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Kinematical Study on the Densification Process During Pressure Sintering of Alloy Powder Utilizin Superplasticity.

Research Project

Project/Area Number 63460198
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 金属加工(含鋳造)
Research InstitutionRitsumeikan University

Principal Investigator

TOKIZANE Masaharu  Ritumeikan University, Mechanical Professor Engineering,, 理工学部, 教授 (50066528)

Co-Investigator(Kenkyū-buntansha) AMEYAMA Kei  Ritumeikan University, Mechanical Assistant Engineering,, 理工学部, 助手 (10184243)
Project Period (FY) 1988 – 1990
Project Status Completed (Fiscal Year 1990)
Budget Amount *help
¥4,900,000 (Direct Cost: ¥4,900,000)
Fiscal Year 1990: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1989: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 1988: ¥2,900,000 (Direct Cost: ¥2,900,000)
KeywordsZn-22%Al Alloy Powder / SCr420 Steel / TiNi Shape Memory Alloy / Vacuum Hot Pressing / Densification Mechanism Map / PREP Powder / Superplasticity / Pre-strain / TiNi / ホットプレス / 緻密化 / 形状記憶 / Zm-22%Al合金粉末 / 真空ホットプレス
Research Abstract

An application of superplastic behavior for the pressure sintering of the alloy powder was investigated in the present study.
As a fundamental study, the effects of the microstructure of the powder on the densification behavior during vacuum hot pressing (VHP) of Zn-22%Al alloy powder at 523 K was clarified based on the theoretical equation and densification mechanism map. Namely, the powder consists of fin microduprex structure was dencified by superplastic deformation in the limited range of relative density and applied pressure, while the powder consists of lamellar structure was densified according to the power low creep behavior.
As the first application of the fundamental knowledge mentioned above, the effects of thermomechanical treatment which performed by combination of priorball milling and vacuum hot pressing on the densification process of SCr420 steel powder produced by plasma rotating electrode process (PREP) was examined. The results showed that the densification of the thermomechanically treated powder progressed by superplastic deformation of the powder during VHP, and the compact was composed of fine grained ferrite and spheroidized cementite particles.
As the second application in the present study, we performed the examination of the densification of TiNi shape memory alloy powder produced by PREP. In this case, the densification process at temperatures from 973 to 1173 K was accelerated by prior ball milling of the powder due to considerable grain refinement. Such a grain refinement became the noticeable increase in the shape recovery strength.

Report

(4 results)
  • 1990 Annual Research Report   Final Research Report Summary
  • 1989 Annual Research Report
  • 1988 Annual Research Report
  • Research Products

    (19 results)

All Other

All Publications (19 results)

  • [Publications] M.Tokigane,K.Isomishi,M.Hashii,K.Ameyama: "The effects of Microstructure of gasーatomized Znー22%Al Alloy Powder on Densification Process During Hot Pressing" Modern Revelopments im Powder Metallungy. 20. 675-680 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 磯西 和夫,橋井 光弥,時実 正治: "Znー22%Al合金粉末のホットプレスにおける緻密化機構図" 鉄と鋼 4月号(No.4). 77. (1991)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 磯西 和夫,橋井 光弥,時実 正治: "Znー22%合金粉末を用いた超塑性ホットプレス" 材料とプロセス(日本鉄鋼協会講演論文集). 1. 1146-1149 (1988)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 磯西 和夫,滝川 裕之,時実 正治: "低合金鋼粉末のホットプレス過程における組織変化と機械的性質" 日本塑性加工学会春期講演会予稿集. 685-686 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 磯西 和夫,滝川 裕之,時実 正治: "低合金鋼粉末の緻密化挙動に及ぼすホットプレス法の影響" 日本塑性加工学会春期講演会予稿集. 687-690 (1990)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] M. Tokizane, K. Isonishi, M. Hashii, K. Ameyama: "The effects of Microstructure of gas-Atomized Zn-22%Al Alloy Powder on Densification Process During Hot Pressing" Modern Developments in Powder Metallurgy. Vol. 20. 675-680 (1988)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Isonishi Kazuo, Hoshii Mitsuya, Tokizane Masaharu: "Densification Mechanism Maps of Zn-22%Al Alloy Powder Based on Hot Pressing" Tetsu-to-Hagane. Vol. 77, No. 4. (1991)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] M.Tokizane,K.Isonishi,M.Hashii,,K.Ameyama: "The effects of Microstructure of Gasーatomized Znー22%Al Alloy powder on Densification Process During Hot Pressing" Modern Developments in Powder Metallurgy. 20. 675-680 (1988)

    • Related Report
      1990 Annual Research Report
  • [Publications] 磯西 和夫,橋井 光弥,時実 正治: "Znー22%Al合金粉末のホットプレスにおける緻密化機構図" 鉄と鋼. 77. 4(NO4) (1991)

    • Related Report
      1990 Annual Research Report
  • [Publications] 磯西 和夫,橋井 光弥,時実 正治: "Znー22%Al合金粉末を用いた超塑性ホットプレス" 材料とプロセス(日本鉄鋼協会構演論文集). 1. 1146-1149 (1988)

    • Related Report
      1990 Annual Research Report
  • [Publications] 磯西 和夫,滝川 裕之,時実 正治: "低合金鋼粉末のホットプレス過程における組織変化と機械的性質" 日本塑性加工学会春期講演会予稿集. 685-686 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] 磯西 和夫,滝川 裕之,時実 正治: "低合金鋼粉末の緻密化挙動に及ぼすホットプレス法の影響" 日本塑性加工学会春期講演会予稿集. 687-690 (1990)

    • Related Report
      1990 Annual Research Report
  • [Publications] M.Tokizane,K.Isonishi,M.Hashii,K.Ameyama: "The Effects of Microstructure of Gas-atomized Zn-22%Al Alloy Powder on Densification Process During Hot Pressing" Modern Developments in Powder Metallurgy. 20. 675-680 (1988)

    • Related Report
      1989 Annual Research Report
  • [Publications] 磯西和夫,橋井光弥,時実正治: "Znー22%合金粉末を用いた超塑性ホットプレス" CAMPーISIJ. 1. 1146-1149 (1988)

    • Related Report
      1989 Annual Research Report
  • [Publications] 磯西和夫,滝川裕之,時実正治: "低合金鋼粉末の緻密化挙動に及ぼすホットプレス方法の影響" 日本塑性加工学会誌(塑性と加工).

    • Related Report
      1989 Annual Research Report
  • [Publications] 磯西和夫,滝川裕之,時実正治: "低合金鋼粉末のホットプレス過程における組織変化と機械的性質" 日本塑性加工学会誌(塑性と加工).

    • Related Report
      1989 Annual Research Report
  • [Publications] M.Tokizane;K.Isonishi;M.Hashii;K.Ameyama: Modern Development in Powder Metallurgy. 20. 675-680 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 磯西和夫,橋井光弥,時実正治: 材料とプロセス(日本鉄鋼協会講演論文集). 1. 1446-1449 (1988)

    • Related Report
      1988 Annual Research Report
  • [Publications] 磯西和夫,橋井光弥,飴山恵,時実正治: 「鉄と鋼」に発表の予定. (1988)

    • Related Report
      1988 Annual Research Report

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Published: 1988-04-01   Modified: 2016-04-21  

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