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A study on the Evaluation of Crystal Perfection by Means of the Measurement of Static Debye-Waller factors in the Pendellosung Oscillations

Research Project

Project/Area Number 63490012
Research Category

Grant-in-Aid for General Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 広領域
Research InstitutionUniversity of Toyama

Principal Investigator

SUGITA Yoshimitsu  Toyama University, Faculty of Science, Professor, 理学部, 教授 (20134992)

Co-Investigator(Kenkyū-buntansha) IIDA Satoshi  Toyama University, Faculty of Science, Research Associate, 理学部, 助手 (50168069)
Project Period (FY) 1988 – 1989
Project Status Completed (Fiscal Year 1990)
Budget Amount *help
¥7,000,000 (Direct Cost: ¥7,000,000)
Fiscal Year 1989: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 1988: ¥6,200,000 (Direct Cost: ¥6,200,000)
KeywordsEvaluation of Crystal Perfection / Crystal Inclination Method / Pendellosung Oscillation / Static Debye-Waller Factor / III-V Compound Semiconductor / Silicon / 結晶評価法 / 静的デバイワラ-因子 / 半導体結晶材料 / 静的デバイワラー因子
Research Abstract

The crystal inclination method has been applied to the evaluation of the crystalline perfection of undoped semi-insulating liquid-encapsulated Czochralski (LEC) and silicon doped horizontal Bridgman (HB) GaAs crystals. The results obtained in this study are summarized in the following.
(1) The static Debye-Waller factor in the as-grown LEC crystals was smaller than that of the LEC crystals subjected to the three-step annealing process. That is, the annealed crystals have more crystal perfection than the as-grown crystals.
(2) No change could be recognized in the static Debye-waller factors of the HB crystals having the dislocation density from zero to 1x10^<-4>cm^2.
(3) There was no substantial change in the static Debye-Waller factors between the as-grown LEC crystals having dislocation density of 2.5x10^4cm^2 and the HB crystals having silicon impurities of 2x10^<18>cm^<-3> and dislocation density of zero to 1x10^<14>cm^<-2>.(4) In addition, the measurements were made on Czochralski silicon crystals annealed at 800^゚C for 150h. The experimental results were analyzed using the statistical dynamical theory. The static Debye-Waller factor and correlation length were determined. The static Debye-Waller factor obtained in this study coincided with the static Debye-Waller factor which was determined by different method, the Pendellosung fringe in the section topography.
(5) X-ray topographic observation of GaAs crystals showed that there was a strong interaction between dislocation and impurities or point defects.

Report

(3 results)
  • 1990 Final Research Report Summary
  • 1989 Annual Research Report
  • 1988 Annual Research Report
  • Research Products

    (5 results)

All Other

All Publications (5 results)

  • [Publications] S.Iida,K.Ueda and Y.Sugita: "Evaluation of the crystal perfection of semiconducotr crystals by Pendellosung oscillation" Japanese Journal of Applied Physics.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Y.Sugita,S.Iida,S.Takasaki and K.Ueda: "Xーray topographic observation of defect structures in GaAs crystals" Japanese Journal of Applied Physics.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] S. Iida, K. Ueda and Y. Sugita: "Evaluation of the crystal perfection of semiconductor crystals by Pendellosung oscillation" Japanese Journal of Applied Physics.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] Y. Sugita, S. Iida, S. Takasaki and K. Ueda: "X-ray topographi observation of defect structures in GaAs crystals" Japanese Journal of Applied Physics.

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      1990 Final Research Report Summary
  • [Publications] 飯田敏 他: "Application of the Single Crystal Inclination Method to Study on Microdefects in Silicon(仮題)" Japan,J.Appl,Phys.

    • Related Report
      1989 Annual Research Report

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Published: 1988-04-01   Modified: 2016-04-21  

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