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Study on High Temperature Strength of Oxide-Dispersion-Strengthened Mechanical Alloy

Research Project

Project/Area Number 63460073
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 機械材料工学
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

OHTANI Ryuich  Department of Engineering Science, Faculty of Engineering, Kyoto University, Professor, 工学部, 教授 (50025946)

Co-Investigator(Kenkyū-buntansha) KITAMURA Takayuki  Department of Engineering Science, Faculty of Engineering, Kyoto University, Ins, 工学部, 助手 (20169882)
Project Period (FY) 1988 – 1989
Project Status Completed (Fiscal Year 1989)
Budget Amount *help
¥6,400,000 (Direct Cost: ¥6,400,000)
Fiscal Year 1989: ¥2,600,000 (Direct Cost: ¥2,600,000)
Fiscal Year 1988: ¥3,800,000 (Direct Cost: ¥3,800,000)
KeywordsOxide-dispersion-strengthened-superalloy / Mechanical alloy / Fracture at high temperature / Grain boundary / Fracture mechanics / Stochastic model / Computer simulation / メカニカルアロイ / 酸化物分散強化 / ODS合金 / 高温強度 / き裂伝ぱ / 微小き裂
Research Abstract

1. Crack propagation tests were conducted in creep-fatigue at 900 ゚C and 1000 ゚C in air using notched plate specimens of nickel base superalloy, Inconel MA754, which was an oxide (Y_2O_3) dispersion strengthened alloy made by mechanical alloying. The grains were elongated by directional recrystallization during the annealing process. As the crack tip approached a grain boundary perpendicular to the propagation direction on the specimen surface, the crack propagation drastically decelerated and temporarily halted. It implied that the grain boundaries were obstacles to the propagation. Despite of the microstructural inhomogeneity, the total area of crack increased smoothly because the randomness was averaged along the crack front through the specimen thickness of 5mm (10 grain diameters). The average crack propagation rate was correlated well with creep J-integral range which was a non-linear fracture mechanics parameter and represented the intensity of creep strain in the vicinity of crack tip.
2. The crack propagation tests were conducted in creep-fatigue at 800゚C and 900゚C in air using notched plate specimens of Inconel MA754 without the directional recrystallization and base alloy without the oxide particle dispersion, Nimonic 75. The cracks propagated smoothly and the propagation rate was correlated well with the creep J-integral range. The relations coincided with that of directionally recrystallized Inconel MA754 was far superior to the others in terms of the high temperature strength.
3. A stochastic model was developed for the random initiation and propagation of small cracks due to the microstructural effect. Three dimensional simulation was numerically carried out and the validity of model was examined by comparisons with experimental observation.

Report

(3 results)
  • 1989 Annual Research Report   Final Research Report Summary
  • 1988 Annual Research Report
  • Research Products

    (50 results)

All Other

All Publications (50 results)

  • [Publications] 大谷隆一: "SUS304の高温低サイクル疲労微小表面き裂の発生と初期成に及ぼすひずみ波形および高温酸化の影響" 日本機械学会講演論文集. No.880-2. 43-48 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 大谷隆一: "粒界破壊抵抗分布モデルによるクリ-プ疲労微小き裂の発生と初期伝ぱのシミュレ-ション" 日本機械学会論文集(A編). 54. 1312-1316 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 栗山義英: "耐熱鋼のクリ-プ疲労微小き裂の発生と成長に関する研究" 日本材料学会第26回高温強度シンポジウム前刷集. 94-98 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] Takayuki Kitamura: "Stochactic Modeling of Crack Initiation and Short-Crack Growth Under Creep and Creep-Fatigue Conditions" NASA Technical Memorandum 101358. (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R.Ohtani: "Behavior of Initiation and Growth of Creep and Creep-Fatigue Small Cracks in Austenitic Stainless Steels" “Advances in Fracture Research"Proc.7th International Conference on Fracture,Pergamon press. 1. 213-221 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] Takayuki Kitamura: "Creep Life Prediction Based on Stochastic Model of Microstructurally Short Crack Growth" J.of Engineering Materials and Technology,Trans.ASME. 111. 169-175 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R.Ohtani: "Numerical Simulation of Initiation and Early Propagation of Creep-Fatigue Small Cracks Based on a Model of Random Fracture Resistance of Grain Boundaries" “Structural Design for Elevated Temperature Environments-Creep,Ratchet,Fatigue,and Fracture",ASME PVP. 123-127 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T.Kitamura: "Stochastic Damage Variable Based on Randomly Distributed Micro-Cavities During Creep" “Advances in Plasticity 1989",Proc.of PLASTICITY'89,Pergamon Press. 687-690 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 大谷隆一: "SUS304の高温における一方向引張とクリ-プ疲労の微小き裂発生・成長挙動の相違" 材料. 38. 1067-1072 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 楊王〓: "交流電位差法を用いたSUS304とTi-17の荷重制御下およびき裂中央開口変位制御下のクリ-プ疲労き裂伝ぱ試験" 材料. 38. 1409-1414 (1989)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 大谷隆一: "電位差法における表面半楕円き裂形状・寸法測定" 日本機械学会論文集(A編). 56. 259-264 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 大谷隆一: "クリ-プ疲労条件下の微小き裂発生・成長に及ぼす圧縮ひずみ速度の影響" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 北村隆行: "たたみこみ積分法による3次元微小クリ-プおよびクリ-プ疲労き裂発生確率の解析的検討" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 北村隆行: "SUS304の結晶粒界長さおよび角度分布とそのクリ-プ疲労微小き裂発生・成長に及ぼす影響" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 多田直哉: "三次元粒界破壊抵抗分布モデルによるクリ-プ疲労微小き裂のモンテカルロ・シミュレ-ション" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] 大谷隆一: "耐熱金属平滑材のクリ-プ疲労下における表面微小き裂発生・成長挙動" 材料 掲載予定. 39. (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Effect of Strain Wave form and Environment on Small Crack Initiation and Early Growth in Low-Cycle Fatigue of SUS304 at High Temperature" Preprint of JSME Symposium, No.880-2, pp.43-48, 1988.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Simulation of Initiation and Early Propagation of Creep-Fatigue Small Cracks Based on the Model of Random Fracture Resistance of Grain Boundaries" Trans. JSME (Ser.A), Vol.54, pp.1312-1316, 1988.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] Y. Kuriyama: "Initiation and Growth of Creep-Fatigue Small Cracks in Heat-Resistant Steels" Preprint of the 26th Symposium on High Temperature Strength of Materials, JSMS, pp.94-98, 1988.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T. Kitamura: "Stochastic Modeling of Crack Initiation and Short-Crack Growth Under Creep and Creep-Fatigue Conditions" NASA Technical Memorandum 101358, 1988.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Behavior of Initiation and Growth of Creep and Creep-Fatigue Small Cracks in Austenitic Stainless Steels" "Advances in Fracture Research", Proc. 7th International Conference on fracture, Pergamon Press, Vol.1, pp.213-221, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T. Kitamura: "Creep Life Prediction Based on Stochastic Model of Microstructurally Short Crack Growth" J. of Engineering Materials and Technology, Trans. ASME, Vol.111, pp.169-175, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Numerical Simulation of Initiation and Early Propagation of Creep-Fatigue Small Cracks Based on a Model of Random Fracture Resistance of Grain Boundaries" "Structural Design for Elevated Temperature Environments - Creep, Ratchet, Fatigue, and Fracture", ASME PVP, pp.123-127, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T. Kitamura: "Stochastic Damage Variable Based on Randomly Distributed Micro-Cavities During Creep" "Advances in Plasticity 1989", Proc. of PLASTICITY '89, Pergamon Press, pp.687-690, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Difference Between Monotonic Tension and Creep-Fatigue in the Behavior of Small Crack Initiation and Early Growth of 304 Stainless Steel at Elevated Temperature" J. of Society of Materials Science, Japan, Vol.38, pp.1067-1072, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] W. Yang: "Creep-Fatigue Crack Propagation Tests of SUS304 and Ti-17 Under Load Control and Crack Center Opening Displacement Control Using A.C. Electric Potential Method" J. of Society of Materials Science, Japan, Vol.38, pp.1409-1414, 1989.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] N. Tada: "Electric Field Analysis for Determination of Shape and Size of Semi-Elliptical Surface-Crack by Means of D.C. Potential Drop Technique" Trans. JSME (Ser.A). Vol.56, pp.259-264, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Effect of Compression-Going Strain Rate on Initiation and Growth of Small Cracks Under Creep-Fatigue Condition" Trans. JSME (Ser.A). Vol.56, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T. Kitamura: "Stochastic Analysis of Small Crack Initiation in Creep and Creep-Fatigue by the Convolution Integral Method" Trans. JSME (Ser.A). Vol.56, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] T. Kitamura: "Distribution of Grain-Boundary Length and Inclination of Type 304 Stainless Steel and Its Effects on Small Crack Initiation and Growth Under Creep-Fatigue Conditions" Trans. JSME (Ser.A). Vol.56, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] N. Tada: "Monte Carlo Simulation of Creep-Fatigue Small Cracks Based on a Three-Dimensional Model of Random Fracture Resistance of Grain Boundaries" Trans. JSME (Ser.A). Vol.56, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R. Ohtani: "Surface Small Crack Initiation and Growth of Heat Resisting Alloys in Creep-Fatigue" J. of Society of Materials Science, Japan, Vol.39, 1990.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1989 Final Research Report Summary
  • [Publications] R.Ohtani: "Behavior of Initiation and Growth of Creep and Creep-Fatigue Small Cracks in Austenitic Stainless Steels" “Advances in Fracture Research"Proc.7th International Conference on Fracture,Pergamon Press. 1. 213-221 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] Takayuki Kitamura: "Creep Life Prediction Based on Stochastic Model of Microstructurally Short Crack Growth" J.of Engineering Materials and Technology,Trans.ASME. 111. 169-175 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] R.Ohtani: "Numerical Simulation of Initiation and Early Propagation of Creep-Fatigue Small Cracks Based on a Model of Random Fracture Resistance of Grain Boundaries" “Structural Design for Elevated Temperature Environments-Creep,Ratchet,Fatigue,and Fracture",ASME PVP. 123-127 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] T.Kitamura: "Stochastic Damage Variable Based on Randomly Distributed Micro-Cavities During Creep" “Advances in Plasticity 1989",Proc.of PLASTICITY '89,. 687-690 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] 大谷隆一: "SUS304の高温における一方向引張とクリ-プ疲労の微小き裂発生・成長挙動の相違" 材料. 38. 1067-1072 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] 楊王〓: "交流電位差を用いたSUS304とTi-17の荷重制御下およびき裂中央開口変位制御下のクリ-プ疲労き裂伝ぱ試験" 材料. 38. 1409-1414 (1989)

    • Related Report
      1989 Annual Research Report
  • [Publications] 大谷隆一: "電位差法における表面半楕円き裂形状・寸法測定" 日本機械学会論文集(A編). 56. 259-264 (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 大谷隆一: "クリ-プ疲労条件下の微小き裂発生・成長に及ぼす圧縮ひずみ速度の影響" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 北村隆行: "たたみこみ積分法による3次元微小クリ-プおよびクリ-プ疲労き裂発生確率の解析的検討" 日本機械学会論文集(A編)掲載予定. 56. (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 北村隆行: "SUS304の結晶粒界長さおよび角度分布とそのクリ-プ疲労微小き裂発生・成長に及ぼす影響" 日本機械学会論文集(A編). 56. (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 多田直哉: "三次元粒界破壊抵抗分布モデルによるクリ-プ疲労微小き裂のモンテカルロ・シミュレ-ション" 日本機械学会論文集(A編). 56. (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 大谷隆一: "耐熱金属平滑材のクリ-プ疲労下における表面微小き裂発生・成長挙動" 材料. 39. (1990)

    • Related Report
      1989 Annual Research Report
  • [Publications] 大谷隆一: 日本機械学会論文集(A編). 54. 1312-1316 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 大谷隆一: 日本機械学会講演論文集. No.880ー2. 43-48 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 大谷隆一: 第32回材料研究連合講演会前刷集. 215-220 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 栗山義英: 日本材料学会第26回高温強度シンポジウム前刷集. 94-98 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 楊王〓: 材料.

    • Related Report
      1988 Annual Research Report
  • [Publications] Ryuichi,Ohtani: 7th International Conference on Fractureにて発表予定. (1989)

    • Related Report
      1988 Annual Research Report

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Published: 1988-04-01   Modified: 2016-04-21  

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