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1992 Fiscal Year Final Research Report Summary

Soft Magnetic Thin Films Composed of Ultra Fine Crystallites

Research Project

Project/Area Number 03555152
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field 金属材料(含表面処理・腐食防食)
Research InstitutionTohoku University

Principal Investigator

FUJIMORI Hiroyasu  Inst. for Mater. Res. Tohoku Univ. Prof., 金属材料研究所, 教授 (60005866)

Co-Investigator(Kenkyū-buntansha) OBI Yoshihisa  Inst.for Mater. Res. Tohoku Univ. R. Assoc., 金属材料研究所, 助手 (80005925)
MORITA Hiroaki  Inst. for Mater. Res. Tohoku Univ. A. Prof., 金属材料研究所, 助教授 (50005914)
HASEGAWA Naoya  Alps Cor. Ltd. Researcher, 研究員
TAKANASHI Koki  Inst. for Mater. Res. Tohoku Univ. R. Assoc., 金属材料研究所, 助手 (00187981)
KATAOKA Noriyuki  Fac. of Engi. Tohoku Univ. A. Prof., 工学部, 助教授 (90194761)
Project Period (FY) 1991 – 1992
KeywordsNano-crystal / Multilayer / Metastable alloy / Soft Magnetism / Magnetoresistance / Magnetostriction / Sputtering
Research Abstract

Soft Magnetic Properties of Fe Based Nano-Crystalline Thin Films: FeHFC then films and Fe/FeHFC multilayered thin films were prepared by a sputter method. The FeHFC was amorphous in the as-prepared state, while it transformed into the mano-crystalline state by a heat treatment. The Fe layers were in the nano-crystalline state even without heat treatment. As a result, both the films showed excellent soft magnetic properties. Particularly, the Fe/FeHFC multilayers were superior in high magnetic induction, because of the high concentration of Fe. In addition. it was found that the nano-crystalline state in the multilayers was stable up to high temperatures as about 700゚C. The stability was thought to be attributed to the pinning effect of the HFC fine crystallites precipitated at the boundaries of Fe fine crystallites.
Giant Magnetoresistance in Co-Fe/Cu and Co-X/Cu Multilayered Thin Films: It was found that the magnetostriction depended on the alloying elements into Co and about 10 at% of Fe gave rise to an enhanced magnetoresistance, larger than that of Co/Cu multilayer. Moreover, we succeeded to reduce the magnetic field for exciting magnetoresistance in the new multilayer of Co-Fe/Cu/Co-Fe.
Magnetostriction in TbFe_2-B and SmFe_2-B Amorphous Alloys: Huge magnetostrictions saturated easyly in low magnetic fields (about 60 x 10^<-6> at 200 Oe) were obtained in TbFe_2-B and SmFe_2-B amorphous alloys prepared by a high rate sputtermethod.

  • Research Products

    (32 results)

All Other

All Publications (32 results)

  • [Publications] 長谷川 直也: "高飽和磁化,高耐熱性を有するFe/Fe-Hf-C多層膜の軟磁気特性" 日本応用磁気学会誌. 15. 403-406 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "Effect of Ar-ion Bombardment on Soft Magnetic Properties of Fe and Fe-Hf Films Produced by Dual-Type Ion Beam Sputtering" Sci.Rep.RITU.36. 36-47 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "High frequency permeability of nanocrystalline Fe-Cu-Nb-Si-B single and multilayer films" J.Appl.Phys.70. 6238-6240 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.HASEGAWA: "Structural and soft magnetic properties of Fe/Fe-Hf-C multilayered films with the high Bs and thermal stability" J.Appl.Phys.70. 6253-6255 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "Magnetoresistance of Fe-Co/Cu metallic multilayer and its annealing effect" Mater.Trans.JIM.33. 151-154 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 潟岡 教行: "Fe-Co合金の磁歪の希土類元素添加による制御" 日本応用磁気学会誌. 16. 235-238 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 長谷川 直也: "炭化物分散Fe-Si-Hf-C微結晶膜の軟磁気特性" 日本応用磁気学会誌. 16. 253-256 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.SHIMA: "Soft Magnetic Properties of Nanocrystalline Fe-Cu-Nb-Si-B Thin Films and Multilayers" Sci.Rep.RITU.36. 224-238 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.HASEGAWA: "Microstructure of Carbide-Dispersed Nanocrystalline Fe-Ta-C Films" Mater.Trans.,JIM. 33. 632-635 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 嶋 敏之: "Fe-Co-RE(RE;希土類金属)系DC3極スパッタ膜の磁歪および磁気特性" 日本応用磁気学会誌. 17. 337-340 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.HASEGAWA: "SOFT MAGNETIC PROPERTIES OF CARBIDE-DISPERSED MANOCRYSTALLINE FILMS WITH HIGH THERMAL STABILITY" ASM's J.Mater.Eng.Performance.

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "Mossbauer study and soft magnetic properties of nanocrystalline Fe-Hf-C films" Nuclear Instruments and Methods on Physics Research. Section B. (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "Magnetoresistance of Co-X/Cu multilayers" J.Magn.Magn.Mater.(1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.FUJIMORI: "THERMAL STABILITY OF NANOCRYSTALLINE MULTILAYERED STRUCTURE IN SOFT-MAGNETIC Fe/Fe-Hf-D FILMS" J.Magn.Magn.Mater.(1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.KATAOKA: "Magnetoresistance of Co_<90>Fe_<10>/Cu_XFe_<100-X>/Cu metallic multilayers" J.Magn.Magn.Mater.(1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.HASEGAWA: "Relation between microstructure and soft magnetic properties of nanocrystalline Fe/Fe-Hf-C multilayers" J.Magn.Magn.Mater.(1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.FUJIMORI: "Hugh magnetoresistance of amorphous bulk (Sm,Tb)Fe_2-B with low exciting fields" J.Magn.Magn.Mater.(1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 長谷川 直也: "炭化物分散型超微細粒軟磁性薄膜材料" 日本金属学会会報. 30. 685-694 (1991)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 潟岡 教行: "合金化によるFe系薄膜の微細化と軟磁気特性" 日本金属学会会報. 31. 34-40 (1992)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Kataoka,Noriyuki: "Effect of Ar-ion Bombardment on Soft Magnetic Properties of Fe and FeHF Films Produced by Dual-type Ion Beam Sputtering" Sci. Rep. RITU. 36. 36-47 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kataoka,Noriyuki: "High Frequency Permeability of Nanocrysatlline Fe-Cu-Nb-Si-B Single and Multilayer Films" J. Appl. Phys.70. 6238-6240 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hasegawa,Naoya: "Structural and Soft Magnetic Properties of Fe/FeHFC Multilayered Films with The High B_s and Thermal Stability" J.Appl. Phys.70. 6253-6255 (1991)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kataoka,Noriyuki: "Magnetoresistance of Fe-Co/Cu Metallic Multilayers and Its Annealing" Mater. Trans. Trans.33. 151-154 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Shima,Toshiyuki: "Soft Magnetic Properties of Nanocrystalline Fe-Cu-Nb-Si-B Thin Films and Multilayers" Sci. Rep. RITU. 36. 224-238 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hasegawa,Naoya: "Microstructure of Carbide-Dispersed Nanocrystalline Fe-Ta-C Films" Mater. Trans. JIM. 33. 632-635 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hasegawa,Naoya: "Soft Magnetic Properties of Carbide-Dispersed Nanocrystalline Films with High Thermal Stability" ASM's J. Mater. Eng. (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kataoka,Noriyuki: "Mossbauer Study and Soft Magnetic Properties of Nanocrystalline Fe-HF-C Films" Nuclear Instru. and Method on Phys. Res.(1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kataoka,Noriyuki: "Magnetoresistance of Co-X/Cu Multilayers" J. Magn. Mater.(1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Fujimori,Hiroyasu: "Thermal Stability of Nanocrystalline Multilayered Strucuture in Soft Magnetic Fe/FeHFC Films" J. Magn. Magn. Mater.(1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kataoka,Noriyuki: "Magnetoresistance of Co_<90>Fe_<10>/Cu/Co_xFe_<1-x>/Cu Metallic Multilayers" J.Magn. Magn. Mater.(1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hasegawa,Naoya: "Relation Between Microstructure and Soft Magnetic Properties of Nanocrystalline Fe/FeHfC Multilayers" J.Magn. Magn. Mater.(1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Fujimori,Hiroyasu: "Huge Magnetostriction of Amorphous Bulk (Sm,Tb)Fe_2-B with Low Exciting Fields" J.Magn. Magn. Mater.(1992)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1994-03-24  

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