolution. However, studies have been done on hot surfaces. On the other hand. low remperature surfaces are very inreresting problems and some interesting works have been done on alkali-metal atoms on Si surfaces. The purpose of the present project is to make a special specimen holder for the study of low temperture surfaces and to study adsorption fo gasses on surcaes.
The most difficult problem in the present project is to make a specimen holder. with which specimens can cooled for the obvservation and can be heated for cleaning. So that the speicmen should be thermally isolated during heating and it should thermally well contacted with the cooling reservoir, We used the characteristics of saphire crystal which is a good insulator at high temperatures byt is a good thermal conductor around 50K. It is as good as copper. We adopted a design of REM (reflection electron mictoscpy) holder which was developed by us for the studies of surfaces. Flow type cooling method is used where staianless tube cools a saphire frame of the specime holder and the specime can be cooles through the frame and the merallic electrode. Thus the heat floe during heating is refuced.
As a preliminary experiment, we studied chanages of surface structues and step configurations when the Si(001) and (111) surface are exposed to molecular exygen and atomec hydrogen. In the case of atomic hydrogen, so called delta 7x7 structure is formed bur step shapes do not change. They do not change when the hydrgen atoms atoms desorb from the surfaces. In the case of oxygen step shapes do not change but on hearing SiO or SiO2 is formed and step configuration chenges.
The method will be applide to solis gas adsoption problems.

Report

(2 results)
  • 1987 Final Research Report Summary
  • 1986 Annual Research Report
  • Research Products

    (8 results)

All Other

All Publications (8 results)

  • [Publications] 八木 克道: J.Appl.Cript.20. 147-160 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 八木克道,谷城康眞: Surfce.Sci. 191. 28-44 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 八木克道,谷城康眞: J.Vac.Sci.TeClr.A5. 1735-1738 (1987)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] N. Shimizu, Y.Tanishito, K.Takayanagi and K.Yagi: "On the vacancy formation and diffusion on tahe Si(111)7x7 surfaces under exposures loe oxygen prssure studied by in-situ reflection electron mictoscopy" Suface Sci.191. 28-44 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] K.Yagi: "Reflection Electron Mictosopy" J.Appi, Cryst.20. 28-44 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] S.Ogawa, Y.Tanishiro and K.Yagi: "Reflection electron microscope study of Pt(111) surfaces" J.Vac. Sci. Tech.A5. 1735-1738 (1987)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1987 Final Research Report Summary
  • [Publications] 八木克道: Proc.×1 th Int.Cong.n Electron Microscopy. 1. 79-82 (1986)

    • Related Report
      1986 Annual Research Report
  • [Publications] 太瀬憲寛 他: Jpn.J.Appl.Phys. (1987)

    • Related Report
      1986 Annual Research Report

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Published: 1987-03-31   Modified: 2016-04-21  

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